추황배(Pyrus pyrifolia Nakai cv. Chuhwangbae) 과피로부터 1종의 Sterol과 3종의 배당체 화합물의 단리·동정

이유건(Yu Geon Lee1),조정용(Jeong-Yong Cho),이현주(Hyun Joo Lee),이용현(Yong Hyun Lee),이상현(Sang-Hyun Lee),한태호(Tae-Ho Han),김월수(Wol-Soo Kim),박근형(Keun-Hyung Park),문제학(Jae-Hak Moon) 한국식품과학회 2013 한국식품과학회지 Vol.45 No.5

본 연구에서는 배의 유용성 증명을 위한 일환으로 배의 화학성분을 분자수준에서 밝히고자 하였다. 이에 배 과피 MeOH 추출물을 용매분획하여 얻은 EtOAc-산성 분획과 EtOAc-중성분획을 대상으로 Sephadex LH-20, silica gel, 그리고 ODS colmn chromatography와 HPLC를 이용하여 정제 및 단리하였다. 그 결과, EtOAc-산성 분획과 EtOAc-중성 분획으로부터 각각 2종씩의 화합물을 단리하였다. 단리된 화합물 1-4는 1H- 및 13C-NMR 분석을 통하여 각각 (S)-(+)-2-cis-abscisic acid O-β-D-glucopyranosyl ester (화합물 1), 1-[4-O-β-D-glucopyranosyl]phenyl ethanone(piceoside, 화합물 2), β-sitosterol (화합물 3), 그리고 β-sitosteryl 3-O-β-D-glucopyranoside (화합물 4)로 동정되었다. 단리된 3종의 배당체 화합물(화합물 1, 2, 4)들은 본 연구에 의해 배로부터 처음 동정되었으며, 화합물 3은 추황배로부터 처음 동정되었다. 본 연구결과가 배 함유 성분연구는 물론 배의 기능성 해명 연구에도 추후 중요한 기초자료로 활용되길 기대한다. We isolated and identified antioxidants from acidic and neutral ethyl acetate fractions of the peel of pear (Pyrus pyrifolia N. cv. Chuhwangbae). We isolated 4 compounds from the methanol extract, by using 3 different types of column chromatography (Sephadex LH-20, silica gel, and octadecylsilane) and preparative HPLC. We identified the isolated compounds as (S)-(+)-2-cis-abscisic acid O-β-D-glucopyranosyl ester (compound 1), 1-[4-O-β-D-glucopyranosyl]phenyl ethanone (picroside, compound 2), β-sitosterol (compound 3), and β-sitosteryl 3-O-β-D-glucopyranoside (compound 4) by nuclear magnetic resonance analysis. We are the first to report the identification of compounds 1, 2, and 4 from pear.

단상 유도형 동기 전동기(LSPM)의 특성해석에 관한 연구

정대성,김승주,이진헌,최재학,이주,Jung, Dae-Sung,Kim, Seung-Ju,Lee, Jin-Hun,Choi, Jae-Hak,Lee, Ju 한국조명전기설비학회 2007 조명·전기설비학회논문지 Vol.21 No.3

