상아질 접착제를 사용한 광중합 복합레진과 Glass lonomer Cement의 전단 결합력에 관한 연구

이제호,이종갑,권병렬,최형준 大韓小兒齒科學會 1996 大韓小兒齒科學會誌 Vol.23 No.2

The purpose of this study was to compare shear bond strength of composite resin using several dentin bonding agents and light cured glass ionomer cement(Fuji Ⅱ LC). 40 Bovine primary anterior teeth were used for this experiment.Labial surface of teeth were flattened.It were divided into four groups.Each group was composed of 10 teeth.The material used for this experiment were Scotchbond Multipurpose-Z-100,Allbond 2-Aelitefil,Gluma-Pekalux,light and cured glass ionomer cement(Fuji Ⅱ LC). Each of the materials was applied to the exposed surface of 10 teeth by insertion into a cylindrical shaped matrix which is 3mm diamiter and 3mm in height. The completed specimens were stored at 37℃ under 100% humidity for 24 hours:the shear bond strength of material to detin surface were measured with INSTRON universal testing machine. The results were as follows: 1.Shear bond strength to detin surface increased in oder of light cured glass ionomer cement(Fuji Ⅱ LC),Gluma,Allbond 2,Scotchbond Multipurpose. 2.Between shear bond strength of light cured glass ionomer cement(Fuji Ⅱ LC) and Allbond 2,there was statistical significace(P<0.05). 3.Between shear bond strength of light cured glass ionomer cement(Fuji Ⅱ LC) and Scotchbond Multipurpose,between shear bond strength of Gluma and Scotchbond Multipurpose,there was statistical significace(P<0.01). The shear bond strength of detin bonding agents were higher than light cured glass ionomer cement.The reason is that material and quality of detin bonding agent were enhanced.Further investigation is necessary to improve shear bond strength of light cured glass ionomer cement.

졸 - 겔법에 의한 다공성 알루미나 미분체 제조에 관한 연구 : 2 . 물과 알콕시드의 비가 알루미나 미분체의 결정화 공정에 미치는 영향 2 . The Effect of [ H2O ] / [ Al - alkoxide ]on The Crystallization Mechanism of As - Prepared Particles

이성원,박형상,윤호성,황운연,구기갑,유승준,김용렬,이정운 한국화학공학회 2001 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.39 No.2

알루미늄 알콕시드의 반응속도를 제어하기 위한 혼합용매와 입자제조 과정에서의 응집을 방지하기 위한 분산제로 HPC를 첨가하는 방법에 의하여 구형의 다공성 알루미나 미분체를 제조하였으며, XRD, FT-IR 및 TG-DTA 분석을 통하여 공정변수로 선정한 물과 알루미늄 알콕시드의 비가 제조된 미분체의 결정화 공정에 미치는 영향에 대하여 고찰하였다. 축중합 반응에 첨가된 물과 Al-알콕시드의 비는 제조된 미분체 및 하소 공정을 거친 미분체의 결정구조에 영향을 미침을 알 수 있었다. [H₂O]/[ASB]의 비가 증가할수록 제조된 미분체는 비정질의 Al(OH)₃로부터 점진적으로 AlO(OH)의 화학조성을 갖는 의사-보헤마이트로 결정성이 바뀌었다. 그리고 건조 공정을 거친 미분체의 결정성이 좋을수록 δ와 θ-Al₂O₃는 저온에서 생성되었으나, α-Al₂O₃는 고온에서 생성되었다. 이와 같은 결과는 Al^(3+)이온의 결정 내에서의 배위체 변화와 관계됨을 알 수 있었다. 그리고 [H₂O]/[ASB]=2의 조건에서 제조된 입자는 다른 시료와 달리 600℃에서 η-Al₂O₃로 1,100℃에서 α-Al₂O₃2로 상전이 되었다. Spherical porous alumina particles were prepared by mixed solvent to control the reaction rate of Al-alkoxide and the particle shape with hydroxy-propyl cellulose(HPC). HPC was used as a dispersant to prevent aggregation during the formation of particles. The effect of [H₂O]/[ASB] ratio on the crystallization reactions of as-prepared particles was studied by XRD, FT-IR, and TG-DTA analysis. The mole ratio of water and Al-alkoxide added in the condensation reaction had an important effect on the crystal structure of as-prepared particles and the calcined particles. As the [H₂O]/[ASB] ratio increase, the crystal structure of as-prepared particles was continuously varied from amorphous Al(OH)₃ to pseudo-boehmite with chemical composition of AIO(OH). The samples which have higher crystallinite after drying process were transformed into the δ- and θ-Al₂O₃ at lower calcination temperature, but these sample were transformed into α-Al₂O₃ at higher calcination temperature. This result was thought to be the transformation of the coordination number of Al^(3+) ion in the crystal structure. The particles prepared by [H₂O]/[ASB]=2 condition crystallized to α-Al₂O₃at 600℃ and converted to η-Al₂O₃at 1,100℃ without intermediate phases.

