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조경열,우미희,김난주 대구효성가톨릭대학교 응용과학연구소 1993 응용과학연구논문집 Vol.2 No.-
Rosa maximowicziana Regel(Rosaceae) is a deciduous, latifoliate shrub growing in most parts of Korea. The sprout of this plant has been used for food, and the fruit for treating thirst. Also, the root of this plant has been used fr rheumatism in a Korean folk medicine. From the roots of this plant, sterol and its flucoside, and t재 triterpenoid saponins were isolated and the structrues were elucidated by chemical and spectroscopic methods. So, these compounds were identified as β-sitosterol, β-sitosterool-3-O-β-D-glucopyranoside, 2α, 3β, 19α-trihydroxyurs-12-ene-28-oic acid 28-O-β-D-glucopyranosyl ester(kajiichigoside F1) and 2α, 3β, 19α-trihydroxyurs-12-ene-28-oic acid 28-O-β-D-glucopyranosyl ester(rosamultin), and were encounted in this plant for the first time.
Aromatic Toxicants에 의해 유도된 간기능 장해에 미치는 쑥의 영향
조경열,손경선,윤수홍,박은주 효성여자대학교 부설 한국환경위생연구소 1991 환경위생연구 Vol.1 No.1
간장해 물질인 phenylbutazone, aniline, benzo(a)pyrene을 이용하여 유도한 rats의 간독성발현에 미치는 쑥 추출액의 효과와 간장해 예방 효과를 관찰하여 다음과 같은 결과를 얻었다. 1. 성분 분석 결과 8종의 무기성분이 검출되었으떠 특히 potassium의 함량이 가장 높았고magnessium과 sodium의 함량이 높았다. 2. 총 14증의 지방산이 확인되었으며 그중 필수지방산인 linoleic acid와 linolenic acid의 함량이높았다. 3. 아피노산 분석 결과 총 16종이 검출되었으며 특히 aspartic acid, glutamic acid와 같은 산성아미노산의 함량이 높았다. 4. 쑥 추출액의 전처리는 phenylbutazone의 투여로 증가한 혈청과 조직중의 AST, ALT, ALP함량 증가를 현저히 회복신켰으나 혈청 LDH의 활성과 bilirubin 함량에는 효과를 나타내지않았다. 5. Aniline의 투여로 증가한 혈청과 간장중의 AST, ALT, LDH, ALP 활성을 쑥 추출액의 투여로크게 감소시킬 수 있었다. 그러나, bilirubin 함량에는 큰 변화가 없었다. 6. 쑥 추출액을 투여함으로씨 benzo(a)pyrene의 독성으로 증가한 혈청과 조직중의 AST, ALT,LDH, ALP 활성을 크게 감소시킬 수 있었으며 특히 LDH의 활성 회복 효과가 현저했다. In search for new drugs and methods of pharmacotherapy of liverdamage, we measured the chemical compositions of mugwort. And the mugwortextract was administrated to the experimental animal and investigated its bioche-mical effects in the serum and liver when aromatic hepatotoxicants - phenylbuta-zone, aniline and benzo(a)pyrene- was administrated. As the results are as follows : 1. 14 kinds of fatty acids,16 amino acids and 8 kinds of minerals were quantita-tively analyzed at mugwort. And major components of them were linoleic acid,aspartic acid, potassium and calcium. 2. The increase of serum and liver aminotransferase activity and bilirubin con-tent in hepatotoxicants treated group was markedly decreased by mugwortpretreatment.
조경열,우희미,정순옥 대한약학회 1995 약학회지 Vol.39 No.2
Four steroids have been isolated from the subterranean parts of Smilax nipponica Miquel (Liliaceae). The structures of these compounds were characterized on the basis of chemical and speectral data. They were $\beta$-sitosterol, $\beta$-sitosterol-3-O-$\beta$-D-glucopyranoside, neotigogenin-3-O-$\beta$-D-glucopyranoside and a new steroidal saponin designated as smilanippin A which was elucidated as neotigogenin-3-O-$\beta$-D-fucopyranosyl(1$\rightarrow$6)-$\beta$-D-glucopyranos ide.
