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최대호,김태호,이상양,이수완 선문대학교 ·중소기업기술지원연구소 2002 선문공대 연구/기술 논문집 Vol.7 No.1
먼저 소형 배합기를 사용하여 특정 방식을 가지고 혼합한 후 일정 성형 조건하에서 브레이크 마찰재 시편을 제작한다. 제조된 브레이크 마찰재 시편을 가지고, 정량적인 마모시험기를 통하여 마모계수를 측정하고 그 마모면을 SEM과 광학현미경을 이용하여 관찰하여 마모 기구를 조사하고, 마찰재의 열전도도 측정, 온도에 따른 TGA, DSC 측정, 분석 등 다양한 열적 특성을 분석하여 열 안정성을 평가하였다. By utilizing small mixer we can make brake frictional materials's specimen with special formulas in the condition of constant pressure and forming processes. The frictional coefficients were measured quantitatively with utilizing tribometer (TE77 reciprocating configuration), the worn surfaces were observed by a SEM (scanning electron microscopy), and the wear mechanism will be investigated. The thermal conductivity of the frictional materials was examined, and, TGA (thermal gravitation analysis), and DSC (differencial scanning calorimeter analysis) were used to study thermal properties and to evaluate the thermal stability of the frictional materials). On the bases of results from these experiments, the quantitative characteristics of frictional materials can be obtained.
생체 세라믹스용 마모시험장비의 제작 및 정방정지르코니아의 마모특성
김성호,류득배,문병규,이수완 선문대학교 중소기업기술지원연구소 2001 선문공대 연구/기술 논문집 Vol.6 No.1
생체 세라믹스용 마모시험장비를 제작하였다. 마모시험기는 lever system을 이용하여 하중인가가 되게 설계되었으며 step motor를 사용하여 회전수 조절이 용이하게 하였다. DAQ (Data Acquisition System)을 이용하여 하중을 측정하여 마찰계수를 측정할 수 있게 하였다. 성능평가를 위해 정방정지르코니아를 Ringer's solution에서 선속도 40 mm/s, 인가하중 10, 20, 30 N에서 마모시험 하였다. Grooving, crack networking등의 마모기구가 관찰되었다. A wear testing machine for bioceramics was designed and made, which loading and rotating parts consisted of a lower systemed and a step motor, respectively. Friction coefficient was determined by DAQ(Data Acquisition System). Wear resistance of tetragonal zirconia was measured under linear velocity of 40 mm/sec, applied load of 10, 20, 30 N in Ringer's solution, which showed grooving, crack networking on worn surfaces.
Behavior of residual stress in plasma sprayed ZrO₂ coatings with different contents of LaPO₄
Soo Wohn Lee,Jia Zhang,Huang Chen,Tohru Sekino,Seung Ho Kim 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.6
In this study, ZrO2-LaPO4 composite coatings were deposited by a plasma spraying technique. For nondestructive evaluation and easy practicability, the X-ray diffraction method was chosen to determine the residual stress in plasma sprayed ZrO2- LaPO4 composite coatings. The relationship between residual stress and content of LaPO4 was investigated. In this study, ZrO2-LaPO4 composite coatings were deposited by a plasma spraying technique. For nondestructive evaluation and easy practicability, the X-ray diffraction method was chosen to determine the residual stress in plasma sprayed ZrO2- LaPO4 composite coatings. The relationship between residual stress and content of LaPO4 was investigated.
Gyawali, Gobinda,Lee, Soo Wohn American Scientific Publishers 2016 Journal of nanoscience and nanotechnology Vol.16 No.11
<P>Ag3PO4/MoS2 composite photocatalysts with 1 to 10 wt% of MoS2 have been synthesized by the microwave assisted hydrothermal process. Prepared Ag3PO4/MoS2 composites were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), UV-vis diffuse reflectance spectroscopy (DRS), and X-ray photoelectron spectroscopy (XPS). It was found that the as prepared Ag3PO4 revealed micron-sized particles, whereas Ag3PO4/MoS2 composites have shown a significantly reduced size of Ag3PO4 particles which were found to be deposited on the surface of MoS2. The Ag3PO4/MoS2 composites exhibited enhanced photocatalytic activity for the photocatalytic degradation of methyl orange (MO) under a simulated solar light condition. The photocatalytic reaction rate of Ag3PO4/3 wt% MoS2 composite is found to be the highest among all other samples. Furthermore, the photocatalytic stability of Ag3PO4/3 wt% MoS2 composite is significantly enhanced in comparison to bare Ag(3)PO4 photocatalyst.</P>
Low friction and high strength of 316L stainless steel tubing for biomedical applications
Amanov, Auezhan,Lee, Soo–,Wohn,Pyun, Young–,Sik Elsevier 2017 Materials Science and Engineering C Vol.71 No.-
<P>We propose herein a nondestructive surface modification technique called ultrasonic nanocrystalline surface modification (UNSM) to increase the strength and to improve the tribological performance of 316L stainless steel (SS) tubing. Nanocrystallization along nearly the complete tube thickness of 200 pm was achieved by UNSM technique that was confirmed by electron backscatter diffraction (EBSD). Nano-hardness of the untreated and UNSM-treated specimens was measured using a nanoindentation. Results revealed that a substantial increase in hardness was obtained for the UNSM-treated specimen that may be attributed to the nanocrystallization and refined grains. Stress-straip behavior of the untreated and UNSM-treated specimens was assessed by a 3-point bending test. It was found that the UNSM-treated specimen exhibited a much higher strength than that of the untreated specimen. In addition, the tribological behavior of the untreated and UNSM-treated specimens with an outer diameter (OD) of 1.6 mm and an inner diameter (ID) of 1.2 mm was investigated using a cylinder-on-cylinder (crossed tubes of equal radius) tribo-tester against itself under dry conditions at ambient temperature. The friction coefficient and wear resistance of the UNSM-treated specimen were remarkably improved compared to that of the untreated specimen. The significant increase in hardness after UNSM treatment is responsible for the improved friction coefficient and wear resistance of the tubing. Thus, the UNSM technique was found to be beneficial to improving the mechanical and tribological properties of 316L SS tubing for various potential biomedical applications, in particular for coronary artery stents. (C) 2016 Elsevier B.V. All rights reserved.</P>