정보화사회의 삶의 질 향상과 여가현상에 대한 연구

이진,김형렬 한국스포츠리서치 2003 한국 스포츠 리서치 Vol.20 No.1

A sound physical activity experience designed to enhance knowledge of the body and its potential for movement will develop healthy long-term physical activity attitudes. The purpose of the study, as reviewed in literature, is to define the importance of leisure industry and leisure education for enhancing quality of life under the society environments orienting the informatial society. More details, to reconsider relationship among leisure industry, leisure education and informatioal society, we studied etmosphere between leisure industry and informatioal society, between leisure education and informational society, and between leisure industry and informational society.

PVD 방법에 의한 TiN barrier metal 형성과 공정개발

염병렬,박형호,최치규,이종덕,김건호,이정용,서경수,강민성 濟州大學校 基礎科學硏究所 1997 基礎科學硏究 Vol.10 No.2

Ar과 N₂?가스가 혼합된 분위기에서 반응성 스퍼터링 방법에 의하여 TiN 박막을 증착하였다. N₂ 가스의 농도는 화학양론적으로 TiN이 형성되는 조건에 맞도록 조절하였으며, 기판의 온도는 실온에서 부터 700℃의 범위내로 유지하였다. (111) texture 구조를 가지면서 화학양론적으로 Ti??N??인 박막은 기판의 온도가 600℃ 이상에서 형성되었고, 기판의 온도가 600℃ 이하에서는 형성된 박막은 N-과다형이었다. XRD, XPS 및 RBS 분석 결과 TiN 박막의 조성비는 기판의 온도에서 다소 의존하였으나 약 5% 이내에 불과하였다. TiN 박막의 면저항은 기판온도의 증가에 따라 감소하였고, 기판온도가 600℃에서 증착된 TiN 박막의 면저항능 14.5Ω/□ 였고, Ar―가스 분위기에서 700℃로 30초간 열처리한 후는 8.9Ω/□ 이었다. 따라서 반응성 스퍼터링방법에 의하여 형성되는 양질의 TiN 박막은 기판온도가 600℃이상이 최적조건임을 알았다. Titanium nitride (TiN) films were prepared by reactive sputter deposition in mixed gas of Ar+N₂?. The volume percentage of N₂ in the working gas was chosen so as to grow stoichiometric TiN films and the substrate temperature during film growth was set from room temperature to 700℃. stoichiometric Ti??N?? films with (111) texture were grown at temperatures over 600℃, while films prepared at temperatures below 600℃ showed N-rich TiN. The composition x and y in the Ti??N?? films determined by XPS and RBS varied within 5% with the substrate temperature. The sheet resisstance of the TiN films decreases as the substrate temperature increased. TiN film prepared at 600℃ showed 14.5Ω/□, and it decreased to 8.9Ω/□ after the sample was annealed at 700℃, 30 sec in Ar-gas ambient by RTA. By far, high quality stoichiometric TiN films by reactive sputtering in the mixed gas ambient could be prepared at substrate temperature over 600℃.

중온형 고체전해질 연료전지용 전해질 개발

임형렬,이주성,정순기 한양대학교 에너지 ·환경기술연구소 1995 에너지·環境技術論文集 Vol.2 No.-

고체전해질형 연료전지의 작동온도를 낮추기 위해 고체전해질인 ??를 고상반응법으로 제조하여 그 전기화학적 특성을 살펴보았으며 소결온도 및 첨가제 함량이 이온전도도에 미치는 영향에 대해서도 고찰하였다. 1500℃에서 10시간동안 소결한 ??의 경우 Yb₂O₃의 함량이 ZrO₂에 대해 8㏖%일 때 가장 뛰어난 특성을 보여 890℃, 공기 중에서 ??의 이온전도도를 나타내었다. ?? were prepared by solid state reaction and its electrochemical characteristics were investigated to lower the operating temperature of solid oxide fuel cell. Also the effects of sintering temperature and additive content on ionic conductivity were studied. In case of ?? sintered at 1500℃ for 10hr, the best characteristics were showed when x is 0.08 and the value was ?? at 890℃ in air.

