정향의 화학 성분

박만기 강원대학교 종합약학연구소 1998 약학연구 Vol.10 No.-

GC/FPD를 利用한 ${\beta}$-락탐系 抗生物質의 分析(II)

박만기,조영현,양정선,박정일,Park, Man-Ki,Cho, Yung-Hyun,Yang, Jeong-Seon,Park, Jeong-Hil 대한약학회 1984 약학회지 Vol.28 No.4

For gas chromatographic determination with the sulfur-specific flame photometric detector, nine ${\beta}$-lactam antibiotics without ${\alpha}$-amino group were esterified with borontrifluoride-methanol complex and then N-benzoylated with benzoyl chloride. The gas chromatographic separation of these products was successfully carried out on various silicon polymers (OV-1, OV-101, OV-17, OV-225, and QF-1) coated on the acid washed, silanized diatomite. The structure of the esterified and N-benzoylated product was confirmed by mass spectromer.

초록집 ( 1993 . 4 . 15 ) : 제 1 분과 ( 합성 , 천연물 ) ; 조구등 ( Uncaria Hooks ) 의 성분에 관한 연구

박만기,박정일,김종문,한방희 한국응용약물학회 1993 학술대회 Vol.1993 No.1

아미노산 분석기에 의한 제제중 Taurine의 분리 정량에 관한 연구

박만기,한달수 대한약학회 1984 약학회지 Vol.28 No.1

High performance amino acid analyzing method has been developed for the routine analysis of taurine in preparations. Ion-exchange resin #2619 Hitachi Custom Ion-Exchange Resin, $2.6(I.D.){\times}150$(length)mm was used as column, buffer I, pH 3.3 as mobile phase. The retention time of taurine was 7 minutes. Calibration curve by peak height for standard taurine was linear from 2.5ppm to 25ppm. The reproducibility showed relative standard deviation $\pm$1.9% when analyzed 10 times for standard solution. The samples could be continuously analyzed without regenerating the resin between samples. Five samples were applied to column every 12 min. and then the resin was regenerated for 30 min. during one analyzing cycle time, 90 min. The automatic amino acid analyzer has made it possible to assay multiple samples in a relatively short period of time using the analytical magnetic program card. The high sensitivity and specificity of the analytical column of the automatic amino acid analyzer permits the routine analysis of taurine in preparations.

아미노산 Phenylthiohydantoin 유도체를 키랄 고정상으로 한 GC에 의한 아미노산 광학 이성질체의 상호분리

박만기,양정선,고창범,이미영,Park, Man-Ki,Yang, Jeong-Seen,Ko, Chang-Bum,Lee, Mi-Yung 대한약학회 1988 약학회지 Vol.32 No.3

The resolution of five amino acids derivatives by gas chromatography on phenylthiohydantoin derivatives as chiral stastionary phase was investigated. (S)-5-isopropyl, isobutyl, (sec)-butyl and benzoyl derivatives of $N^3-phenyl-2-thiohydantoin$ were synthesized from L-valine, L-leucine, L-isoleucine and L-phenylalanine, respectively. The phases were employed at several column temperatures ($140^{\circ}C{\sim}210^{\circ}C$). The separation factors were compared with each stationary phase with varying R groups. The possible mechanism of chiral recognition was investigated by NMR technique.

FID를 이용한 수중의 TOC 분석법

박만기,한대석,임병연 대한약학회 1978 약학회지 Vol.22 No.3

Total organic carbon(TOC) can be determined by means of combustion and flame ionization detector. The principle of string method is that a sample acidified to pH2 and transferred into combustion tube by string is oxidized with air. Another combustion tube method is that organic compounds are oxidized in the combustion tube charged with CuO and cobalt asbestos after the acidified sample is injected directly by microsyringe. Carbon dioxide evolved was reduced under specially treated nickel catalyst and hydrogen, the methane produced was detected by flame ionization detector. Linear relationship was found between concentration and the peak height by the string method. The peak area in the case of combustion tube method is in the range of 1-200ppm. The coefficient of variation by string method was 2.3% and that by combustion tube method was 1.8%. The lower detectable limit was about 10mol. Advantages of the latter are simplicity, sensitivity and reproducibility. TOC in contineous stream can also be determined automatically by means of the string method.

