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졸-겔 공정에 의한 YMnO<sub>3</sub> 박막의 전기적 특성
김응수,김병규,김유택,Kim, Eung-Soo,Kim, Beng-Gu,Kim, Yoo-Taek 한국세라믹학회 2002 한국세라믹학회지 Vol.39 No.5
$Y(NO_3)_3{\cdot}5H_2O$ 과 $Mn(CH_3CO_2)_2{\cdot}4H_2O$를 출발물질로 하여 졸-겔(sol-gel)법으로 Si(100) 기판위에 육방정계의 $YMnO_3$ 박막을 제조하였다. $YMnO_3$ 박막의 열처리 온도변화, 가수분해시 가수의 양(Rw)과 촉매제의 첨가에 따른 결정 구조 및 전기적 특성을 조사하였다. $YMnO_3$ 박막의 결정화는 700${\circ}C$부터 시작되었고 완전한 결정화는 800${\circ}C$-1시간 열처리하여 이루어 졌으며, $YMnO_3$ 박막의 가수의 양 Rw=6일때 육방정계 $YMnO_3$상의 c-축 (0001) 우선 배향성을 나타내었고, Rw=1 과 Rw=12인 경우에는 Rw=6인 경우보다 c-축 배향성은 감소하였다. 산성이나 염기성 촉매제 첨가에 따라 $YMnO_3$ 박막의 결정성 및 우선 배향성은 영향을 받아 c-축 우선 배향성은 감소하고 사방정계의 $YMnO_3$ 상을 형성하였다. Rw=6일 때 $YMnO_3$박막은 0.2V인가 전압에서 $1.2{\times}10-8 A/cm^2$으로 우수한 누설 전류 밀도를 나타내었고 누설 전류 밀도는 인가 전압에 따라 크게 변하지 않았다. Hexagonal $YMnO_3$ thin films were prepared from $Y(NO_3)_3{\cdot}5H_2O$ and $Mn(CH_3CO_2)_2{\cdot}4H_2O$ as starting materials on the Si(100) substrates by the sol-gel method. The crystal structure and the electrical properties of the $YMnO_3$ thin films were investigated as a function of heat treatment temperature, the amount of water(Rw) of hydrolysis and the addition of catalysis. The crystallization of the $YMnO_3$ thin film began at 700${\circ}C$ and completed at 800${\circ}C$ for 1 h. The c-axis (0001) preferred orientation of hexagonal $YMnO_3$ was detected for the $YMnO_3$ thin films with Rw=6 and that was decreased for the $YMnO_3$ thin films with Rw=1 and Rw=12. The crystallinity and preferred orientation of the $YMnO_3$ thin films were depended on the addition of acid and/or alkali catalysis, which, in turn, the preferred orientation of c-axis was decreased and the orthorhombic phase of $YMnO_3$ was detected to the specimens with the addition of catalysis. The $YMnO_3$ thin film with Rw=6 showed good leakage current density of $1.2{\times}10-8 A/cm^2$ at the applied voltage of 0.2V and the leakage current density was not changed drastically with applied voltage.
