Jo,Kyung-Yul

조경열,최윤수,석경순 대구효성가톨릭대학교 1986 연구논문집 Vol.32 No.1

A new spectropotometric determination of citric acid was examined using carbonyldiimidazole (CDI) which has been used in petide synthesis. CDI was reacted with citric acid to form yellow acyl-imidazole derivative (λ??443nm) in dichloroethane. This colored reaction was so characteristic with tricarboxylic acid that can be used selective determination of citric acid in common carboxylic acid. As increasing the reaction temperature, the acyl compound was decomposed to produce the substance of which physical property was similar to the hydrolized compound. Citric acied was calibrated in the range of 1-6μg/ml and the extinction coefficient of the acyl-imidazole compound was 28000 in this condition.

한열변증에 따른 중풍 환자의 제반특성 비교

김민경,이인환,신애숙,김나희,김혜미,심소라,나병조,조승연,박성욱,정우상,문상관,박정미,고창남,조기호,김영석,배형섭,Kim, Min-kyung,Lee, ln-whan,Shin, Ae-sook,Kim, Na-hee,Kim, Hye-mi,Shim, So-ra,Na, Byung-Jo,Cho, Seung-yeon,Park, Seong-uk,Jung, Woo Sang 대한중풍순환신경학회 2010 대한중풍.순환신경학회지 Vol.11 No.1

Object : This study was conducted as part of the national project to standardize stroke diagnosis in Korean medicine. In this study, we aimed to evaluate the characteristics of acute stroke between heat pattern group and cold pattern group. Methods : We recruited stroke patients from 5 universities(Kyung-Hee University oriental medical center, Kyung-Hee University East-West Neo medical center, Kyungwon university lncheon oriental medical center, Kyungwon university Songpa oriental medical center and DongGuk university llsan oriental medical center) from April, 2007 until February, 2010. We diagnosed them and selected 463 heat pattern patients and 182 cold pattern patients. Results : We find that the risk factor of smoking, alcohol, diet(prefer to meat) are more associated with the heat pattern group. On the other hand, inflammation history in recent 3 months and diet(prefer to sea food) are more associated with the cold pattern group. RBC, Hg, Hct, TG, CK and Cl are more related to the heat pattern group. CPT, total cholesterol and HDL are more related to the cold pattern group. Tae-eum type takes high distribution of the heat pattern group, and So-eum type takes high distribution of the cold pattern group. Conclusions : This study provides evidence that the heat pattern group have more risk factor than the cold pattern group.

황남대총 98호분 출토 유리의 과학적 분석

조경미,유혜선,강형태 국립중앙박물관 1999 박물관보존과학 Vol.1 No.-

황남대총 98호분 북분과 남분에서 출토된 유리시료 40점에 대한 과학적인 분석을 실시하였다. 유리의 성분조성은 주사전자현미경-에너지분산형분광기(SEM-EDS)를 사용하여 정량분석 하였고 다변량해석법을 통하여 시료를 분류하였다. 그 결과 시료 40점 모두 Na₂O를 약 20%정도 함유한 소다-석회(Na₂O CaO-SiO₂)유리임을 확인하였으며, 다시 5개 주성분(SiO₂, AI₂O₃, Na₂O, CaO, K₂O)으로 다변량해석[주성분분석(PCA)]을 실시한 결과 2개의 群으로 분류되었다. I 群에 포함된 시료는 Al₂O₃의 농도가 9.7%로 높고 CaO의 농도는 2.2%인데 비하여 Ⅱ群에서는 각각 3.2%,4.9%의 범위로 나타났다. 특히 시료 No.12의 노란 색으로 편석된 부분을 미소부위 XRD로 분석한 결과 PbSnO₃임을 국내 최초로 확인할 수 있었다. 鉛을 함유한 시료 중 No.12, 17은 열이온화질량분석기(TIMS)로 납동위원소비를 측정하였고 선형판별식 분석법(SLDA)을 이용하여 납의 산지를 추정하였다. 그 결과 각각 중국 남부, 한국 남부의 납광석을 사용한 것으로 나타났다. Elemental analysis of 40 glass samples from the Northern Tomb and the Southern Tomb of Hwangnam-daechong No. 98 was performed. Fourteen compositions of each sample were analyzed quantitatively by SEM-EDS and glass samples were classified by multivariate analysis such as PCA. All of 40 samples were confirmed to be Na₂O CaO-SiO₂ system with about 20% of Na₂O. Samples were classified into two groups by doing PCA on concentrations of 5 major elements (SiO₂, AI₂O₃, Na₂O, CaO, K₂O). Samples included in group I showed the concentration of AI₂O₃ is about 9.7% and that of CaO, about 2.2%. In group II, concentration of Al₂O₃ is about 3.2% and that of CaO, about 4.9%. Especially yellow grains embedded in sample No.12 were shown to be PbSnO₃ by micro XRD, which was the first coloring material ever found in Korea. Lead isotope ratios of samples No.12 and No.17 which contained lead were measured by TIMS. The origin of lead was traced by means of multivariate analysis such as SLDA. The result showed that lead from southern China and southern Korea had been used for making glass.

