HVPE 법을 활용한 GaN 성장 시 질화처리에 관한 연구

이승훈,이주형,이희애,오누리,이성철,강효상,이성국,양재득,박재화,Lee, Seung Hoon,Lee, Joo Hyung,Lee, Hee Ae,Oh, Nuri,Yi, Sung Chul,Kang, Hyo Sang,Lee, Seong Kuk,Yang, Jae Duk,Park, Jae Hwa 한국결정성장학회 2019 한국결정성장학회지 Vol.29 No.4

HVPE is one of the GaN single crystal manufacturing methods which has been commercially widely used due to its high growth rate. HVPE method consists of a number of processes, in particular the nitridation of the substrate prior to GaN growth has a significant effect on the crystalline quality of the manufactured GaN single crystal. In this study, we investigated the effect of nitridation for crystalline quality of GaN when it was grown on the sapphire substrate. The whole growth conditions except for the nitridation process were the same, and the gas flow rate supplied to the sapphire substrate was variously changed during the nitridation. Here, we examined the effect of nitridation via the surface characterization of GaN single crystal grown by HVPE. HVPE는 GaN 단결정의 제조 방법 중 하나로 빠른 성장 속도가 장점인 상업적으로 널리 사용되는 성장 방법이다. HVPE 법에 의한 GaN 단결정 성장은 여러 공정으로 이루어지며, 특히 GaN 성장 전 기판의 질화 처리는 성장되는 GaN 단결정 품질에 상당한 영향을 미친다. 본 연구에서는 사파이어 기판 위에 GaN 단결정 성장 시 기판의 질화처리가 성장되는 GaN 단결정 품질에 미치는 영향을 알아보고자 하였다. 질화 처리를 제외한 다른 성장 조건은 동일하게 하였고 질화처리 시 기판에 공급되는 가스 유량을 다양하게 변화시킨 후 GaN 박막을 성장시키고, 성장된 GaN의 표면 특성평가를 통하여, HVPE 법에서의 질화처리 효과를 고찰하여 보고자 하였다.

플라즈마 처리에 의한 폴리비닐리덴플로라이드 나노섬유의 젖음성

이승훈,장선호,소윤미,이헌수,양철민,윤중현,김찬,Lee, Seung-Hoon,Jang, Seon-Ho,So, Yun-Mi,Lee, Hun-Su,Yang, Cheol-Min,Yun, Jung-hyun,Kim, Chan 한국섬유공학회 2018 한국섬유공학회지 Vol.55 No.1

Poly(vinylidene fluoride) (PVDF) is a critical polymeric material used in the mass production and application of electrospun nanofibers, and is popular due to its excellent properties. However, electrospun PVDF nanofibers are very hydrophobic and possess low surface energies, limiting their broad application. In this work, we investigated practical methods for the hydrophobic surface modification of PVDF nanofibers using four techniques: radio-frequency (RF) and PIN-type atmospheric plasmas, planar inductively coupled plasma (ICP), and planar capacitively coupled plasma (CCP). The use of RF atmospheric plasma was ineffective under the experimental conditions used, while the PIN-type atmospheric plasma efficiently modified PVDF nanofiber surfaces locally. The application of planar CCP to PVDF nanofibers was more effective than planar ICP for the same experimental conditions. In particular, the water contact angles of samples treated with planar CCP for 600 s and 900 s were $25^{\circ}$ and $10^{\circ}$ respectively, and wettability improved. Analysis with FT-IR, XPS, and FE-SEM showed that the surface CF and CH hydrophobic groups were destroyed without damaging the PVDF nanofibers, and hydrophilic species such as C=O, OH, and COOH were formed. As a consequence, quantitative analysis of nanofiber chemical composition is necessary when treated by plasmas, providing insight into the correlation of specific property changes with processing conditions, and indicating precise research results and application examples.

