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HPLC를 이용한 Isoproturon, Phenmedipham, Pyridate 및 Nitenpyram 4종 성분의 잔류농약 분석법 개발
양성용(Sung-Yong Yang),구윤창(Yun-Chang Koo),Zeng Wang,허경(Kyeong Heo),김형국(Hyeongkook Kim),안은미(Eun-Mi An),신한승(Han-Seung Shin),이진원(Jin-Won Lee),이광원(Kwang-Won Lee) 한국식품영양과학회 2010 한국식품영양과학회지 Vol.39 No.8
Bis-carbamate계(phenmedipham), urea계(isoproturon), thiocarbamate계(pyridate) 및 vinyllidenediamine계(nitenlyram) 4종의 농약을 HPLC를 이용하여 분석하는 방법을 개발하였다. 사용된 칼럼은 C-18(250 ㎜×4.6 ㎜, 5 ㎛ diameter particle size)이며 isoproturon, phenmedipham은 acetonitrile과 물을 50:50으로 섞어서 사용하였으며, pyridate는 acetonitrile과 물을 85:15로, nitenpyram은 phosphoric acid를 이용하여 pH 2.5로 맞춘 50 mM KH₂PO₄와 acetonitrile을 90:10으로 섞어 유속 1 mL/min의 isocratic 조건으로 분석하였다. 시료 주입량은 10 μL이며 retention time은 isoproturon 6.12분, phenmedipham 8.63분, pyridate 9.40분, nitenpyram 12.76분, 정량한계는 모두 0.05 ㎎/㎏이었다. 회수율 실험은 쌀, 사과 및 대두에 4종의 농약 표준품을 각각 0.05, 0.1 및 0.5 ㎎/㎏이 되도록 세 가지 농도로 spiking 하였으며, 회수율 및 분석오차는 70.18~118.08% 범위와 10% 이내를 만족하였다. A method for the determination of four pesticide compounds, urea (isoproturon), bis-carbamate (phenmedipham), thiocarbamate (pyridate) and vinyllidenediamine (nitenpyram) were examined and analyzed by HPLC with C-18 column (250 ㎜×4.6 ㎜, 5 ㎛ diameter particle size). Mobile phase consisted of deionized water, acetonitrile and 50 mM KH₂PO₄ (pH 2.5). Isoproturon and phenmedipham analytical condition was isocratic elution of the column with 50% solvent A (acetonitrile) and 50% solvent B (deionized water); pyridate was 85% solvent A (acetonitrile) and 15% solvent B (deionized water) at a flow rate of 1 mL/min; and nitenpyram analytical condition was 90% solvent A (50 mM KH₂PO₄, pH 2.5) and 10% solvent B (acetonitrile) at a flow rate of 1 mL/min. In results, retention times were 6.12, 8.63, 9.40 and 12.76 min for isoproturon, phenmedipham, pyridate and nitenpyram, respectively. All injection volumes were 10 μL and the limit of quantitation was 0.05 ㎎/㎏ for four pesticide compounds, respectively. Recovery rate test was performed with three farm products, rice, apple and soybean. Four pesticide compounds were spiked at concentrations of 0.05, 0.1 and 0.5 ㎎/㎏. The recovery rates were ranged from 70.18% to 118.08% and the standard deviations of all experiments were within 10%.
재고미의 가공처리에 따른 in vitro, in situ 소화율 및 발효성상 평가
양성재,정은상,김한빈,신택순,조병욱,조성근,김병우,서자겸,Yang, Sung-Jae,Jung, Eun-Sang,Kim, Han-Been,Shin, Taek-Soon,Cho, Byung-Wook,Cho, Seong-Keun,Kim, Byeong-Woo,Seo, Ja-Kyeom 한국유기농업학회 2018 韓國有機農業學會誌 Vol.26 No.2
This study was conducted to evaluate the effect of different processing of rice on rumen fermentation in in vitro and in situ experiments. Different processing treatments (extruding, roasting, and steaming) were used in this study and all treatments were ground through a cyclone mill (Foss, Hillerød, Denmark) fitted with a 1 mm screen. Non-treated rice was considered to a control substrate. Then, all treatments were used in in vitro and in situ experiments. Total gas production and dry matter digestibility in control were lower than any other treatment at all incubation times (P<0.01). The lowest ammonia nitrogen ($NH_3-N$) concentration was observed in control among treatments at 6, 12, and 24 h incubation (P<0.01). Extruding had a highest total volatile fatty acids (VFA) concentration at 6, 12 h incubation (P<0.01) and Steaming exhibited a highest total VFA at 24 h (P<0.01). The lowest total VFA concentration was observed in control at 6, 12, and 24 h (P<0.01). In an in situ, The highest value of soluble fraction, degradation rates, effective degradability was observed in extruding (P<0.01). It was considered that feed processing increased dry matter digestibility, total VFA concentration, and decreased pH as well as $NH_3-N$ concentration indicating that processing may increase nutrient degradation of rice in the rumen. 