CIRCULAR THIN LAYER CHROMATOGRAPHY에 依한 無機 ION의 分離

趙庚烈 대구효성가톨릭대학교 1970 연구논문집 Vol.6 No.1

The conclusion of this experiment was carried out apply to circular thin layer chromatography method. 1. Chrular thin layer chromatography can analysis ions more easily than paper chromatography in a short space of time. 2. When the Rf value is needed to calculate, thin layer chromatography can be seperated easily without piling up each other, result from the solvent developped in fan form and make a narrow, long zone. Therefore, circular developping is very convenient to certify the unknown samples. 3. Cirular thin layer chromatography is more convenient for applying the most part of drug analysis than the other method. 4. Comparing cirular thin layer chromatography with previous analysis, that method has a merit to be done with extreme minimum sample amount. 5. As I explained above, this circular thin layer chromatography equipment can apply any kind of samples within the constant developping speed, and the constant developping time.

Ferric Ammonium Sulfate에 依한 Tannic Acid의 定量에 關한 硏究

趙庚烈 대구효성가톨릭대학교 1974 연구논문집 Vol.14 No.1

The study on tannic acid colirimetric determination was attempted with ferric ammonium sulfate. Concentration of tannic acid, then used, was 3.1×10-4M.∼1.2×10-3M., and that of ferric ammonium sulfate 2.0×10-4%. The two 325㎛ and580㎛ peaks apperaed on absorption curve, and the former was used, in this determination. The caribration curve was drawn at about pH value 3.7, and 325㎛. The analytical method mentioned above was applied to a number of cases, and was found comparatively good result.

주걱송편버섯(Pycnoporus cinnabarinus) SCH-3의 Laccase 생산에 미치는 유도원의 영향

조경언,이현수,윤경하 순천향대학교 기초과학연구소 2004 순천향자연과학연구 논문집 Vol.10 No.2

This study was performed to examine the effect of inducer on laccase production of Pycnoporus cinnabarinus SCH-3 isolated from Korea. The different inducers including 2,5-xylidine were added in the culture of Pycnoporus cinnabarinus SCH-r respectively. 2,5xylidine was predominant of the inducers tested in laccase production. Addition of 2,5-xylidine enhanced 12-fold laccase production, While nothing of inducers produced isoenzyme of laccase, as determined by non-denaturing polyacrylamide gel electrophoresis.

유압 윈치 CLD시스템의 제어

조중선,정경욱 國立 昌原大學校 産業技術硏究所 1995 産技硏論文集 Vol.9 No.-

Control of an electro-hydraulic servo-controlled winch system which has no distinct performance specifications is investigated in this paper. Because of the lack of the performance specification, the research is focused to finding effective parameters which give clear physical meanings for the behavior of the system. Two new parameters named "settling rotation angle" and "settling safety ratio" are proposed for the control of general winch system. The physical meanings of the two parameters are explained precisely. Performance specifications for the target winch system are derived by using the proposed two parameters and a controller is designed to meet the performance specifications. Simulation results show that the designed controller gives responses which can be accepted for the target winch system. The concepts of the new design parameters proposed in this paper can be applied to any kind of servo-controlled winch systems.

카페인 섭취가 400M 자유형 기록에 미치는 영향

조인호,이병두,장경태 韓國體育大學校 1997 論文集 Vol.20 No.-

The purpose of this study was to investigate the ergogenic benefit of caffeine in the performance of a 400 meter swim. Caffeine(5mg/kg) or placebo was administered one hour prior to the swim trial in a double-blind crossover design. Swimming time in each 100m, blood lactate level after exercise, and heart rate at the final minute were measured. The results were as follows: 1. There were significant differences in 300m and 400m swimming times between caffeine and placebo trials. 2. There was significant difference in heart rate measured at the final minute of swimming between caffeine and placebo trials. 3. There was significant difference in blood lactate level at 5 minutes postexercise between caffeine and placebo trials. The results of the study suggest that caffeine ingestion can enhance the performance during short term, intense exercise.

회전자에 정류회로를 가지는 유도전동기의 교류회로 모델에 의한 해석

조용철,좌종근,문경주 濟州大學校工科大學産業技術硏究所 1998 尖端技術硏究所論文集 Vol.9 No.2

In this paper, the characteristics of induction motor which has rotor rectifier circuit are analyzed using a new six elements ac model. The effects of resistance on dc circuit which are caused by current over lap angle and voltage drop of rectifier are considered in the proposed model for this analysis. The proposed model and Sen's five elements ac model which is not considered these effects are used to analyse. and the analyzed results are compared with the experimental results in order to verify the Proposed model. It is found that the results of the proposed method are good agreement with the experimental results.

남성화를 보이는 여성에서 발견된 난소의 Steroid Cell Tumor 1예

조인호,정대훈,박영미,서영진,손영실,정철회,강영미,정수전,김영남,이경복,성문수,김기태 인제대학교 2006 仁濟醫學 Vol.27 No.-

Steroid cell tumor is a rare ovarian sex cord-stromal tumor which accounts for 0.1% of all ovarian tumors. Until now, only 4 cases have been reported in domestic literatures. Steroid cell tumor often secrets testosterone and presents virilization in adult women or precocious puberty in children. Treatment is often performed by surgical removal, adjuvant chemotherapy and radiation, but completely accepted treatment was not existed. We experienced a case of steroid cell tumor, which was manifested by typical virilization in a 43-year old patient, who was previously performed hysterectomy and unilateral oophorectomy. So, we present with a brief review of the literatures.