중저온 SOFC용 Ba_0.5Sr_0.5Co_0.8Fe_0.2O_3−δ (BSCF)/Ce_0.9Gd_0.1O_2−δ (GDC) 및 La_0.6Ba_0.4Co_0.2Fe_0.8O<sub>3−δ

이승훈,윤종설,차영철,이준,황해진,문지웅,Lee, Seung-Hun,Yoon, Song-Seol,Cha, Young-Chul,Lee, Jun,Hwang, Hae-Jin,Moon, Ji-Woong 한국세라믹학회 2007 한국세라믹학회지 Vol.44 No.12

The potential candidates for IT-SOFCs cathode materials, $Ba_{0.5}Sr_{0.5}Co_{0.8}Fe_{0.2}O_{3-{\delta}}$ (BSCF) and $La_{0.6}Ba_{0.4}Co_{0.2}Fe_{0.8}O_{3-{\delta}}$ (LBCF) powders, were synthesized by a EDTA-citrate combined method from $Sr(NO_3)_2$, $Ba(NO_3)_2$, $La(NO_3)_3{\cdot}6H_2O$, $Co(NO_3)_2{\cdot}6H_2O$, $Fe(NO_3)_3{\cdot}9H_2O$, citric acid and $EDTA-NH_3$. The cathode performance of symmetrical electrochemical cells consisting of BSCF-GDC or LBCF-GDC composite electrodes and a GDC electrolyte was investigated using by AC impedance spectroscopy at the temperature range of 500 to $700^{\circ}C$. It was found that a single phase perovskite could be successfully synthesized when the precursor is heated at $850^{\circ}C$ for 2 h. Due to thermal expansion mismatch between BSCF and GDC, the composite cathodes with lower GDC content than 45 wt% were peeled off from the GDC electrolyte and their electrode polarization resistance was estimated to be high. The thermal expansion coefficient of BSCF-GDC composites was decreased with increasing the GDC content and the electrode peeling off did not occur in BSCF-45 and 55 wt% GDC composites. BSCF-45 wt% GDC composite electrode showed the lowest area specific resistances (ASR) of 0.15 and $0.04{\Omega}{\cdot}cm^2$ at 600 and $700^{\circ}C$, respectively. On the other hand, LBCF-GDC composite cathodes showed higher ASR than the BSCF-45 and 55 wt% GDC and their cathode performance were decreased with the GDC content.

BPMN기반의 모델 단축을 이용한 서비스 시스템의 테스트 케이스 생성 기법

이승훈,강동수,송치양,백두권,Lee, Seung-Hoon,Kang, Dong-Su,Song, Chee-Yang,Baik, Doo-Kwon 한국정보처리학회 2009 정보처리학회논문지D Vol.16 No.4

시스템 개발에서 초기 테스트는 오류수정 비용을 현저하게 낮출 수 있으며 이는 SOA기반 서비스 시스템에서도 여전히 중요한 요소이다. 그러나 서비스 시스템을 위한 기존 테스트 케이스 생성 기법들은 XML 기반 언어를 사용하여 웹서비스에 한정적이라는 한계점을 가진다. 이를 극복하기 위해서 본 논문에서는 BPMN에 따라 작성된 비즈니스 프로세스 기반으로 서비스 시스템의 테스트 케이스 생성 기법을 제시한다. 테스트 노력을 최소화 하기 위해 기존 BPM을 워크플로우의 기본 요소로만 단순화 시킨 S-BPM을 사용한다. 테스트 케이스 생성 과정은 목표서비스 시스템에 대해 S-BPM을 생성하고, 이를 방향성 그래프로 변환 후, 시나리오 검색 알고리즘을 적용하여 서비스 시나리오를 생성하고, 메시지의 이동 정보를 추출함으로써 이루어진다. 본 기법을 적용하면 웹서비스에 한정적이지 않으면서도 범용 서비스에 적용이 가능한 효율성 높은 테스트 케이스를 얻을 수 있으며, 이 결과물은 SOA의 비즈니스 관점 지향 특징을 반영한 테스트 케이스로 볼 수 있다. The early test can greatly reduce the cost of error correction for system development. It is still important in SOA based service system. However, the existing methods of test case generation for SOA have limitations which are restricted to only web service using XML. Therefore, this paper proposes a method of test case generation using BPMN-based model reduction for service system. For minimizing test effort, an existing BPM is transformed into S-BPM which is composed of basic elements of workflow. The process of test case generation starts with making S-BPM concerning the target service system, and transforms the target service system into directed graph. And then, we generate several service scenarios applying scenario searching algorithm and extract message moving information. Applying this method, we can obtain effective test cases which are even unlimited to web service. This result is the generation of test case which is reflected in the business-driven property of SOA.

