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- 저자 : 정용삼 (검색결과 121 건)
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정용삼,문종화,정영주,박광원 한국지하수토양환경학회 1998 지하수토양환경 Vol.5 No.4
In general the concentration of uranium in natural water such as fresh water and sea water is in the range of 0.01∼5 ppb, therefore trace analytical technique is required. The aim of present work is to compare a direct and preconcentration methods by evaporation and to investigate rapid and accurate trace analysis of uranium in groundwater using Instrumental Neutron Activation Analysis (INAA) which are sensitive and nondestructive method. Identification of analytical procedure was carried out using uranium standard solution of the range of 0.5∼100 ppb. In the given concentration, the deviation of calibration curve was less than 2%, and the standard deviation of measured values at each concentration was the range of 2∼12%. The difference of U content with sampling time for the same sample site was about 10.3%. Using this established method, the concentrations of uranium in samples collected at the 17 spring of Choongchung areas were found to be in the range of 1∼80 ppb.
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정용삼,문종화,정영주,박용준,이길용,윤윤열,이수형,김경태 한국지하수토양환경학회 1998 지하수토양환경 Vol.5 No.2
For the application of study on pollution and conservation of environment determination of 33 elemental concetrations in different sediment samples were carried out using instrumental neutron activation analysis (INAA). For verification and evaluation of the analytical method, three standard reference materials (two NIST SRMs and one NRCC CRM) were chosen and the accuracy and precision of the analysis were estimated by comparison to the certified values. Under the optimum condition, the analytical procedure to apply a practical sample was estimated. Neutron irradiation of sample was done at the irradiation facilities (neutron flux, 1-3${\times}$10$\^$13/n/$\textrm{cm}^2$$.$s) of the TRIGA MARK-III and HANARO research reactor in the Korea Atomic Energy Research Institute. In addition, analysis of two IAEA's sediment was performed according to the pre-established analytical method. The analytical results of elements such as Al, As, Co, Cr, Fe, Sb and Zn by INAA were intercompared with those of WD-XRF, ICP-MS and AAS, and are relatively agreed with each other.
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정용삼,문종화,조현제,김영진,Chung, Yong-Sam,Moon, Jong-Hwa,Cho, Hyun-Je,Kim, Young-Jin The Korean Society of Analytical Science 2005 분석과학 Vol.18 No.1
A comparison of the analytical data obtained by three $k_0$-NAA software programs was carried out using both the airborne particulate matter collected from an urban site and the certified reference materials of the air filter and urban dust to evaluate the performance of the analysis. The individual $k_0$-NAA standardization methods of three countries, Korea, China and Vietnam which had been modified from the well established $k_0$-program were used for the comparative analysis. The measured concentrations of 30 elements from the two kinds of air samples based on this software were in agreement with each other within about 20% analytical error except for a few elements. By contrast, the results of China and Vietnam were moderately higher than that of Korea due to a systematic error associated with the detection efficiency, gamma peak analysis and geometric effect.
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