혼합용매법에 의한 Mullite 전미분체 생성기구에 관한 연구

황운연,이정운,박형상,김용렬,구기갑 한국화학공학회 2003 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.41 No.4

Si-와 Al-알콕시드의 반응속도 차이를 조절하기 위한 부분 가수분해법과 입자 형태를 제조하기 위한 혼합용매법을 이용하여 구형의 미세한 mullite 전미분체를 제조하였다. Mie 이론을 적용시켜 반응시간에 따른 반응용액의 탁도 및 입자 수밀도의 변화를 측정하여 혼합용매법에 의한 입자 생성기구에 대하여 고찰하였다. 알콕시드와 옥탄올 용액에 아세토니트릴을 첨가하면 알콕시드의 용해도가 낮아지고 따라서 알콕시드의 일부가 액적을 형성하며, 액적은 안정화제 (HPC)에 의하여 구형을 유지하게 된다. 그리고 가수분해 및 축합중합 반응에 의하여 액적의 입자 크기는 감소하며, 동시에 혼합용액에 용해되어 있던 알콕시의 가수 분해 및 축합중합 반응에 의하여 미세 입자가 생성된다. 액적형태로 생성된 큰 입자와 미세 입자의 응집에 의하여 최종 입자가 생성되었다. In this study, spherical fine pre-mullite particles were prepared by partial hydrolysis method to control the reaction rate difference of two alkoxides, and by mixed solvent method to control the particle shape. Based on the adaptation of Mie theory, the formation mechanism of pre-mullite particle in alkoxide-octanol-acetonitile system has been investigated by measuring of the turbidity of solution, the number density and the size of the particles during the reaction. As the acetonitrile was added in the alkoxide-octanol solution, the solubility of the alkoxide decreased. A part of alkoxide was segregated from solution in the form of droplets. whereas the rest of the alkoxide existed as dissolved state in octanol. The droplets are stabilized with stabilizer (HPC). In the next step. hydrolysis and condensation reactions of the alkoxide droplets decrease the size of droplets and, at the same time, fine particles are formed from the alkoxide dissolved in octanol. Subsequently, the final particles are produced by aggregation between the large particles through the droplet form and the fine particles.

HPLC-MS/MS를 이용하여 혈장 중 레보티인정의 정량분석

채석,오형근,이상선,김형기,손동렬,염윤기,맹주양,권준택 순천향의학연구소 2008 Journal of Soonchunhyang Medical Science Vol.14 No.2

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性別 및 年齡에 따른 體格과 體力의 特性과 變化에 關한 縱斷的 硏究 Ⅰ : 體育專攻 大學生을 中心으로 Emphasised on College Men of Physical Education

金尙國,姜東洹,金昇一,徐再均,金耕知,孫斗玉,鮮于攝,崔榮烈,尹宇相,金亨燉,方永鎭,李錫元 慶熙大學校 體育科學大學 1988 體育科學論叢 Vol.- No.1

The purpose of this study was to compare the characterists and change in physique and physical function by college student of physical education major(287males and 40 females of age groups ranging from 18 to 26). The results were as following; 1) The characteristics of physique and physical function by sex and age. ① The male group of 18yrs old showed higher values in Height, Weight, Upper Limb Length, Strength, Flexibility, and Vital Capacity than any other groups, but female group showed lower values in Height, Weight, Chest Girth, Lower Limb Length, Thigh, Girth, Calf Girth and all of the Physical function. ② The male group of 19yrs old showed high values in power and Agility, then female group showed in Strength and Flexibility. ③ The male group of 20yrs old showed the lower values in Weight, Waist Girth, Upper Limb Length, Fore Arm Girth, Thigh Girh.Calf Girth, Vital Capacity, and female group are very lowed in Upper Arm Lenght, Fore Arm Length, Skin Fold Thickness and 5 minute Run. ④ The male group of 23yrs old showed the high values in Upper Arm Girth, Fore Arm Girth and Balance, and then female group higher in Weight, Chest Girth, Waist Girth, Upper Arm Girth, Fore Arm Girth, Thigh Girth, Power, Shuttle Run, Balance and vital capacity than any other age Groups. ⑤ In male group, Chest Girth, and Blood Pressure were significantly related, and Side Step and Trunk Extension were nagatively related to the age at 0.1% level, and then in female group, Sargent Jump, Standing Long Jump and Vital Capacity were showed a significantly related at 0.5% level. 2) The difference of physique and physical function between male and female by age. ① Everage difference in whole physique items except skinfold thickness was 9.8%, and that 21.1% in all of physical function except Trunk Flextion between male and female group subjects. ② About the ages, the 18yrs old male group showed the 22.8% higher values of 26 items, but 22yrs old male group were about 12.2% in 23 items, thus it is very lower than any other groups. 3) The difference of physique and physical function between General group and physical education group in age-matched. ① In the physique male physical education groups showed about 7% higher in Weight, Chest Girth, Upper Limb Length, Upper Arm Girth, Thigh Girth, and female group showed about 7% higher in Weight and Upper Limb Length. ② In the physical function, Trunk Flextion, 5 minute Run, and Blood Pressure(Diastolic) were about 8% high values in whole group, and female group showed about 8% higher in Standing Long Jump, Shuttle Run, and Trunk Extension. ③ In 22yrs old male and female physical education group were very dominated in physique and physical function than the other age group against the general group.