고주파 온열치료시 케모포트의 열적 변화 연구

이승훈,이선영,김양수,양명식,차석용,Lee, seung hoon,Lee, sun young,Gim, yang soo,Kwak, Keun tak,Yang, myung sik,Cha, seok yong 대한방사선치료학회 2015 대한방사선치료학회지 Vol.27 No.2

목 적 : 고주파 온열치료 시 약물투여 및 혈액채취에 사용되는 케모포트로 인한 열적 변화를 알아보고자 한다. 대상 및 방법 : 전극 크기 20 cm인 고주파 온열치료기(EHY-2000, Oncotherm Kft, Hungary)를 이용하여 현재 본원에서 사용 중인 케모포트 중 재질이 플라스틱인 소재, 티타늄을 둘러싼 에폭시 소재와 티타늄 소재 케모포트를 자체 제작한 직경 20 cm, 높이 20 cm 원통형 한천(Agar)팬텀에 삽입하여 온도를 측정하였다. 온도측정기(TM-100, Oncotherm Kft, Hungary) 그리고 Sim4Life(Ver2.0, ZMT, Zurich, Switzerland) 프로그램을 사용하여 실제 측정된 온도변화와 비교 분석하였다. 측정위치는 전극 중심축 및 중심축 측면 1.5 cm지점에 각각 0 cm(표면), 0.5 cm, 1.8 cm, 2.8 cm 깊이별로 하였다. 측정조건은 온도 $24.5{\sim}25.5^{\circ}C$, 습도 30 ~ 32%, 출력 전력 100 W로 5분 간격으로 총 60분을 측정 하였다. 결 과 : 케모포트 미사용, 플라스틱, 에폭시 그리고 티타늄 케모포트를 사용한 경우의 최고온도는 전극 중심축 2.8 cm 깊이에서 측정값 $39.51^{\circ}C$, $39.11^{\circ}C$, $38.81^{\circ}C$, $40.64^{\circ}C$와 모의실험값 $42.20^{\circ}C$, $41.50^{\circ}C$, $40.70^{\circ}C$, $42.50^{\circ}C$이며, 전극 중심축 1.5 cm 측면 2.8 cm 깊이에서 측정값 $39.51^{\circ}C$, $39.32^{\circ}C$, $39.20^{\circ}C$, $39.46^{\circ}C$와 모의실험값 $42.00^{\circ}C$, $41.80^{\circ}C$, $41.20^{\circ}C$, $42.30^{\circ}C$이다. 고안 및 결론 : 고주파 전자기장에 의한 케모포트 주위의 열적 변화량은 부도체 물질인 플라스틱과 에폭시 소재에서 미사용의 경우보다 낮게 나타났으며, 도체 물질인 티타늄 케모포트에서는 약간의 차이를 보였다. 이는 케모포트내 금속 함유량 및 기하학적 구조에 의한 것과 이용 장비의 낮은 고주파 대역를 사용함에 있는 것으로 여겨진다. 즉 본 연구에 사용된 케모포트는 열 변화가 미미하여 장해를 고려하지 않아도 된다고 사료된다. Purpose : This study evaluate the thermal changes caused by use of the chemoport for drug administration and blood sampling during radiofrequency hyperthermia. Materials and Methods : 20cm size of the electrode radio frequency hyperthermia (EHY-2000, Oncotherm KFT, Hungary) was used. The materials of the chemoport in our hospital from currently being used therapy are plastics, metal-containing epoxy and titanium that were made of the diameter 20 cm, height 20 cm insertion of the self-made cylindrical Agar phantom to measure the temperature. Thermoscope(TM-100, Oncotherm Kft, Hungary) and Sim4Life (Ver2.0, Zurich, Switzerland) was compared to the actual measured temperature. Each of the electrode measurement position is the central axis and the central axis side 1.5 cm, 0 cm(surface), 0.5 cm, 1.8 cm, 2.8 cm in depth was respectively measured. The measured temperature is $24.5{\sim}25.5^{\circ}C$, humidity is 30% ~ 32%. In five-minute intervals to measure the output power of 100W, 60 min. Results : In the electrode central axis 2.8 cm depth, the maximum temperature of the case with the unused of the chemoport, plastic, epoxy and titanium were respectively $39.51^{\circ}C$, $39.11^{\circ}C$, $38.81^{\circ}C$, $40.64^{\circ}C$, simulated experimental data were $42.20^{\circ}C$, $41.50^{\circ}C$, $40.70^{\circ}C$, $42.50^{\circ}C$. And in the central axis electrode side 1.5 cm depth 2.8 cm, mesured data were $39.37^{\circ}C$, $39.32^{\circ}C$, $39.20^{\circ}C$, $39.46^{\circ}C$, the simulated experimental data were $42.00^{\circ}C$, $41.80^{\circ}C$, $41.20^{\circ}C$, $42.30^{\circ}C$. Conclusion : The thermal variations were caused by radiofrequency electromagnetic field surrounding the chemoport showed lower than in the case of unused in non-conductive plastic material and epoxy material, the titanum chemoport that made of conductor materials showed a slight differences. This is due to the metal contents in the chemoport and the geometry of the chemoport. And because it uses a low radio frequency bandwidth of the used equipment. That is, although use of the chemoport in this study do not significantly affect the surrounding tissue. That is, because the thermal change is insignificant, it is suggested that the hazard of the chemoport used in this study doesn't need to be considered.