Gas-chromatography에 의한 핵산염기성분의 분석

박만기,백남호 대한약학회 1974 약학회지 Vol.18 No.2

콜라주 집단미술치료를 활용한 렉시오 디비나가 중년 여성의 분노와 영적 안녕감에 미치는 영향

박만기 한국미술치료학회 2017 美術治療硏究 Vol.24 No.5

The purpose of this study was to investigate the effects of group art therapy on the anger and spiritualwell-being of middle - aged women. The study participants were recruited persons wishing to participate bynotifying the “group art therapy that utilizes the Lectio Divina” for the housewife of middle-aged womenbetween 40 years and 65 years old who are a member of the ‘Z’ local Catholic church. Sixteen participantswere designated as an experimental group, the other 16 as a comparative group, and the remaining 16 as acontrol group. In the final analysis, data for 33 participants were analyzed. This included 11 subjects inthe experimental group, 11 in the comparative group, and 11 in the control group 5 subjects were excludeddue to low attendance(in experimental and comparative groups) and due to too high or low scores (incontrol group). The Spiritual Well-being Scale and Anger Scale were used as are search tools. Data wereanalyzed using repeated measures ANOVA with groups (experimental and control) and test points (before,after, and follow-up) as variables. The results are as follows. First, group art therapy that utilizes the LectioDivina was found to be effective in the anger and spiritual well-being of middle-aged women. Second, theeffectiveness of the Lecio Divina program using art therapy was more effective than the Lectio Divinaprogram alone. 본 연구는 콜라주 집단미술치료를 활용한 랙시오 디비나가 중년여성의 분노와 영적안녕감에 미치는 효과를알아보기 위한 것이다. 연구 대상은 Z지역 가톨릭교회의 교인인 40세에서 65세 사이의 중년기 기혼 여성을 대상으로 하였다. 가톨릭교회에 프로그램의 내용과 실시시간을 공지하고 참가희망자를 모집하여 연구에 동의한사람을 대상으로 실험집단(렉시오 디비나와 미술치료를 함께 하는 집단), 비교집단(렉시오 디비나만 실시), 통제집단(아무런 중재를 하지 않음)에 각각 16명씩 배치하여 프로그램을 진행했으나 본 연구의 최종 분석 자료는출석율이 저조하거나(실험, 비교집단에서) 점수가 지나치게 낮거나 높은 사람(통제집단에서)을 각각 5명씩 제외하여 실험 11명, 비교 11명, 통제 11명, 총 33명의 자료를 분석하였다. 연구도구는 분노 척도, 영적안녕감 척도를 사용하였다. 프로그램의 효과를 검증하기 위해 집단(실험집단, 비교집단, 통제집단)과 검사 시기(사전, 사후,추후검사)에 따른 반복측정 이원변량분석을 실시하였고, 결과는 다음과 같다. 첫째, 콜라주 집단미술치료를 활용한 렉시오 디비나 프로그램은 중년 여성의 영적안녕감과 분노에 영향을 미치는 것으로 나타났다. 둘째, 콜라주 집단미술치료를 활용한 렉시오 디비나 프로그램은 렉시오 디비나 프로그램만을 적용한 것 보다 효과가 지속되었다.

게르마늄의 분석법

박만기,박정일 한국약제학회 1995 유기게르마늄 Vol.0 No.-

세월호 침몰사고 관련 애니메이션 캠페인 영상 사례로 본 인포그래픽-애니메이션의 효과와 활용방안

박만기 한국만화애니메이션학회 2019 만화애니메이션연구 Vol.- No.55

This study aims to establish an independent area of animation studies by combining animation practice and theory through collaborative research with other academic fields. The animation campaign video (Two Contrasting views of the South Korea Ferry Accident, 2015) produced within this context is designated as a practical case or case study to systematically investigate how it has positively affected the audience. For this, approximately 40 interviewees are organized to see if there has been a change in existing thinking amongst interviewees before and after watching the video and identify whether or not they would cleary understand the solid message of campaign video intended by the producer. In order to gain more concrete feedback, the in-depth interview will be conducted with 14 university students who were high school students at the time of the sinking of the ferry Sewol. In this case, the literature research is carried out in advance to systematically organize and analyze the answers and responses of interview panels who watched the video by subdividing the questions into cognitive, emotional, and psychological elements. Based on these results, this study explore the effects of animation campaigns and further find out the meaning and characteristics of infographic-animation. Through this approach, it will eventually investigate a new convergence approach, in which the fields of animation studies and humanities/social sciences work together. 본 연구는 타 학문 분야와의 협동연구를 통해 애니메이션 실습과 이론을 함께 병행함으로써, 애니메이션 스터디의 독립적 영역을 구축하고자 기획되었다. 이러한 맥락 안에서 제작된 애니메이션 캠페인 영상(두 가지 관점에서 바라본 세월호 침몰 사고, 2015)을 실습사례 또는 사례 연구로 지정하여, 과연 일반 시청자들에게 어떠한 반응과 영향을 끼쳤는지를 체계적으로 조사한다. 이를 위해 약 40명의 인터뷰 패널을 구성하여, 해당 캠페인 영상을 시청 전과 시청 후로 나누어 제작자의 의도대로 이해하고 있는지, 또한 어떠한 생각의 변화가 생겼는지를 알아본다. 그러나 보다 구체적인 피드백을 얻기 위해서 반 구조화 인터뷰 방식으로 세월호 침몰 사고 당시 고등학생이었던 14명의 대학생들과 심층적으로 진행한다. 이때, 문헌연구를 시작으로, 인지적, 감정적, 심리적 특성을 살펴보고 이를 인뎁스 인터뷰에 들어갈 질문지에 반영하여 영상을 시청한 인터뷰 패널들의 반응을 체계적으로 정리, 분석한다. 이렇게 도출된 답변 결과로 토대로 본 연구는 애니메이션 캠페인 영상의 효과와 활용방안에 대해서 알아보고 나아가 인포그래픽 애니메이션의 의미와 그 특징에 대해서 고찰한다. 이를 통해 향후 애니메이션 디자인 분야와 인문/사회과학 분야가 함께 협업하는 새로운 융합적 접근방식(Interdisciplinary Approach)의 가능성을 탐색한다.