Free Paper Session : Biliary Diseases ; Endoscopic Balloon Dilatation For The Treatment Of Recurrent Choledocholithiasis In Patients With Previous Sphincterotomy

( Jun Young Lee ),( Jong Ryul Eun ),( Byung Ik Jang ),( Tae Nyeun Kim ),( Heon Ju Lee ),( Sung Bum Kim ),( Hee Jung Moon ),( Sang Hoon Lee ),( Kyeong Ok Kim ),( Kyu Hyung Lee ),( Si Hyung Lee ),( Jae 대한소화기학회 2007 SIDDS Vol.9 No.-

Background/Aims: Endoscopic sphincterotomy (EST) is an established method for the treatment of cholangiopancreatic disease and most commonly performed to remove bile duct stones. However, post-EST complications such as pancreatitis, bleeding, perforation or cholangitis occur in 5 to 10 percent of patients. Especially in previous EST state, additional EST may increase the risk of bleeding and perforation. Endoscopic papillary balloon dilatation (EPBD) appears to offer advantages over EST in minimizing hemorrhage and perforation. This study was designed to evaluate the therapeutic outcome and complications of EPBD in patients with recurrent CBD stones who underwent EST previously for the treatment of CBD stones. Methods: Between January 2006 and April 2007, 20 patients with recurrent CBD stones who had a history of EST due to previous CBD stones were studied retrospectively. All patients underwent EPBD without additional EST for the removal of CBD stones. The size of balloon for papillary dilatation was 12-18 mm according to the size of CBD stones and the duration of dilatation was 60 seconds. We analyzed the therapeutic outcomes and complication associated with EPBD. Results: 16 patients were men and 4 patients were women. The mean age was 68.4±12.5 years. Of the 20 patients, 6 patients had periampullary diverticulum and 2 had underlying liver cirrhosis. The interval between EPBD and previous EST was 30.3±36.6 months. 12 patients had a single stone and 8 had multiple CBD stones. The size of the stone was 13.8±7 mm CBD stones were successfully removed by EPBD without stone fragmentation in all patients. No pancreatitis, bleeding, perforation or cholangitis associated with EPBD occurred. Conclusions: EPBD is a useful and safe method of the treatment for the removal of recurrent CBD stones in patients with previous EST state.

허혈성 대장염에서 심초음파의 임상적 유용성

이규형 ( Kyu Hyung Lee ),장병익 ( Byung Ik Jang ),김경옥 ( Kyeong Ok Kim ),이시형 ( Si Hyung Lee ),최재원 ( Jae Won Choi ),박윤선 ( Youn Sun Park ),이상훈 ( Sang Hoon Lee ),이준영 ( Jun Young Lee ),은종렬 ( Jong Ryul Eun ),김태년 대한장연구학회 2007 Intestinal Research Vol.5 No.2

Background/Aims: Ischemic colitis is recognized as the most common intestinal vascular disorder, especially in the elderly. Several predisposing factors, especially a cardiac embolism, have been reported for ischemic colitis. The aims of this study were to evaluate the prevalence of cardiovascular disease and the role of echocardiography in ischemic colitis. Methods: Thirty-six patients with ischemic colitis from January 2000 to February 2007 were analyzed retrospectively. Results: The mean age of subjects was 68.8±8.4 years. The prevalence of cardiovascular disease in ischemic colitis patients was 33% (12/36 cases). There were eight ischemic heart disease cases, four valvular heart disease cases, three arrhythmia cases and one hypertrophic cardiomyopathy case. Echocardiography was performed in 21 cases; cardiovascular disease could be detected in 11/12 cases (92%) and four cases were previously unknown. Anticoagulant therapy was required in 25% of the patients. Factors influencing hospital stay were the presence of cardiovascular disease. The presence of an associated medical illness did not influence hospital stay. Conclusions: Echocardiography may be useful to evaluate predisposing factors and to determine the use of anticoagulation therapy in ischemic colitis. (Intest Res 2007;5:165-169)