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김응수,김용현,김준철,방규석,Kim, Eung-Soo,Kim, Yong-Hyun,Kim, Jun-Chul,Bang, Kyu-Seok 한국재료학회 2001 한국재료학회지 Vol.11 No.8
($Pb_{0.2}$$Ca_{0.8}$ )[($Ca_{1}$3$Nb_{2}$3/)$_{1-x}$ $Ti_{x}$ ]O$_{3}$ 세라믹스의 $^{4+}$ 치환량 변화에 따른 마이크로파 유전특성을 고찰하였다. $Ti^{4+}$ 치환량이 증가함에 따라 x=0.05부터 x=0.15까지의 조성범위에서는 단일상의 페롭스카이트상을 얻을 수 있었으며, x=0.2이상에서는 $Ti_2$와 $CaNb_2$$O_{6}$ 가 제 2상으로 존재하였고, 결정구조는 x=0.05에서 사방정(orthorhombic) 구조가 x=0.35에서 이방정(cubic) 구조로 전이하였다. 유전상수(K)는 $Ti^{4+}$ 치환량의 증가에 따라 rattling 효과의 증가로 인하여 증가되었으며, B-자리 양이온의 평균이온반겨의 세제곱의 반비례하였다. 그러나 결정립 크기의 감소와 제 2상의 존재로 인하여 Qf값은 감소하였다. $Ti^{4+}$ 치환량이 증가됨에 따리 tolerance factor(t)와 B-자리 결합원자가의 영향으로 공진주파수의 온도계수(TCF)는 -27.36ppm/$^{\circ}C$값으로부터 +18ppm/$^{\circ}C$r값으로 조절되었다. $1350^{\circ}C$d서 3시간 소결한 ($Pb_{0.2}$ $Ca_{0.8}$ )[(Ca$_{1}$3$Nb_{2}$3)$_{1-x}$ /$Ti_{x}$]$O_{3}$ 시편에서 K=51.67, Qf=7268(GHz), TCF=0 ppm/$^{\circ}C$의 우수한 특성을 얻을 수 있었다. Microwave dielectric properties of $(Pb_{0.2}Ca_{0.8})[(Ca_{1/3}Nb{2/3})_{1-x}Ti_x]O_3$ ceramics were investigated as a function of $Ti^{4+}$ content (0.05$\leq$x$\leq$0.35). A single perovskite phase was obtained from x=0.05 to x=0.15, and $TiO_2$ and $CaNb_2O^6$ were detected as a secondary phase beyond x=0.2. The structure was changed from orthorhombic at x=0.05 to cubic at x=0.35. Dielectric constant(K) was increased with increase of $Ti^{4+}$ content due to increase of rattling effect, and was inversely proportional to the cube of the average radius of B-site cation, however, Qf value was decreased, which was due to the decrease of grain size and the secondary phase. With the increase of $Ti^{4+}$ content, the temperature coefficient of resonant frequency(TCF) was controlled from -27.36 ppm/$^{\circ}C$ value to +18.4 ppm/$^{\circ}C$ value, which was caused by the influence of tolerance factor(t) and the bond valence of B-site. Typically, K of 51.67, Qf of 7268(GHz), TCF of 0 ppm/$^{\circ}C$ were obtained in the $(Pb_{0.2}Ca_{0.8})[(Ca_{1/3}Nb_{2/3})_{0.8}Ti_0.2]O_3$ sintered at 13$50^{\circ}C$ for 3h.
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김응수,Joo Hyeon Kim 대한금속·재료학회 2020 ELECTRONIC MATERIALS LETTERS Vol.16 No.6
Microwave dielectric properties of CaW1−x(Mo1/2Te1/2)xO4 (0.01 ≤ x ≤ 0.17) ceramics with (Mo1/2Te1/2)6+ substitution wereinvestigated. For the specimens sintered at 825–950 °C for 3 h, a single phase of a scheelite structure was observed up tox = 0.13, while secondary phases were detected above x = 0.17. The relative densities of the specimens were higher than 95%,and the grain morphologies were uniform and clean for the entire range of compositions. The quality factor (Qf) dependedon the intrinsic factors such as the W-site bond characteristics of CaWO4evaluated by the bond valence and degree of covalency,and confirmed by the full width at half maximum of the internal mode peak of Raman spectroscopy. However, Qf wasalso affected by the extrinsic factors, such as the formation of the secondary phases, which showed the maximum Qf value(167,800 GHz) at x = 0.13 and then decreased. The dielectric constant (K) increased with (Mo1/2Te1/2)6+ substitution, whichwas affected by the dielectric polarizabilities of constituent ions. As the (Mo1/2Te1/2)6+ content increased, the temperature coefficient of resonant frequency (TCF) decreased, which was associated with an increase of oxygen bond valence.