가전분야에서의 전동기 효율향상을 통한 에너지 소비절감 효과는 상당히 크지만 이를 위한 전동기의 설계/해석 기술 확보가 아직은 미흡한 상태이다. 이에 따라 유도형 동기전동기가 제안되었지만, 유도형 동기 전동기는 유도전동기와 통기전동기의 특성을 동시에 가지고 있어, 해석 및 설계가 쉽지 않다. 따라서 본 논문에서는 기존의 냉장고 압축기용 전동기인 단상유도전동기를 대처할 수 있는 단상 유도형 동기전동기를 이용해 파라미터에 따라 특성이 어떻게 바뀌는가에 대해 서술하였다. 그에 따라 단상유도전동기의 정상상태 특성을 해석하고 제안모델의 성능을 기존모델과 비교하고 실험하여 해석결과의 신뢰성을 검증한다. 또한 본 논문에서는 제안모델의 기존 고정자 형상이나 권선 스팩을 유지하고 회전자의 형상이나 구조만을 변경시켜 성능향상을 도모하였다. 해석방법으로는 전자장 수치 해석적인 방법으로 널리 이용되고 있는 유한요소법(Finite Element Method : FEM)을 이용하였다. Electric motor efficient improvement from home appliance field is important to the effect reducing the energy consumption. But the electric motor design/analysis technology is still insufficient. Specially the electric motor design/analysis technology of satisfying characteristic of both the induction motor and the synchronous motor such as Line start permanent motor. Therefore the electric motor design/analysis technology is urgently demanded reliability. This paper proposes the sing1e-phase line-start permanent magnet motor to develop the motor it with be able to alternate the sing-phase induction motor it is a refrigerator compressor motor. The sing-phase induction motor is analyzed in the steady state. And we have a certification test to compare our single-phase line-start permanent magnet motor with the sing-phase induction motor. In order to improve the performance, the stator of the single-phase line-start permanent magnet motor is same as the stator of the sing-phase induction motor and changes the rotor form and has the permanent magnet. It used the Finite Element Method(FEM) which is widely used with electronic-magnetic field numerical analysis method.

韓國歷史地理硏究 : 陸上 交通(主로 驛站制를 中心으로)에 關한 考察 (The system of Yeuk-Cham in the over-land communication)

李聖學 경북대학교 1968 論文集 Vol.12 No.-

1. The system of Yeuk-Cham (驛站) is a conveying method of an official document in the system of bureaucratic government and centralization. It is essential function but has transformation. 2. The Yeuk-Cham divides up three types according to the significance. 3. The distribution of Yeuk-Cham means human development and the circumstance, and a number of the large-Yeuks is posted near the Capital and the province of Pyong-An, but the many little-Yeuks is at the southern Korea. 4. The management of Yeuk is different by rank. Its- treatment had different grade by official status. 5. The system of Phal-Cham(撥站) has other function, and it is Ki-Phal(騎撥) (carried by house) from the Capital to I-Chu. For Korea has a deep relation with China, but from Dong-Rae to Ham-Kyung it is Bo-Phal(步撥). 6. The settlements originated by Yeuk-Cham, disregarded by the society at Yi-Dynasty. 7. Yeuk-Cham was abolished by the development of railway and road, but their relation is importance.

한국북방경역의 역사지리학적 연구(Ⅰ)

이성학 慶北大學校 1969 論文集 Vol.13 No.-

1) A study of historical change on the north frontiers of Korea. 2) The north boundary was the region of Yo-Dong (遼東) or the river of Pea (浿水) during Ancient-Korea dynasty. It was changed by the vicissitudes or rise and fall of the northern nations. 3) The Emperor of Han (漢) governed the peninsula of Han (韓). Its southern frontier was chiefly the northern region of the Han River (漢江) and the mountaion of Chul-Yung (鐵嶺) 4) Kokuryo(高句麗) occupied the greatest northern territory at the time of King, Yung Rak(永樂): the northern boundary was the eastern region of the river of Yo (遼河) and the region of the Song-Wha River was the large territory which were from Jang-Chun (長春) Nong-An(農安) Ha-L-Bin(哈爾濱) to the East-Sea. (東海) 5) Shilla(新羅) unified three states, yet the did not occupied all of Kokuryo territory but a part of it. The north-western frontier of Shilla was region on the river of Tea-Dong (大同江) Chung-Wha(中和) Sang-Won(祥原) and Kok-San(谷山). The north-eastern frontier of Shilla was the northern region of Chul-Yung(鐵嶺) An-byun(安邊) and northern Kang-Won(江原) of today. Shilla should have occupied the larger northern region, but it was not so large. Note : This is the northern frontier from Ancient-Korea to Shilla Dynasty, but those of Koryo(高麗) and Rhee Dynasty(李朝) will be mentioned at the next number.