본 연구에서는 재고미의 사료가치 평가를 위해 무처리(Control)를 비롯한 Extruding, Roasting, Steam 처리구들의 영양소 성분분석, in vitro 소화율, in situ 소화율을 분석하였다. In vitro 실험에서 Extruding은 건물 소화율과 gas 발생량이 타 처리구에 비해 상대적으로 높았고, 가장 낮은 pH를 보였으며, 특히 배양 시간 초기에 소화가 신속히 발생하였다. $NH_3-N$ 함량은 배양 6 h 이후에서 Control이 Extruding, Roasting, Steam에 비해 유의적으로 높은 값을 보였고, 이는 가열처리된 단백질의 반추위 미생물의 이용성 저하에 따른 결과로 보이나, 더 정확한 결과를 위해 건물 소화율 분석뿐 아니라 CP 소화율 분석이 필요할 것으로 사료된다. VFA 발생량에서는 Extruding이 다른 처리구들에 비해 배양 6, 12 h에서 유의적으로 높았는데 이는 Extruding 처리구의 분해가 배양 초기에 주로 이어져 발생한 결과로 추정된다. 전분을 발효시키는 박테리아에 의해 높은 비율로 생산되는 propionate 증가 폭에서도 같은 경향을 보였다. In situ 소화율은 in vitro의 소화율과는 다소 차이가 있는 것으로 여겨지나, 이는 실험 방법에 대한 오차로 여겨질 수 있으며, ED(유효분해율)를 통해 in vitro 시험과 소화율의 경향성이 유사한 것을 알 수 있었다. 따라서 본 연구결과를 근거로 상대적으로 적합한 사료가공 처리방법은 무처리, Roasting 및 Steaming인 것으로 보여진다. 또한 무처리(control)의 경우 가공처리에 따른 추가비용 발생이 없으므로 경제적으로 유리할 것으로 판단된다. 재고미가 TMR의 원료로 이용될 수 있다면 국내에서 자급 가능한 사료원료로써 우수한 경제성을 지닐 수 있을 것이다.
양성은 ( Sung Eun Yang ),송태옥 ( Tae Ok Song ) 한국컴퓨터교육학회 2014 한국컴퓨터교육학회 학술발표대회논문집 Vol.18 No.1
본 연구의 목적은 청소년의 인터넷 게임중독과 정서조절 사이에 관련성을 파악하는데 있다. 전문계 고등 학교 220명을 대상으로 연구한 결과, 게임중독 점수에 있어서 남녀사이에는 커다란 차이가 있다는 것을 확인할 수 있었으며, 인터넷 게임중독이 청소년의 정서조절에 영향을 미치고 있는 것으로 나타났다.
룸 코너 콘 칼로리미터 시험(ISO 9705)과 비교를 통한 FDS 열분해 모델의 신뢰성 분석
양성진(Sung-Jin Yang),이창덕(Chang-Deok Lee),오지은(Ji-Eun Oh),강찬용(Chan-Yong Kang),김학범(Hag-Beom Kim),이덕희(Duck-Hee Lee) 한국철도학회 2011 한국철도학회 학술발표대회논문집 Vol.2011 No.5
Actual fire test under a laboratory and fire simulation by using computer are considered into main methodology in order to estimate and predict fire size of railway train. Even if practical fire size could be obtained from the full-model railway car test such as a large scale cone- calorimeter test, it is not always possible and realistic due to that expensive cost and attendant dangers could in no way be negligible. In this point of view, fire simulation analysis method based on the computational fluid dynamics could be proposed as an alternative and it seems to be also efficient and reasonable. However, simulation results have to be verified and validated in accordance with the proper procedure including comparing analysis with the actual fire test. In this paper, fire load and growth aspect was investigated through the room corner test (ISO 9705) for the mock-up model of the actual railway car. Then, it was compared with the output data derived from the simulation by using Pyrolysis Model of the FDS (Fire Dynamics Simulator, by NIST) for the exact same domain and condition corresponding with pre-performed room-corner test. This preliminary verified and validated fire modeling method could enhance the reliability of output data derived from the fire simulation under the similar domain and condition.
공감과 사회적 평가가 아동의 친사회적 행동에 미치는 영향
양성은(Sung Eun Yang),정문자(Moon Ja Chung) 한국아동학회 1995 아동학회지 Vol.16 No.2
The purpose of this study was to investigate the effect of selected internal and situational factors on children`s prosocial behaviors. While child`s sex and trait empathy were chosen as internal factors, state empathy and social evaluation were regarded as situational factors. The subjects were 72 bays and 72 girls chosen from 288 eleven-year-olds. This selection was based on their emplathic scores measured by the Bryant Empathy Scale (1982). Half of the 144 children belonged to the high-trait empathic group and the other half to the low-trait empathic group. Within each of the high-and the low-trait empathic groups, equal numbers of boys and girls were randomly assigned to one of the two state empathy conditions and two social evaluation conditions. The state empathy conditions were divided into the arousal condition and the disregarding condition. To control social evaluation, subjects were led to believe that the experimenter either would or would not evaluate their donation of colorful ball-point pens to handicapped children. The data was analyzed by 4-way ANOVA (sex(2)×trait empathy(2)×state empathy(2)×social evaluation(2)). The results were that (1) children`s prosocial behaviors were significantly different by sex, state empathy, and social evaluation, and (2) children`s prosocial behaviors were not significantly different by their trait empathy level.