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헤드스페이스-가스크로마토그래피-질량분석법에 의한 체모 중 포름알데하이드 측정법 연구
신호상,안혜실,Shin Ho-Sang,Ahn Hye-Sil 한국환경보건학회 2006 한국환경보건학회지 Vol.32 No.1
A gas chromatography/mass spectrometric method was developed for the determination of formaldehyde in hair. 0.3mg of hair was placed in 10ml headspace vial. 1.5mM pentafluorophenylhydrazine solution (pH 2) in 0.03 M phosphoric acid and $20\;{\mu}l$ of 500 mg/l $acetone-d_6$ as internal standard were added in vial and sealed tightly with cap. The solution was heated for 30 min at $90^{\circ}C$ in heating block. The extraction, the derivatization and the evaporation were performed simultaneously. After heating of the solution, 0.5 ml of headspace was taken up and analyzed by gas chromatography-mass spectrometry (GC-MS). Low limit of detection (LaD) and Low limit of quantitation (LOQ) of formaldehyde were 0.5 and 1.5 ng/g, respectively. The method was used to analyze formaldehyde in rat hair after oral exposure. The developed method may be valuable to be used to analyze formaldehyde in human hair.
에틸렌옥사이드에 폭로된 흰쥐의 혈액에 형성된 헤모글로빈 부가체에 대한 연구
이진헌,신호상,안혜실,Lee Jin-Heon,Shin Ho-Sang,Ahn Hye-Sil 한국환경보건학회 2006 한국환경보건학회지 Vol.32 No.2
Ethylene oxide is a genotoxic carcinogen with widespread uses as industrial chemical intermediate and gaseous sterilant. 2-hydroxyethylated N-terminal valine in Hb is a good biomarker for biological monitoring of ethylene oxide exposure, because of its stability. For measuring the hemoglobin adduct formed by exposure of ethylene oxide, we studied the determination of (N-2-hydroxy-ethyl)valine(HEV) in hemoglobin adduct by using GC/MS. Firstly we synthesized HEV with 2-amino-ethanol and bromoisovaleric acid(BIVA) and confirmed it with GC/MS-FID. Its fragmentations were m/z 116(base ion, M+-45) and m/z 130(M+-31). For measuring HEV with higher sensitivity, we use derivatives which were PFPITH(pentafluorophenylisothiocianate) and TBDMS (tributyldimethylsilylation) by using Edman procedure. Its fragmentation were m/z 425(M+-57), m/z 383(M+-99) and m/z 172(M+-310) by using GC/MS. We did biological monitoring for mice inhalation exposure with 400 ppm ethylene oxide. The concentrations of hemoglobin adduct were $168{\pm}3.8\;and\;512{\pm}04$(nmol g-1 globin) at 0.5 hr/day 400 ppm ethylene oxide inhalation exposure group, and $631{\pm}17\;and\;2265{\pm}9.4$(nmol g-1 globin) at 1.0 hr/day 400 ppm ethylene oxide inhalation exposure for 1 and 4 weeks, respectively. We confirmed that (N-2-hydroxy-ethyl)valine(HEV) of hemoglobin was a good biomarker for biomonitoring of ethylene oxide exposure, and can measured with derivatives such as PFPITH(pentafluorophenylisothiocianate) and TBDMS(tributyldimethylsilylation) by using GC/MS.
이원호 ( Won Ho Lee ),안혜인 ( Hye In Ahn ),신현실 ( Hyun Sil Shin ),하태일 ( Tae Il Ha ),김소현 ( So Hyeon Kim ) 한국전통조경학회 2015 한국전통조경학회지 Vol.33 No.1
본 연구는 조경학 관점에서 백거이의 중은사상과 원림을 살펴보고 백거이의 조영활동이 갖는 의미와 그의 원림에서 나타난 사상과 조영방식이 후에 미친 영향에 대해서 고찰한 결과 다음과 같다. 첫째, 백거이의 ‘중은설’은 은일이론을 향상시켰으며 ‘중은’이론의 탄생은 사대부들의 문화예술 뿐만 아니라 원림 예술까지 발달하게 되는 계기가 되었다. 또한 산 속에 은거하여 원림을 조영하던 이전과는 달리 도회지로 나와 원림을 조영하게 되는 전환점을 마련하였다. 둘째, 백거이의 원림에 나타난 ‘호중천지’의 공간원칙은 화려하고 웅장했던 이전의 원림과는 달리 한정되고 소형화된 공간에서 바위의 배치, 동산의 조형, 꽃의 배치 등 자연을 끌어들이기 위한 하나의 수단이자 원칙이었다. 원림은 외부 경관만이 아니라 내면세계가 반영된 ‘심원’의 공간이 되었다. 셋째, 백거이의 시에 나타난 정원조영 행위와 사상은 후에 시가 차운되고 인용되면서 그림으로 그리고 자신의 정원으로 표현되었다. 결과적으로 백거이의 문학적 예술관과 사상은 자신의 원림을 경영했다는 실천적인 활동을 통해 후대 문인원림의 유행과 그 양식적 특징의 형성에 기반을 마련하였다. 넷째, 백거이의 유교적 체득의 경지와 섬세한 미의식은 산체와 수체의 융합, 가산 쌓는 법, 태호석의 미의식 발견을 통해 원림 경관의 의미를 부여하였고, 이후 원림 문화 형성에 영향을 끼쳤다. The purpose of this study was to look at the Jungeun-sasang(中隱思想) and garden of Bai Juyi in the perspective of landscape architecture and inquiry the meaning of Bai Juyi``s construction activities, thought shown in his gardens, and how his construction method influenced later and the result is as follows. First, the ``Jungeun-sasang(中隱思想)`` of Bai Juyi improved the Eunil-sasang(隱逸思想) and the birth of ``Jungeun-sasang(中隱思 想)’ became a clue to be developed up to the garden art. In addition, different from before that built gardens hiding in mountains, it prepared the turning point to build gardens in cities. Second, the space principle of ``paradise`` shown in the garden of Bai Juyi was a means and principle to absorb the nature such as positioning rocks, formation of mounds, and positioning of flowers in the limited and small spaces different from previous gardens of splendid and magnificent. The garden became not only outer scene but also the ‘Simwon(心園) that reflected the inside world. 12) Third, the gardening act and thought appeared in the poem of Bai Juyi were expressed in pictures and his own gardens as his poem was borrowed and quoted. As a result, Bai Juyi``s literary view on the art and thought prepared the base in the popularity of literary gardens and forming of characteristic styles through practical activities that he managed his own gardens. Forth, Bai Juyi``s level of Confucianism realization and delicate aesthetical consciousness gave meanings to the scene of gardens through the discovery of the fusion of mountains and creeks, ways of adding, and the aesthetical consciousness of Taihushi(太湖石)and influenced in the forming of garden culture later on.