표면 SH파 모드의 분산특성 해석과 그 응용

이상용,박익근,윤종학,노승남,안형근 한국공작기계학회 2001 한국공작기계학회 춘계학술대회논문집 Vol.2001 No.-

A new flaw detection technique using by SH angle beam method has been discussed. The SH-wave is horizontally polarized shear wave and the surface SH wave has a characteristic of traveling along near surface layer. The surface SH wave technique is valuable for the detection of fatigue cracks at fillet weld heels which cannot be detected by other ultrasonic technique such as angle beam technique and The dispersion curves of it has simple characterization. In this work, using these beneficial chraterization, quality evaluation of spot weld with ultrasonic sound intensity of SH-wave passing through nugget area of spot weld are verified experimentally.

포도에 대한 Captafol 수화제의 안전사용기준 설정

李載球,慶箕性,金學南 충북대학교 농업과학기술연구소 1993 農業科學硏究 Vol.11 No.1

In order to establish the criteria for the safe use of the fungicide captafol on grapes, 12 plots with different spray frequency and different spray time were placed and sprayed on stems and leaves with the captafol wettable powder up to 3, 7, 15, 30, 45, 60 days before harvest. The results of the analysis of captafol residues on the sample grapes were as follows : 1- Recovery values obtained from fortified control samples were 85.3 and 90.0%, respectively, at the 0.1 and 1.0 ppm levels, the detection limits being 0.06 ng(0.015 ppm). 2. Captafol residues were detected in all samples, ranging from 0.25 to 5.79 ppm. 3. Captafol residues had a tendency to become the more, the more spray frequency and the closer spray time to harvest. 4. The captafol residues on grapes were within the maximum residue limits in the samples sprayed 4 times involving those sprayed up to 3 days before harvest, whereas the residues in the samples sprayed 5 times were beyond the limits. 5. It was recommended that the captafol WP should be sprayed on grapes 4 times up to 7 days before harvest.

주한 미군부대 Card Holder의 물품구매방식에 대한 실증적 분석

이재하,최승학 남서울대학교 2005 남서울대학교 논문집 Vol.11 No.2

The purpose of this study is to analyze the purchase behavior of GPCH and to scheme a strategic purchase way. The categories for purchase behavior are classified by purchase way, purchase difficulty, purchase mistake, observance of SOP rules, and ability of GPCH etc. The sample size of this study is 49 GPCH. The major findings of this study are as follows. 1) GPCH attached much importance to purchased cost, purchased quality of goods, and time limit for purchase. 2) GPCH generally get information on purchased goods from goods magazine, and Internet. But there is very encourage in confirming the goods for purchased with his own eyes before purchase. 3) GPCH preferred local purchase to global purchase, because of easy for identifying goods and enough exchange of views. But GPCH have to make remarkable progress in English communication to prepare for global business era. 4) The major reasons for mistake in uses of the GPCH were double approval to vendor and insufficiency understanding of SOP. 5) The group of single limit 2,000 $ below showed more faithful to his duties than single limit 2,000 $ above. Concurrently, the results of this study will be useful guidelines for strategically purchase goods to GPCH.

