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오미현,임무성,채정영,김은정,조중훈,임철수,최선옥 한국식품위생안전성학회 2017 한국식품위생안전성학회지 Vol.32 No.2
A rapid, sensitive analytical method for glucuronolactone in beverages was developed and validated using hydrophilic interaction liquid chromatography coupled to electrospray ionization tandem mass spectrometry (HILIC-ESI-MS/MS). To determine the optimum analytical conditions for glucuronolactone, three different kinds of HILIC columns and two mobile phases with different pH values were examined. An amide-bonded stationary phase with a pH 9 acetonitrile-rich mobile phase was the best condition in terms of column retention, ESI-MS/MS response area, and signal-to-noise ratio. After extraction, glucuronolactone was separated through the HILIC amide column and detected by negative ESI-MS/MS in selected reaction monitoring (SRM) mode. Nine energy drinks sold in Korea were spiked with glucuronolactone at a concentration of 5 ng/mL; the Monster EnergyTM sample showed the smallest peak area and its signal-to-noise ratio was used for method validation. Good linearity was obtained in the concentration range from 20 to 1500 ng/mL with a correlation coefficient > 0.998. The developed method had a limit of detection (LOD) of 6 ng/mL and a limit of quantitation (LOQ) of 20 ng/mL. The recovery of this method at concentration of 20, 100, 500, and 1000 ng/mL was 96.3%-99.2% with relative standard deviations (RSD) of 1.6%- 14.0%. A reproducibility precision assessment at concentration of 100 and 500 ng/mL was carried out among three laboratories. The recovery of that evaluation was 95.1%-102.3% with RSD of 2.7%-7.0%. An analysis of variance indicated that there was no difference between the recovery results of the three laboratories at the 5% significance level. The validated method is applicable to inspecting beverages adulterated with glucuronolactone in Korea.
박영민 ( Youngmin Park ),임무성 ( Musung Lim ),이성석 ( Sungseok Lee ),이연우 ( Yeonwoo Lee ),김경호 ( Kyung-ho Kim ) 한국정보처리학회 2009 한국정보처리학회 학술대회논문집 Vol.16 No.1
본 논문에서는 해상무선통신시스템(Maritime Wireless Communication System)을 이용하여 Simulator를 구현하는 방식에 관해서 연구 하였다. VHF, CDMA, WiBro와 같이 3가지 무선통신 방식들에 대해서 해상 무선통신에 적용가능한지를 분석하고, Matlab의 GUI를 사용하여 구현된 해상무선통신방식 시뮬레이터를 바탕으로 해상무선통신 채널환경에서 무선통신방신에 대한 성능을 검증하는 시뮬레이션 프레임워크를 제시하였다. 현재까지 기본적으로 CDMA방식으로 무선통신방식 시뮬레이터를 구축하고, 추후 OFDM기반의 WiBro 전송방식에 대해서도 추가로 시뮬레이터를 설계하여 성능을 검증해 보겠다.