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Shin, Man Sub,Park, Yoon Kook,Nam, Sung Chan,Hwang, Kwang-Jin The Chemical Society of Japan 2012 Chemistry letters Vol.41 No.2
<P>This investigation demonstrated that bicarbonate ions were selectively formed over carbamate in a CO<SUB>2</SUB> absorption process using piperidine and piperazine derivatives based on <SUP>13</SUP>C NMR. Piperidines with methyl or hydroxymethyl substituent at 2 position (PiP-Me and PiP-MeOH) and 2,5-dimethylpiperazine (DM-PiZ) generated the bicarbonate ions as main adducts in reaction with CO<SUB>2</SUB>. The absorptions of CO<SUB>2</SUB> by those aqueous amines (PiP-Me and DM-PiZ) were faster than those of MEA (2-aminoethanol).</P>
Modeling and Applications of Electrochemical Impedance Spectroscopy (EIS) for Lithium-ion Batteries
Choi, Woosung,Shin, Heon-Cheol,Kim, Ji Man,Choi, Jae-Young,Yoon, Won-Sub The Korean Electrochemical Society 2020 Journal of electrochemical science and technology Vol.11 No.1
As research on secondary batteries becomes important, interest in analytical methods to examine the condition of secondary batteries is also increasing. Among these methods, the electrochemical impedance spectroscopy (EIS) method is one of the most attractive diagnostic techniques due to its convenience, quickness, accuracy, and low cost. However, since the obtained spectra are complicated signals representing several impedance elements, it is necessary to understand the whole electrochemical environment for a meaningful analysis. Based on the understanding of the whole system, the circuit elements constituting the cell can be obtained through construction of a physically sound circuit model. Therefore, this mini-review will explain how to construct a physically sound circuit model according to the characteristics of the battery cell system and then introduce the relationship between the obtained resistances of the bulk (R<sub>b</sub>), charge transfer reaction (R<sub>ct</sub>), interface layer (R<sub>SEI</sub>), diffusion process (W) and battery characteristics, such as the state of charge (SOC), temperature, and state of health (SOH).
신현수,허옥순,이진하,김세은,주인선,신동우,강석종,박만종,김지연,김근희,강숙경,정래석,허숙진,소유섭,최장덕,문병우,김진수 식품의약품안전청 2001 식품의약품안전청 연보 Vol.5 No.-
본 연구는 패류중 중금속함량 측정을 위한 분석효율이 높고 간편한 분해법을 찾아내어 그 방법에 의끓 유종중인 패류중 중금속함량을 파악하고자 수행하였다. 시료를 분해시키는 Microwave와 습식, 건식회법을 비교한 결과 변형습식회화르가 가장 적합하였다. 변형습식회차딘는 려린0,3+C104+H2SOf의 혼찰산을 쪼 · j 1 (v/v)의 비율로 혼합하여 사용하였 을 때 회수을 Pb린틴. Cd 97.8, Cu 94.2, Zn 92.8%를 나타내었근 분해시간은 2~2.5시간 소요되었다. 유통중인 패류중 중금속함량 」최소~최대(평균), mgAgl 은 Pb 0.028~o.528(0.153), Cd 0.OO7~1,832(0.587), Cu 0.360~37.375(4.6691, Zn 6.317~233.2iO(38.881), Hg 0.001 ~O.151(0.012)mg/ltg으로 나타났다. 또한 유통중인 5종의 패류중 중금속평균항량이 생산지 하재지역에서 구입한 패류에 비해 모든 중금속언써 약간 높은 함량을 보였으나 오염된 수준이 아닌 자연함유량수준이었다. This study was conducted to improve the digestion method for the determination of heavy metals in shellfishes and to estimate the contents of heavy metal in commercial shellfishes by their digestion method. This digestion method was compared microwave with wet and dry ash digestion for shellfish samples, obtained results showed that the modified wet ash Ⅱ digestion was convenient and easy to use. For the modified wet ash Ⅱ digestion, The mixed acid of HNO₃+HClO₄+H₂SO₄(25:5:1, v/v) was used. Under this condition, Recoveries were Pb 94.3, Cd 97.8, Cu 94.2 and Zn 92.8% and digestion time was ∼2.5 hours. The contents of heavy metal [minimum∼maximum (mean), mg/kg in commercial shellfishes were as follows ; Pb:0.028∼0.528(0.153), Cd:0.007∼1.832(0.587), Cu:0.360∼37.375(4.669), Zn:6.317∼233.250(38.881), Hg:0.001∼0.151(0.013). The contents of heavy metal in commercial shellfishes of five species were slightly greater than those of shellfishes purchased at Hajae. There was no great difference between the contents of heavy metal of Hajae and those of shellfishes purchased at Whole market.
비금속광물 제품제조업에서 발생하는 분진 농도와 분진 노출기준 적용에 따른 문제점 고찰
신창섭,김현욱,노영만,피영규,원정일,고원경 한국산업위생학회 2000 한국산업보건학회지 Vol.10 No.1
This study was carried out to estimate current status of dust concentrations in the factories producing non-metallic products in Korea. Data were gathered from the environmental monitoring reports by 40 workplace environmental monitoring institutes and the questionnaire designed for the study by the authors. A total of 1838 dust samples from 368 plants were obtained from the reports and were analyzed with no data modifications. But data on asbestos, rock wool, and welding fumes were excluded in this evaluation. The factories were classified into eight groups according, to the standard industrial classification scheme un Korea. The results of this study were as follows: 1. The factories included were glass, non-refractory ceramic, refractory ceramic ware, structural non-refractory clay and ceramic, cement and lime, articles of concretes, and stone. Mean(geometric mean) concentrations of total dust samples ranged from 1.75(0.84)㎎/㎥ to 5.87(2.84)㎎/㎥. Statistically significantly higher dust concentrations were found in the cement and lime industries compared with other industries. 2. The non-compliance rates were 15.2% in glass and 20.6% in other non-metallic mineral products industries. Although all institutions surveyed utilized the identical sampling and classification scheme for dusts as specified in the current occupational exposure limits, wide discrepancies were found in collecting samples and classifying dusts. Further problems were discovered in classifying dusts. A dust sample collected could be classified into any of the three groups regardless of silica content. The results of this study showed that dust concentrations in the non-metallic products industries varied widely. Also discovered was classification errors of dust types among workplace monitoring institutes. These errors could adversely affect the results of exposure assessments and the true nature of dust hazards. Further, no institutions performed respirable dust sampling and analysis of crystalline silica. In order to correct these malpractices, current standards of occupational exposure limits should be revised and tight supervision by the Ministry of Labour be suggested.
Test Results of Refrigerant R152a in a Mobile Air-Conditioning System
Shin, Jeong-Sub,Park, Won-Gu,Kim, Man-Hoe The Society of Air-Conditioning and Refrigerating 2008 International Journal Of Air-Conditioning and Refr Vol.16 No.2
This study presents test results of a mobile air-conditioning system using a potential alternative refrigerant, R152a. A series of performance tests have been carried out and cycle characteristics such as cooling capacity, energy efficiency ratio, suction and discharge pressures, and temperatures are presented, compared to those for the baseline R134a system. Tests were conducted with evaporation temperature of $5^{\circ}C$, condensation temperature of $45^{\circ}C$, subcooling temperature of $5^{\circ}C$, superheating temperature of $5^{\circ}C$, and compressor speed of 500-1500 rpm. The performance of R152a system with readjustment of an expansion valve showed better than those of R134a. The effect of oil on the pressure drop in the evaporator was also addressed.