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- 저자 : 장수경(Chang, SooKyung) (검색결과 68 건)
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EPOXY RESIN의 정확도와 인상재와의 친화성에 관한 연구
장수경,장익태,임순호,Chang, Su-Kyoung,Chang, Ik-Tae,Yim, Soon-Ho 대한치과보철학회 1999 대한치과보철학회지 Vol.37 No.3
The indirect technique for making cast restoration requires that dies be as accurate and durable as possible. Currently, stone is the most commonly used material for die. However, it has some problems such as the weakness in its strength and low abrasion resistance. Recently, epoxy resin die systems have become available. The purpose of this study was to examine two commercially available resin die systems and evaluate some characteristics for their clinical performance. This study evaluated the dimensional accuracy of epoxy resins and their wettability with impression materials. In this study, the first experiment was about dimensional accuracy of different die materials. The master model was made of stainless steel. 10 models were made of two epoxy resins (Die-epoxy, Tri-epoxy) and a die stone (Fujirock) each. Occlusal diameter (Dimension I), occluso-gingival height (Dimension II), and interabutment distance (Dimension III) were measured in each model. Next, the contact angles of die materials with impression materials were observed. The blocks were made of polyether, hydrophilic additional silicone, polysulfide impression materials. By drop-ping the same amount (0.05ml) of Tri-epoxy, Die-epoxy, and die stone on the blocks, 10 samples of each die material were made. After setting of materials, the contact angles were measured. The results of this study were as follows. 1. The expansion of stone die and the shrinkage of resin dies in occlusal diameter were observed, and stone and Tri-epoxy were expanded and Die-epoxy was shrinked in occluso-gingival height. There was little change among materials in interabutment distance (p<0.05). 2. In comparison with the master model Tri-epoxy had the least variation in measurement of the three die systems examined. Die-epoxy was next, and die stone showed the greatest variation. 3. The compatibility of die stone for polyether, hydrophilic additional silicone, polysulfide decreased in order, wherease epoxy materials had the decreased compatibility for polyether and polysulnde, hydrophilic additional silicone in order. It was not statistically different between polyether and polysulfide (p<0.05). 4. The contact angles of Tri-epoxy, Die-epoxy, die stone were getting bigger in order.
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은행잎 중 Biflavone의 계절별 함량 변화에 관한 연구
장수경,염정록,강삼식,Chang, Soo-Kyung,Youm, Jeong-Rok,Kang, Sam- Sik 한국생약학회 1993 생약학회지 Vol.24 No.1
The seasonal variations of five biflavones from Ginkgo biloba leaves from May to November were investigated by a reversed phase HPLC method. The total amount of biflavones was increased with time to reach its maximum in yellow autumnal leaves. Each biflavone showed a similar tendency. It increased rapidly about 3.1-fold from May to June and thereafter gradually increased about 2.5-fold. The ratio of each biflavone content to the total amount of biflavones was in the order of as follows: isoginkgetin>sciadopitysin>bilobetin>ginkgetin>amentoflavone.