에폭시/구상실리카 콤포지트의 전기적 절연파괴 및 인장 강도 특성 연구

이승훈,Lee, Seung-Hun 한국전기전자재료학회 2013 전기전자재료학회논문지 Vol.26 No.10

In order to develop a high voltage insulation material, spherical silicas with two average particle sizes of 5 ${\mu}m$ and 20 ${\mu}m$ were mixed in different mixing ratios (1:0, 0.7:0.3, 0.5:0.5, 0.3:0.7, 0:1) and their total filling content was fixed at 65 wt%. In order to observe the dispersion of the spherical silicas and the interfacial morphology between silica and epoxy matrix, field emission scanning electron microscope (FE-SEM) was used. The electrical insulation breakdown strength was estimated in sphere-plate electrodes with different insulation thicknesses of 1, 2, and 3 mm. Electrical insulation breakdown strength decreased with increasing mixing ratio of 5/20 ${\mu}m$ and the thickness dependence of the breakdown strength was also observed. The tensile strength of the neat epoxy was 82.8 MPa as average value and its increased with decreasing particles size and that of epoxy/silica (2 ${\mu}m$) was 107 MPa, which was 130.8% higher value.

화재원인조사실무 - 화재조사 지표로서 유리파괴 분석의 법공학적 가치

이승훈,Lee, Seung-Hun 한국화재보험협회 2014 防災와 保險 Vol. No.

건설사업 설계초기단계 VE 적용방안

이승훈,구교진,현창택,Lee Seung-Hoon,Koo Kyo-Jin,Hyun Chang-Taek 한국건설관리학회 2005 건설관리 : 한국건설관리학회 학회지 Vol.6 No.3

본 연구는 설계초기단계에 적합한 VE 적용방안을 제안하고자 하였다. VE방법론은 설계단계 초기에 적용할 경우 더욱 효과적이므로 본 연구는 설계 프로세스 초기단계의 설계YE에 초점을 맞추고 있다. 관련 연구문헌의 고찰과 실무경험을 바탕으로 국내 건설산업에서 설계VE의 문제점을 도출하였다. 이러한 문제점을 해결하기 위하여 본 연구는 (1)설계단계별 VE실시시기를 구분하고, (2)건설산업에 적합한 VE대상선정 방법을 제안하며, (3)기능분석 프로세스를 보다 합리적이고 실용적으로 개선함으로써 (4)전체 설계VE 수행절차를 효율적으로 개선하고자 하였다. The purpose of this study is to present proper VE application methods to euly design phases. Since VE methodology is more effective on early stage of design phase, the study focused on application of VE methodology in early stage of design process. With the examination of past studies, obstacles of VE application in domestic construction industry are defined. To solve these problems, this paper presents (1) subdivision of VE execution time, (2) an appropriate VE targeting method for construction industry, (3) a resonable and practical function analysis process, and (4) modified design-VE job plan.

