나프틸기를 포함하는 퓨록산 유도체의 합성

黃匡鎭,南賢祐 홍익대학교 산업기술연구소 2002 産業技術 Vol.12 No.-

Furoxan derivatives containing naphthyl group was designed and synthesised as pohtochemical nitric oxide precussor. Naphthyl furoxan 4 was prepared by the [2+3] cycloaddition of the nitrile oxide generated in situ from the iminoyl chloride 3. The preparation of iminoyl chloride 3 was proceeded from naphthyl aldehyde 1 by the reaction with N-chlorosuccinimide following oxime formation. Naphthyl furoxan 4 was irradiated on 300 nm in CH2Cl2 to give alkyne 5 confirming NO generation.

RS485 직렬 통신 인터페이스를 이용한 BLDC 서보 전동기의 안전운전 영역에서의 운전에 관한 연구

우광준,김장기,황규범 단국대학교 1999 論文集 Vol.34 No.-

The servo motor systems is widely applied to the position and speed control system in modern process automation. In this paper, we design the H/W interface including RS232/485 converter and the control S/W interface including RS485 communication protocol for the real time operation of BLDC servo motor using half duplex asynchronous serial communication interface(ASCI). We confirm the servo operation for servo motor system in safety operation region by monitoring the servo status from the reply data of communication protocol and the possibility of real time operation in servo motor system using DIO method as well as ASCI method by the experimental results of proposed scheme.

치은연하 파절로 치조골 소실을 동반한 상악측절치에서 orthodontic extrusive remodeling후 임플란트 식립을 통한 심미수복 : 증례보고

황수연,손원준,한영철,배광식,백승호,이우철,금기연 大韓齒科保存學會 2008 Restorative Dentistry & Endodontics Vol.33 No.1

심미적으로 중요한 전치부에서 단일 치아 임플란트를 이용한 보철수복은 임상의에게 새로운 도전과제 중의 하나가 되었다. 그러나 전치부에서 single-unit implant는 식립할 부위의 치조골 상태가 양호해야 하는데 치은연하 파절로 인해 치아 주위에 골 손실이 있는 경우 immediate implant는 심미적으로 문제를 야기할 수 있다. 따라서 본 증례는 "orthodontic extrusive remodeling"을 통해 파절치와 주위 조직을 교정적으로 정출시켜 임플란트 식립을 위한 연조직과 경조직을 증대시킨 후 임플란트 식립을 통해 상악측절치에서 성공적인 심미수복을 이룬 증례에 관한 것이다. The treatment of esthetic areas with single-tooth implants represents a new challenge for the clinician. In 1993, a modification of the forced eruption technique, called "orthodontic extrusive remodelling" was proposed as a way to augment both soft- and hard-tissue profiles at potential implant sites. This case report describes augmentation of the coronal soft and hard tissues around a fractured maxillary lateral incisor associated with alveolar bone loss, which was achieved by forced orthodontic extrusion before implant placement. Through these procedures we could reconstruct esthetics and function in a hopeless tooth diagnosed with subgingival root fracture by trauma.

니트로크라이센 유도체의 합성에 관한 연구

黃匡鎭,김진국,남현우 홍익대학교 산업기술연구소 2001 産業技術 Vol.11 No.-

In an attempt to provide a useful light-emitting material in the organic electroluminescence diode, nitrochrysene 5 was prepared by the nitration of the tetrahydrochrysene 4 using dinitrogen tetraoxide as a key step. The chrysene 4 was obtained from the methyl cinnamate in 3 steps. The mono-nitration was confirmed by the IR, ^1H-NMR and ^13C-NMR spectra of chrysene 5. The results suggest that the synthetic methods for the nitrochrysene 5 is applicable to the synthesis of various chrysene derivatives containing donor-acceptor groups at 2, 8-positions.

구강 악성 흑색종에서 PCNA 발현에 관한 면역조직화학적 연구

황경균,남윤우,이재일,이종호,심광섭,김명진 大韓顎顔面成形再建外科學會 2002 Maxillofacial Plastic Reconstructive Surgery Vol.24 No.6

Malignant melanoma arising from the mucosa of head and neck region was rare and showed poor prognosis. Some of malignant melanoma were transformed from benign melanotic lesion. Malignant melanoma had high cellular proliferation and rapid growth. The percentage of PCNA-positive cell (labeling index) is high in many malignant tumor. So we compared the pattern of PCNA expression in the melanotic lesion. We performed the immunohistochemical study in malignant melanoma(19 cases), benign melanotic macule(24 cases) and normal mucosa(20 cases) were diagnosed in Seoul National University Dental Hospital between 1980 and 2000. Positive PCNA staining was found mainly in malignant melanoma. The mean PCNA expression in malignant melanoma, melanotic macule, normal tissue were 29.2%, 1.4%, 0%, respectively. Significant differences in PCNA expression were noted between malignant melanoma and melanotic macule(p<0.01), normal mucosa(p<0.01). These result suggested that the PCNA expression seems to be used as a diagnostic indicator for malignancy in malignant melanoma and melanotic lesion.