청가시덩굴(Smilax sieboldii Miq.)의 잎 및 지하부의 성분과 항고지혈작용에 관한 연구
조경열,우미희,오인숙 대구효성가톨릭대학교 응용과학연구소 1991 응용과학연구논문집 Vol.1 No.-
Nutritional value of the leaf and antihyperlipidemic effect of the subterranean part of Smilax siebolidd Miq.(Liliaceae) were investigated in this experiment. 8 minerals, 17 amino acids and 5 fatty acids were quantitatively analyzed in the leaf. In comparison with other vegetables, the content of amino acids was about twice as much as those and a lot of essential amino acids were found. The content of fatty acids was similar with that of other vegetables. In addition, various trace elements such as Mg, Zn and Mn were contained. The chloroform extract of the subterranean part of this plant was effective to decrease total cholesterol and triglyceride level and decrease HDL-cholesterol level in plasma of mouse.
趙庚烈,禹美熙,鄭順玉 대구효성가톨릭대학교 1991 연구논문집 Vol.43 No.1
Schrophularia burgeriana Miquel (Scrophulariaceae) is a peennial herb growing in all parts of Korea. It has been used as Korean folk medicine in treation guttural diseases acting as an antiphlogistics, antipyetics and analgesicss. In this paper, the structural elucidation of chemical componets was studied. From the roots of this plant, a phthalate and an iridoid glycoside were isolated and identified as bis (2-ethy1 hexy1) phthalate was orginaged from solvents. Aucubin was first isolated from Scrophularia buergeriana Miquel.
趙庚烈,禹美熙 대구효성 가톨릭 대학교 1988 연구논문집 Vol.36 No.1
Extraction-spectrophotometric determination of mercury(Ⅱ) was studied by associated complex formation using antipyrine, antipyretics and eosin, halogenated xanthenes. K₂SO₄was added for the promotion of complex formation and it's optimal concentration was 0.3M. Optiaml conditions for the quantitative analysis of trace of mercury(Ⅱ) were investigated. Molar ratio of Hg(Ⅱ)-antipyrine-eosin complex was presumed as 1:4:2. Linear calibration curve was obtained in the range of 6~28㎍/㎖ at 485nm. Mercury(Ⅱ) determination of this method was interfered in the presence of metals such as ??, ??,, ??, ?? and ??, halides an dthiocyanate, but the interferences of metals except ?? were masked with 0.01M-sod. tartrate.
Acorn中에 含有된 Tannin과 Starch 開發에 關한 硏究
權泰勳,趙庚烈 대구효성가톨릭대학교 1976 연구논문집 Vol.18 No.1
The acorn which grew in Korea contained about 10% tannin and 70% starch.To separats tannin and starch,the following physical properties were used:tanin is soluble in ethanol,ether and water,starch is insolube in alkali,brine and water.In this is soluble in ethanol,ether and water,starch is insoluble in alkali,brine and water.In this work,water was used for solvent.Water soluble tannin was developed by paper chromatography.The result of development showed that a kind of acorn contained 6 or 7 kinds of tannic components.The contents of tannin were 6~14%. Qater insoluble precipitation was dried and powered,and then was refined in ethanol.The refined precipitation was assured as polarly substances and saccharine substances.The saccharine substances was determined by polarimetry of C.J. Linter. The contents of polarly substances were 60~70%.
收斂性 止瀉劑의 生藥資源으로서 Tannin含量에 對하여
趙庚烈 대구효성가톨릭대학교 1973 연구논문집 Vol.12 No.1
I collected nine lind of plants around us in order to analyze catechol type tannin which is contained in plants. The analysis was made by Lowenthal's volumetric analysis method and paper chromatography method. At this experiment, the rate of developing solvent of paper chromatography was n-butanol: acetic acid: water=5:2:6(vol.%), and developing, Quercus aliena Blume, Quercus aliena Blume var. acute-serrata Maximowicz ex Wenzig and Quercus aliena Blume var. pellucida Blume, much tannin.