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약산 전처리 조건에 따른 소경 신갈나무 유래 푸르푸랄 및 레불린산의 함량 변화
장수경 ( Soo Kyeong Jang ),정한섭 ( Han Seob Jeong ),홍창영 ( Chang Young Hong ),김호용 ( Ho Yong Kim ),류가희 ( Ga Hee Ryu ),여환명 ( Hwanmyeong Yeo ),최준원 ( Joon Won Choi ),최인규 ( In Gyu Choi ) 한국목재공학회 2015 목재공학 Vol.43 No.6
본 연구에서는 국산 소경 신갈나무를 이용하여 약산 전처리를 실시하고, 당으로부터 변환된 푸르푸랄 및 레불린산의 함량 변화를 평가하였다. 약산 전처리는 반응온도(140-180℃), 반응시간(10-30분), 황산 촉매 농도(0-2%, w/w)에 따라 수행하였고, 전처리 후 액상 내 글루코오스, XMG (자일로오스 + 만노오스 + 갈락토오스), 푸르푸랄, 레불린산의 함량을 측정/분석하였다. 글루코오스는 반응온도의 상승, 반응시간과 황산 촉매 농도의 증가에 의해 그 함량이 높아져최대 16.02%까지 나타났으나, 황산 촉매 농도 2% (반응온도 170℃ 이상, 반응시간 20분 이상)에서 함량이 감소하였다. 한편, XMG 함량은 반응온도의 영향을 크게 받았고, 반응온도와 황산 촉매 농도의 증가에 따라 1.63%까지 감소하였으며, 반응시간의 증가에 의한 함량변화는 적었다. 푸르푸랄 함량은 반응온도, 반응시간, 황산 촉매 농도 증가에 따라 높아져 초기시료 중량 대비 최대 7.61% (반응온도 180℃, 반응시간 20분, 1% 황산 촉매 농도)로 나타났으나, 전처리 조건이 최대 푸르푸랄 함량 조건보다 가혹해지면서 감소하는 경향이 발생하였다. 레불린산 함량은 반응온도, 반응시간, 황산 촉매 농도가 증가함에 따라 높아졌고, 특히 반응온도 170℃ 이상에서 급격한 함량 증가를 확인하였으며, 최대 10.98% (반응온도 180℃, 반응시간 30분, 2% 황산 촉매 농도)로 나타났다. 반면 황산 촉매를 투입하지 않았을 경우 모든 반응온도, 반응시간 조건에서 푸르푸랄 및 레불린산 함량은 1% 미만으로 나타났다. In this study, dilute acid pretreatment was operated using small-diameter Quercus mongolica for evaluating the yield change of furfural and levulinic acid depending on pretreatment factors. The dilute acid pretreatment was conducted depending on reaction temperature (140-180℃), reaction time (10-30 min), and sulfuric acid concentration (0-2%, w/w). Then, glucose, XMG (xylose + mannose + galactose), furfural, and levulinic acid contents in the liquid hydrolyzate were measured and analyzed after pretreatment. Glucose content increased to 16.02% as reaction temperature, reaction time, and sulfuric acid concentration increased, but it decreased at the sulfuric acid concentration of 2% (reaction temperature: > 170℃, reaction time: > 20 min). On the other hand, reaction temperature had a strong influenced on XMG content, and XMG content decreased to 1.63% through increasing of reaction temperature and sulfuric acid concentration, but XMG content was less affected by changes of reaction time. Furfural content increased with the increase of reaction temperature, reaction time, and sulfuric acid concentration, and maximum furfural content was 7.61% (reaction temperature: 180℃, reaction time: 20 min, sulfuric acid concentration: 1%) based on a weight of raw material, while furfural content was dropped in more severe condition than in maximum furfural content condition. Levulinic acid content also increased with higher reaction temperature, reaction time, and sulfuric acid concentration. Especially, the sharp increase of levulinic acid content was observed above 170℃, and maximum levulinic acid content was 10.98% (reaction temperature: 180℃, reaction time: 30 min, sulfuric acid concentration: 2%). However, less than 1% of furfural and levulinic acid content was obtained in non-acidic catalyst condition that in whole conditions of reaction temperature and reaction time.