낙동강 수계의 인, 질소 및 Chl.a 농도 분포 : The distributions of phosphorus, nitrogen, and chlorophyll a concentration in the Nakdong River

허우명,김범철,황길순,최광순,박원규 江原大學校 附設 環境硏究所 1996 環境硏究 Vol.13 No.-

The longitudinal variations of water quality along the mainstream of the Nak-ding River from May 1994 to October was surveyed by the measurement of chl-orophyll a, total phosphorus, total nitrogen, dissolved inorganic phosphorus, nitrate-nitrogen, ammonia-nitrogen concentration, and secchi disc transparancy. Chl. a, TP, TN, DIP, NO_(3) and NH_(3)-N concentration was maintained at high level during the investigation period. And they also showed the peak after the input of Kumho River. Chl. a concentration was increased from 14.2㎎/㎥ in May to 95.2 in October. TP ane TN concentration was maintained always above 100㎎/㎥ and 3~4㎎N/l, respectively. TN/TP ratio were less than 16 from June to September with a few exceptions. Therefore, nitrogen is the limit-ing nutrient in the Nakdong River. Trophic states were in the range of eutrophic to hypertrophic, from 60 to80.

방전관용 전극개발 및 특성에 관한 연구

안성환,황동원,최준영,송시준,전용우,박원주,이광식 영남대학교 공업기술연구소 2001 工業技術硏究所論文集 Vol.29 No.1

This paper describes the development of sputtered tungsten electrode for discharge tube by making use of Sputtering method using plasma. The Xe discharge tube was designed and fabricated by using sputtered tungsten electrode, and the ICCD(Intensified Charged Coupled Device) and monochromator were used in order to observe the discharge image distribution and to measure the signal intensity. As a result, the emission light form the electrode was spreaded almost uniformly over a wide wavelength band, and the discharge image distribution and the signal intensity show quite a uniform distribution. The emission light from the Xe discharge tube was peaked at 488[nm] and 648[nm].

경관 Simulation을 통한 수영강 연접지역의 건축물 고도규제 방안

윤시운,이광국,황영우 東亞大學校 建設技術硏究所 1999 硏究論文集 Vol.23 No.1

This study analyzes the future landscape assesment of Suyoung-River and adjacent areas. Computer Simulation method is used for these purposes. It is expected that the high buildings and high density in Suyoung Information Site might cover the Jang-Mountain view. Therefore this study analyzes the expectations by the experiment of the change of the heights of buildings and the view-point so that Suyoung Information Site can secure the feelings of openness and can be harmonious with natural landscape and skyline. If the high dense buildings are going to be constructed, the optimum condition of development should be between 1.5 and 2.0 of evaluation indicator. The minimum indicator 1.5 would be appropriate as the standard of regulation. The results show that the buildings along the riverside road in the west need to be regulated under the height of 30m(about 10 stories) and the buildings along the Chungryul-Street in the east under the height of 90m(about 30 stories). 하천은 산과 구릉지 등과 함께 도시의 아름다운 경관을 형성하는 중요한 경관요소이다. 도시내 하천변에 나타나는 경관문제는 대부분 대규모 건축물에 의한 경관 훼손에서 비롯된다. 부산의 대부분 하천은 시가지를 통하여 바다로 유입되고 있으나 대부분 복개되었거나 주변지역의 고층건물 입지로 인해 하천 자체가 시민에게 주는 정 (正)의 경관적 요소는 점점 감소하고 있다. 본 연구의 대상지인 수영강은 현재 시가지내를 흐르고 있어 시민에게 주요한 openspace로 기능하고 있다. 주변지역은 지금까지 수영 비행장이라는 기능으로 연해 개발이 유보되어 오다 최근 수영정보단지의 개발계획 등으로 인해 개발압력을 강하게 받고 있다. 향후개발이 진행된다면 수영강변에서 조망할 수있는 주변 자연경관과 시가지 경관은 차폐될 뿐만 아니라, 그 자체의 규모가 크고 형태도 단조로와 위압적이고 획일적인 경관이 형성되게 될 것이다. 현재에도 수영강변의 구릉지에는 아파트 가 입지하여 조망을 차폐하고 있을 뿐 아니라 녹지를 잠식하고 있다. 이러한 현상은 향후 개발압력에 빌려 수영강변의 어느 지역 에서나 발생하는 공통적인 현상이 될 것이다. 이러한 조망차폐, 획일성, 위압감의 조성, 지형의 훼손 및 잠식 등으로 대표되는 수영강의 경관문제는 현행법상 건축심의 시 받는 경관심의로 해결하기에는 한계가 있다. 따라서 본 연구는 수영강과 연접지역, 그리고 배경녹지축인 주변산을 공간적 범위로 하여 첫째, 수영강 연접지역의 범위를 설정하고 연접지역을 몇 개의 경관구역으로 나누어 각 경관구역별 경관의 문제점과 특성을 살펴본다. 둘째, 경관분석을 위하여 Computer를 이용한 수영강변 주요 조망점 에서 사람의 눈에 보이는 대로 주변 경관을 연출해 낼 수 있는 가상의 경관 Simulation을 실시한다. 셋째,이를 바탕으로 수영강 연접지역의 건축물 고도규제 를 위한 기준설정과 고도규제 방안을 제안하는데 목적이 있다.