한국인 부정교합자의 하악 치열궁의 크기와 형태

이성준,백승학,김상철,국윤아 대한치과교정학회 2005 대한치과교정학회지 Vol.35 No.1

본 연구의 목적은 한국인 부정교합자에서 하악 치열궁간의 형태적 차이를 알아보고자 하였다. Ⅰ급 114명. Ⅱ급 119명, Ⅲ급 135명의 부정교합자를 대상으로 하악 모형의 교합면을 복사한 후 13개의 접촉점 중에서 가장 협측면으로 위치한 부분을 digitize 하였고 각 치아의 브라켓 위치에 해당하는 점을 하악치아의 두께에 의거하여 4개의 선계측과 2개의 비율을 측정하였다. 치열궁의 형태는 square ovoid, tapered형으로 분류하여 그 빈도를 조사한 결과 Angle 분류와 남녀 성별에 따른 특별한 치열궁 형태가 존재하지 않았으나, 특정 치열궁 형태의 빈도는 Angle 분류에 따라 다르게 나타났다. 치열궁 크기의 계측항목에서는 대구치간 폭경에서만 남녀 성별 차이를 보였으며, 치열궁 크기에 있어서 Ⅰ급과 Ⅲ급, Ⅱ급 부정교합군간에는 유의한 차이가 있었다. 치열궁 형태의 분포는 Ⅰ급과 Ⅲ급 부정교합군에서는 square, ovoid, tapered 형태 순이었고, Ⅱ급 부정교합군은 square, tapered ovoid 형태 순이었다. 치열궁 형태의 빈도분포에 있어서는 남녀간의 차이는 없었다. The purpose of this study was to clarify morphological differences among mandibular dental arch forms in Korean malocclusion patients. The sample in this study consisted of 114 Class Ⅰ, 119 Class Ⅱ, and 135 Class Ⅲ malocclusion cases. The most facial portions of 13 proximal contact areas were digitized from photocopied images of the mandibular dental arches. Clinical bracket points were calculated for each tooth based on the data of the mandibular tooth thickness. Four linear and two proportional measurements were undertaken. The dental arches were classified into square, ovoid, and tapered forms to compare the frequency distributions. Our results suggested that there was no single arch form specific to any particular Angle classification or sex. It appeared to be the frequency of a particular arch form that varies among the Angle classifications. In comparison of arch measure between male and female, there was no statistical difference except in the intermolar width. In comparison of arch size measurements among the different Angle classifications, there were statistically significant differences between Class Ⅰ and Class Ⅲ malocclusion groups and between Class Ⅱ and Class Ⅲ malocclusion groups. In comparison of frequency distribution of arch forms in Class Ⅰ and Ⅲ malocclusion groups, the square form demonstrated the highest distribution followed by the ovoid and tapered forms in that order. In the Class Ⅱ malocclusion group, the square form showed the highest distribution, followed by the tapered and ovoid forms in that order. There was no statistical difference in the frequency distribution of arch forms between male and female groups.

임신중 우측난소의 자궁내막장종의 성장과 파열의 1례

이종학,홍순도,남상욱,최종호,허광현,박일영 啓明大學校 醫科大學 1993 계명의대학술지 Vol.12 No.2

계명의대 산부인과에서 35세된 경산부에서 임신과 동반된 우측 난소의 자궁내막낭종의 성장과 파열을 경험하였기에 이에 문헌고찰과 함께 보고하는 바이다 Pregnancy had long been considered to have beneficial effect on endometriosis. During the pregnancy, extrauterine endomertrial tissues did not growth or enlarged because of physiologic amenorrhea and producing hormonal effect. However, we experienced a patient who underwent emergency exploratory laparotmy at gestation week 34/4 for rupture of an ovarian endometriotic cyst. The patient had a Cesarean section delivery of a 1,960gm female baby, who died at 1st day of life.

성토사면에 적용된 Soil Nailing의 주면마찰특성 연구

이성철,김명학,김상현,윤성학 인제대학교 2001 仁濟論叢 Vol.16 No.1

Soil Nailing 공법은 사면안정을 목적으로 보강재를 사용하여 지반을 보강하는 현장 지반보강 공법의 일종이다. 지금까지는 일반적으로 Soil nailing이 주로 절토사면을 보강하는 기술로 사용되고 연구되어 왔으나 본 논문에서는 붕괴된 사면에 재성토를 시행한 현장에 대한 보강공법으로서의 적용성을 연구하였다. 이를 위하여 네일에 스트레인 게이지를 부착하고 현장인발실험을 수행하여 최대인발하중을 조사하고 각 지층에서 발휘되는 단위 주면마찰력을 산정하였다. 그리고 본 연구에서 얻어진 겉보기 평균 주면마찰력을 일반적인 절토사면에서 현장인발실험을 수행한 다른 사례의 겉보기 평균주면마찰력과 비교분석해 보았다. Soil nailing is in-situ ground improvement technique of reinforcing soils using passive inclusions for the purpose of slope stability. Also soil nailing, in general, was used and studied as a reinforcement technique at cut slope, but this paper presents the results of study for soil nailing application as a reinforcement technique at the banking over slided slope. In-situ pull-out tests of nails, instrumented with strain gauges, were performed to investigate the maximum pull-out load and to calculate the unit side resistance in each different layer, And the apparent average unit side resistance of this study was compared with that of other sites installed at cut slop.