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장수경(Su-Kyung Chang),이현희(Hyun-Hee Lee),홍석인(Seok-In Hong),한영숙(Young-Sook Han) 한국식품과학회 2010 한국식품과학회지 Vol.42 No.2
메밀 새싹의 유통 중 품질유지를 목적으로 유기산 용액과 염소수에 침지한 후 플라스틱 필름봉투에 밀봉하여 5℃에 저장하면서 여러 가지 품질인자의 변화를 살펴보았다. 미생물학적 측면에서 총균수와 대장균군수의 측정 결과 0.5% citric acid, 0.05% acetic acid의 단독 및 병용처리가 다른 처리구에 비해 미생물 증식제어에 효과적이었다. 수분함량이나 가용성 고형분함량의 경우 6일 저장 중 의미 있는 변화를 관찰할 수 없었다. 색 변화에서도 Hunter L값과 Hunter b값은 처리구별로 유의적인 차이를 보이지 않았으나, Hunter a값의 경우 저장기간이 경과함에 따라 ascorbic acid 및 citric acid 처리구의 변화가 가장 적게 나타났다. 관능평가에 있어서도 저장 중 ascorbic acid 및 citric acid 처리구가 다른 것에 비해 변색, 시듦, 종합적 외관품질 항목 모두에서 유의적으로 구분되어 관능적 품질이 우수한 것으로 평가되었다. 결과적으로 본 연구에서 사용한 유기산 가운데 citric acid를 전처리 침지용액으로 적용할 경우 메밀 새싹의 유통 중 품질유지에 매우 긍정적인 효과가 있음을 확인하였다. Changes in the quality of buckwheat sprout treated with organic acid solutions such as ascorbic, citric and acetic acid were examined during storage in order to judge the feasibility of acid dipping as a pretreatment for extending shelf-life. Quality attributes of buckwheat sprout stored at 5℃ were measured in terms of microbial cell count, moisture content, soluble solids content, chromaticity, and sensory evaluation over different storage times. For microbial growth inhibition, combinations of 0.05% acetic acid and 0.5% citric acid or 1% ascorbic acid and 0.5% citric acid were more effective than other treatments. Slight changes were observed in moisture content among the treatments, whereas soluble solids content of each treatment was increased during storage. In chromaticity, the Hunter‘s a value of buckwheat sprout treated with acetic acid alone or acetic acid combinations showed the largest increase. Dipping treatment with ascorbic acid and citric acid produced only slight changes in color of the sprout. In the sensory evaluation of discoloration (head, stem and root), wilting and overall quality, ascorbic acid and citric acid treatments gave the highest scores. These results suggest that dipping treatment of buckwheat sprout with citric acid can confer more positive effects on storage stability than others.
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승마기구에서 골반자세와 속도가 몸통 및 다리 근 활성에 미치는 영향
김정현,장수경,Kim, Jung-Hyun,Chang, Soo-Kyung 대한물리치료학회 2014 대한물리치료학회지 Vol.26 No.5
Purpose: The purpose of this study was to assess the effects of robo-horseback riding with changes of pelvic tilting and speeds on muscle activities of trunk and lower limb in healthy adults. Methods: Thirty healthy adults were recruited for this study. Subjects performed robo-horseback riding at three pelvic postures (anterior tilting pelvic posture: AP, neutral pelvic posture: NP, posterior pelvic posture: PP) and different speeds (moderate and fast speed). Muscle activities were recorded from the trunk muscles (rectus abdominis [RA], T2 paraspinalis [T2 PS], L2 paraspinalis [L2 PS]) and lower limb muscles (rectus femoris [RF], vastus medialis [VM], vastus lateralis [VL], biceps femoris [BF], gastrucnemius [GCM]). Results: Significantly higher RA activities were observed under the PP condition than under the AP and NP conditions at both speeds. Significantly higher L2 PS activities were observed under the AP condition than under the PP and NP conditions at both speeds. Significantly higher T2 PS activities were observed under the AP condition than under the PP and NP conditions at fast speed. However, the muscle activities of the VM and GCM did not show significant changes with changes in pelvic posture at both speeds. All muscle activities were significantly higher under the fast speed than under the moderate speed in three pelvic postures. Conclusion: There were significant differences in the changes of pelvic tilting on muscle activities of trunk and lower limb were observed in healthy adults. NP condition can be introduced the most efficienct posture for muscle activities of trunk and lower limb in robo-horseback riding.
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