수출용 축양품종 가지의 염절임 공정의 최적화

남학식,김남우,황성희,윤광섭,신승렬 한국식품저장유통학회 ( 구 한국농산물저장유통학회 ) 2003 한국식품저장유통학회지 Vol.10 No.3

가지의 수출 경쟁력 향상을 위한 한 방안으로 수출용 가지품종인 축양품종을 염가공품으로 개발하기 위하여 염절임공정을 최적화하였다. 염절임 시간, 절임온도, 염농도를 독립변수로 하고 절임 후 수분함량, 염도, 표면과 내부의 색도 등을 종속변수로 하여, 중심합성계획법으로 실험을 설계하여 최적조건을 얻고자 하였다. 수립된 이차회귀모형으로 예측식을 수립할 수 있었으며 특히 수분함량이나 염도, 표면과 내부의 L과 b 값에 대하여 높은 적합도를 보여 최적조건을 수립하기 위한 제한 변수로 선정하였다. 염농도를 중심점(30%)에서 고정시켜서 얻은 절임시간과 온도는 각각 5.5~6.5일과 13-17℃였으며, 이때의 종속변수의 제한 요건으로는 수분함량 84%이하, 염도 14%이하 표면 L값 10-20, b값 0이하, 내부 L 값은 70-75, b 값이 16-18이었다. This study was conducted to the optimize salting process of eggplant for development new product and enhancement quality for export. Three variables by five level central composite design and response surface methodology were used to determine optimum conditions for salting time, temperature and salt concentration. Optimization of the process was conducted using the combination of the moisture content, salinity and color of surface and inside of salted eggplant. The regression polynomial model was suitable (P>0.05) by Lack-of-Fit analysis with highly significant. To optimize the process, based on surface response and contour plots, the individual contour plots of the response variables were superimposed. The optimum conditions for this process were 6 days and 15℃ at 30% concentration under the optimum of restricted variables as moisture content was below 84%, salinity was below 14%, L and b value of surface were 10 to 20 and below 0, L value and b value of inside were 70 to 75 and 16 to 18.

자일리톨, 후노란, 제2인산칼슘 및 카제인포스포펩타이드배합껌이 법랑질의 광질재침착에 미치는 영향에 관한 실용실험연구

이병진,배광학,박우철,양준영,황수정,노정,백대일,김종배 대한구강보건학회 2003 大韓口腔保健學會誌 Vol.27 No.4

The object of this study was to investigate caries preventive effect of chewing gum containing xylitol, funoran, calcium hydrogen phosphate and casein phosphopeptide by examining Vickers' hardness and surface roughness with confocal laser microscope. Early caries-like lesions were created using 0.1 M lactic acid-sodium hydroxide buffer(pH 4.0). 8 pieces of 3am diameter bovine enamel specimen with early caries-like lesions were mounted into the recesses of lingual surface of the acrylic mandibular removable appliance. 13 subjects were the appliance for daytime and chewed control and experimental gums 7 times in a day, for 3 days. In order to evaluate the remineralization effect of chewing gum on specimens, we measured vickers' hardness number after chewing gum, 1 day, 2 days, 3 days after and calculated surface roughness immediately after chewing gum. Vickers' hardness number of experimental chewing gum was significantly higher than control in 2 and 3 days after. Surface roughness of experimental chewing gum was significantly lower than control immediately after chewing gum. These results showed that experimental gum has more effective in remineralization of bovine tooth enamel, and it is more effective at immediately after chewing.