TadGAN 기반 시계열 이상 탐지를 활용한 전처리 프로세스 연구

이승훈,김용수,Lee, Seung Hoon,Kim, Yong Soo 한국품질경영학회 2022 품질경영학회지 Vol.50 No.3

Purpose: The purpose of this study was to increase prediction accuracy for an anomaly interval identified using an artificial intelligence-based time series anomaly detection technique by establishing a pre-processing process. Methods: Significant variables were extracted by applying feature selection techniques, and anomalies were derived using the TadGAN time series anomaly detection algorithm. After applying machine learning and deep learning methodologies using normal section data (excluding anomaly sections), the explanatory power of the anomaly sections was demonstrated through performance comparison. Results: The results of the machine learning methodology, the performance was the best when SHAP and TadGAN were applied, and the results in the deep learning, the performance was excellent when Chi-square Test and TadGAN were applied. Comparing each performance with the papers applied with a Conventional methodology using the same data, it can be seen that the performance of the MLR was significantly improved to 15%, Random Forest to 24%, XGBoost to 30%, Lasso Regression to 73%, LSTM to 17% and GRU to 19%. Conclusion: Based on the proposed process, when detecting unsupervised learning anomalies of data that are not actually labeled in various fields such as cyber security, financial sector, behavior pattern field, SNS. It is expected to prove the accuracy and explanation of the anomaly detection section and improve the performance of the model.

Digital Satellite Radio 방송의 채널 정보 Searching 처리 Method에 관한 연구

이승훈,나상신,김영길,Lee, Seung-Hun,Na, Sang-Sin,Kim, Young-Kil 한국정보통신학회 2011 한국정보통신학회논문지 Vol.15 No.4

본 논문은 디지털 위성 라디오 방송의 채널 정보 업데이트 방법에 관한 것으로, 예를 들어 디지털 위성 라디오의 방송 수신 기능이 구비된 홈시어터, MP3 플레이어, 이동 전화기, 카오디오 등 과 같은 다양한 유형의 디지털 기기에서 새로운 디지털 위성 라디오(이하 XM으로 표기) 방송 채널 정보를 수신하게 되면, 현재 수신 중인 XM 라디오 방송 채널과 인접된 N 개의 전/후 방송 채널만을 지그재그(Zigzag) 방식으로 랜덤하게 선별 한 후, 이전의 XM 라디오 방송 채널 정보를 새로 수신된 XM 라디오 방송 채널 정보로 업데이트 함 으로써, 사용자가 거의 선국하지 않는 XM 라디오 방송 채널을 일괄적으로 모두 업데이트 하게 되는 것을 미연에 예방 할 수 있게 되므로, 실시간으로 자주 변경되는 XM 라디오 방송 채널 정보를 보다 효율적으로 신속하게 업데이트 시킬 수 있게 되는 매우 유용한 방법을 제시한다. In this paper, we present a very useful method for updating digital satellite radio broadcast channel information. When a devices equipped with function to receive Digital Satellite Radio such as Home Theater, MP3 player, mobile phones, car audio system and various other types of Digital Devices, receives new Digital satellite radio (will be mentioned as XM radio onwards) broadcast channel information, only the current received XM radio broadcast channel and N number of pre/post nearby broadcast channels are scanned randomly in zigzag manner. Then the previous XM radio broadcast channel information updated with the newly received XM radio broadcast channel information. Since this method can prevent batch update for all XM radio channel, including some channels which less likely did not select by user, update process for real time frequently changed XM radio broadcast channel information can be performed efficiently with minimal or without delay.