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NMR Study of Successive Magnetic Transitions in the A-site Ordered Perovskite LaMn3Cr4O12
Yu Kawasaki,Syota Takase,Yutaka Kishimoto,Takashi Ohno,Ikuya Yamada,Kentaro Shiro,Ryoji Takahashi,Kenya Ohgushi,Norimasa Nishiyama,Toru Inoue,Tetsuo Irifune 한국물리학회 2013 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.63 No.3
We have investigated the successive magnetic phase transitions of the A-site ordered perovskiteLaMn3Cr4O12 by measuring 139La nuclear magnetic resonance (NMR) spectra. The successivemagnetic transitions are revealed by a very small but clear increase in the full width at half maximum(FWHM) of the 139La NMR signal at TM2 = 150 K and by the disappearance of the signal due to theline broadening at temperatures below TM1 = 50 K. These two magnetic transitions are associatedwith independent orderings within the Cr-site sublattice at TM2 and within the Mn-site sublatticeat TM1. Regarding the magnetic structure of the Cr-site sublattice at temperatures below TM2, thecancellation of internal fields at the La site, ruling out ferromagnetic and multi-q antiferromagneticstructures, is consistent with the typical antiferromagnetic structure for perovskites, such as G-,A- and C-type orders. The uncanceled internal field at the La site at temperatures below TM1is also consistent with these typical antiferromagnetic structures in the Mn-site sublattice. Thedifferences in the temperature dependences of the Knight shift K(T) and the bulk susceptibility χ(T) are consistently explained by the independent magnetic orderings of the Cr- and the Mn-sitesublattices and the cancellation of internal field originating from the Cr-site sublattice at the Lasite at temperatures below TM2.
POTENTIAL PROFILE MEASUREMENT OF CARBON NANOTUBE FETs BASED ON THE ELECTROSTATIC FORCE DETECTION
YUKI OKIGAWA,TAKEO UMESAKA,YUTAKA OHNO,SHIGERU KISHIMOTO,TAKASHI MIZUTANI 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2008 NANO Vol.3 No.1
We have measured the potential distribution on carbon nanotube (CNT) field-effect transistors (FETs) using electrostatic force microscopy (EFM) and Kelvin probe force microscopy (KFM). Clearer potential profiles were obtained by EFM than by KFM. When the CNT-FET is in the ON state, the EFM image shows uniform potential distribution along the CNT. In contrast, when the CNT-FET is in the OFF state, nonuniform potential image with dark spots are obtained. The dark spots can be attributed to the defects in the CNTs.
51V-NMR Study of the Quasi-one-dimensional Antiferromagnet BaCo2V2O8
Yukiichi Ideta,Yu Kawasaki,Yutaka Kishimoto,Takashi Ohno,Yoshitaka Michihiro,Zhangzhen He,Yutaka Ueda,Mitsuru Itoh 한국물리학회 2013 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.63 No.3
We have investigated the magnetic properties of quasi-one-dimensional antiferromagnetBaCo2V2O8 by the measurements of 51V-NMR spectrum. With decreasing temperature, Kk showsa broad peak around 30 K signaling the 1D short-range order in the Co2+ spin chain. The estimatedWeiss temperature Θ = −105 K, hyperfine coupling constants Akhf = 2.1 kOe/µB for H k c and Ahf= 2.6 kOe/µB for H ⊥ c at 13 kOe are comparable to those at 70.6 kOe. These results suggest thatstatic magnetic properties in the paramagnetic state are nearly independent of external magneticfield, although the ground N´eel state is suppressed by the application of external magnetic fieldabove Hc = 39 kOe along c-axis. In the antiferromagnetic state below TN = 5.4 K, the doublerectangle-like powder pattern was observed, indicating two V sites exposed to different size of internalfields, HA1 = 2.1 and HA2 = 3.8 kOe. The internal fields at V sites are explained by takinginto account of the classical and pseudo-dipolar fields from Co2+ magnetic moments.
Toshihiko Tomita,Hirokazu Fukui,Daisuke Morishita,Ayako Maeda,Yutaka Makizaki,Yoshiki Tanaka,Hiroshi Ohno,Tadayuki Oshima,Hiroto Miwa 대한소화기 기능성질환∙운동학회 2023 Journal of Neurogastroenterology and Motility (JNM Vol.29 No.1
Background/AimsDiarrhea-predominant irritable bowel syndrome (IBS-D)-like symptoms frequently occur in patients with quiescent Crohn’s disease (CD). To investigate the factors underlying IBS-D-like symptoms in patients with quiescent CD, we performed a comprehensive analysis of the clinical features and intestinal environment in those patients. MethodsWe performed a prospective observational study of 27 patients with quiescent CD (CD activity index [CDAI] ≤ 150; C-reactive protein ≤ 0.3 mg/dL). The presence and severity of IBS-D-like symptoms, health-related quality of life, disease-specific quality of life, and status of depression and anxiety were evaluated. The level of intestinal permeability, fecal calprotectin and organic acids and the profiles of gut microbiome were analyzed. ResultsTwelve of the 27 patients with quiescent CD (44.4%) had IBS-like symptoms, and these patients showed a significantly higher CDAI, IBS severity index and anxiety score than those without. The inflammatory bowel disease questionnaire score was significantly lower in the patients with IBS-D-like symptoms. There were no significant differences in small intestinal/colonic permeability or the levels of organic acids between the patients with and without IBS-D-like symptoms. Fusicatenibacter was significantly less abundant in the patients with IBS-D-like symptoms whereas their fecal calprotectin level was significantly higher (384.8 ± 310.6 mg/kg) than in patients without (161.0 ± 251.0 mg/kg). The receiver operating characteristic curve constructed to predict IBS-D-like symptoms in patients with quiescent CD using the fecal calprotectin level (cutoff, 125 mg/kg) showed a sensitivity and specificity of 73.3% and 91.7%, respectively. ConclusionMinimal inflammation is closely associated with the development of IBS-D-like symptoms in patients with quiescent CD.