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증상을 동반한 제 2형 부주상골에서 교량형 봉합술을 이용한 변형 Kidner 술식의 단기 치료 결과
김응수,문진선,Kim, Eungsoo,Moon, Jinseon 대한족부족관절학회 2016 대한족부족관절학회지 Vol.20 No.2
Purpose: The purpose of this study was to evaluate the clinical outcome of a modified Kidner procedure using a suture bridge technique in symptomatic type II accessory navicular. Materials and Methods: Between January 2013 and December 2014, a total of 35 cases with symptomatic type II accessory navicular were treated with a modified Kidner procedure using the suture bridge technique. The patients were evaluated preoperatively, 3 months after surgery, and at the latest follow-up (at least six months postoperatively) clinically via the American Orthopaedic Foot and Ankle Society (AOFAS) midfoot score, visual analogue scale (VAS), and the self-subjective satisfaction score. Results: The mean AOFAS midfoot score demonstrated significant improvement from a mean of 45.3 preoperatively to a mean of 89.2 at 3 months after surgery. At the latest follow-up, the mean AOFAS midfoot score was 92.6 (p<0.001). The mean VAS also improved significantly, decreasing from 6.7 out of 10 preoperatively to 1.8 at 3 months after surgery. At the latest follow-up, the VAS was 1.2 (p<0.001). The mean time of a single-limb heel raise was 4.6 months postoperatively and the self-subjective satisfaction score was 1.4 out of 4 at the latest follow-up. Conclusion: The short-term surgical results of the modified Kidner procedure with a suture bridge technique for symptomatic type II accessory navicular were good to excellent in terms of pain, functional and clinical assessments. In conclusion, the modified Kidner procedure with the suture bridge technique is a reasonable treatment option for symptomatic type II accessory navicular.
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김응수,Kim, Eung-Soo 한국전자통신학회 2013 한국전자통신학회 논문지 Vol.8 No.9
인간의 건강한 생활을 위해서는 자세 및 골격구조가 중요하며, 이것은 평소의 생활습관과 걸음걸이에 의해서 영향을 받아 변형될 수 있다. 인간의 걸음걸이형태로는 크게 바른걸음, 팔자걸음, 안짱걸음으로 구분할 수 있으며, 이러한 걸음걸이형태를 분석하여 바른자세를 유지하는데 도움이 될 수 있다. 본 논문에서는 스트레인 센서를 이용하여 걸음걸이 패턴을 분석하는 신발을 개발하였으며, 제작된 신발로 걸음걸이 패턴을 구분하여 분석할 수 있었다. The human gait pattern analysis shoes have been developed for our healthy lfe, which is largely dependent on a posture and a skeletal structure affected by daily lifestyle and gait pattern. There are generally 3 types of human gait, such as normal gait, intoeing gait, and outtoeing gait. We have analyzed one's gait pattern through walking put on the developed shoes.
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김응수,이상욱,Kim, Eung-Soo,Lee, Sang-Wook 한국정보통신학회 2012 한국정보통신학회논문지 Vol.16 No.3
신경회로망의 동작과 정보처리 능력 등에 관하여 살펴보고자 할 때, 신경회로망의 구성 요소를 어떻게 모델화 할 것인가는 중요한 문제이다. 소자의 응답특성이 바뀜에 따른 특성의 변화, 결합강도 및 적응규칙이 바뀜으로써 회로망 전체의 다이나믹스가 바뀌는 모습, 소자 상호간의 결합 형태에 따른 정보처리 능력의 변화 등과 같은 신경회로망이 가진 다양한 정보처리 능력을 밝히는 것은 병렬 정보처리의 메카니즘을 이해하는 문제와도 일맥상통하고 있다. 따라서 이러한 문제들에 대하여 신경회로망의 정보처리 능력을 해석적으로 평가하는 것은 병렬분산 정보처리의 본질을 밝힌다는 측면에서 중요하게 여겨진다. 따라서 본 논문에서는 신경회로망을 구성하는 구성요소의 변화, 그 가운데에서도 특히 소자의 히스테리시스 특성이 신경망의 계열연상능력에 미치는 영향에 대한 이론적 해석결과에 대하여 기술한다. It is important to understand how we can deal with elements for the modeling of neural networks when we are investigating the dynamical performance and the information processing capabilities. The information processing capabilities of model neural networks will change for different response, synaptic weights or learning rules. Using the statistical neurodynamics method, we evaluate the capabilities of neural networks in order to understand the basic concept of parallel distributed processing. In this paper, we explain the results of theoretical analysis of the effects of the hysteretic property on the performance of sequential associative neural networks.
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