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우리 나라 배경농도지역의 1996~1997년 미세입자상 탄소성분 측정 결과
김용표,이종훈,문길주,김희강,이종범 江原大學校 附設 環境硏究所 1999 環境硏究 Vol.16 No.-
The concentrations of organic carbon (OC) and elemental carbon (EC) in fine aerosols were determined from the samples collected at the two background sites of Kosan in Cheju Island and Kangwha. Samplings were carried out during the spring and winter of 1996 and the fall and winter of 1997. PM_(2.5) particles were collected on the pre-fired quartz filters for 24 hours and analyzed by the selective thermal oxidation method. The concentrations of OC at the sites were higher than those commonly observed from clean areas around the world, but those of EC at both sites were lower than, or comparable to, other clean areas in the world. Both the OC and EC levels at Kangwha were higher than those at Kosan. According to backward trajectory analysis, most air pollutants collected at thetwo sites were from China. It was found that the OC and EC concentrations in air masses from southern China were higher than those from northern China.
정종헌,원휘준,최왕규,김계남,이성호,오원진 한국공업화학회 2003 응용화학 Vol.7 No.1
Liquid wastes containing uranium ions in high concentration of chemical salts havebeen treated by electrosorption on a activated carbon fibers(ACFs) electrode. Effectiveuranium (VI) removal is accomplished when the potential is -0.5V(vs. Ag/AgCl) ormore negative. For a feed concentration of 100mg/1, the concentration of U(VI) in thecell effluent is reduced to less than 1mg/1, and electrosorption capacity over 500mg/uranium/gACF is reached. The adsorbed uranium can be desorbed up to 99%for 20h by passing a 1.9N NaCl solution at pH 3 through the cell and applying a potential of +1.2V. The amount of desorbed uranium increased as the solution pHwas lowered and the applied potential increased.
9-11세 정상교합 어린이의 연조직 측모에 관한 두부방사선계측학적 연구
이창희,김정욱,김종철,이상훈 大韓小兒齒科學會 2005 大韓小兒齒科學會誌 Vol.32 No.3
본 연구의 목적은 정상교합인 건치 어린이에서 여러 가지 연조직 측모 분석법을 이용한 평균치를 제시하고 연령별, 성별에 따른 차이를 비교함으로써 이 시기에 행해지는 교정진단과 치료에 유용하게 이용하고자 하는 것이다. 2000년에서 2004년까지 서울시 치과의사회가 주관하는 건치 어린이 선발대회에서 선발된 정상교합인 9-11세 어린이 169명(남자 82명, 여자 87명, 9세 26명, 10세 118명, 11세 25명)을 촬영한 측모 두부규격 방사선사진으로 여러 가지 연조직 측모분석법을 이용하여 연조직 평균치를 구한 후 다음과 같은 결론을 얻었다. 1. 성별에 따른 연조직 평균치는 두 가지 항목을 제외하고는 유의성있는 차이를 보이지 않았다(p>0.05). 2. 여자가 남자보다 H line에 대해 하순이 더 돌출된 위치에 존재했으며, 중안모 길이에 비해 하안모 길이가 짧았다(p<0.05). 3. 연령에 따른 연조직 평균치는 유의성있는 차이를 보이지 않았다(p>0.05). The purpose of this study is to develop soft tissue cephalometric standards in children with normal occlusion and to determine the differences between males and females and the differences according to age ranges of 9, 10 and 11 years. The lateral cephalometric radiographs of 169 children(82 boys, 87 girls) among the contestants in 2000-2004 Healthy Dentition Contest in Seoul were studied with several soft tissue profile analyses and cephalometric means and following results were obtained. 1. The sex differences were not statistically significant between males and females soft tissue parameters except for two soft tissue parameters(p>0.05). 2. Females had relatively more protrusive lower lip relative to the H line than males and middle third face height to lower third face height of females was larger than males(p<0.05). 3. The age differences in soft tissue parameters were not statistically significant according to age ranges of 9, 10 and 11 years(p>0.05).
우리나라 청정지역에서 측정한 PM_(2.5) 입자의 특성
이종훈,김용표,문길주,김희강,정용승,이종범 江原大學校 附設 環境硏究所 1998 環境硏究 Vol.15 No.-
Atmospheric fine particles (PM_(2.5)) were collected at the background sites, Kangwha, Taean, and Kosan and characterized to understand their behaviors at the sites. Daily samples of PM_(2.5) mass were measured and ionic species, carbonaceous species, and gaseous species were analyzed. Four-daγ backward trajectory analysis was also carried out. The mean concentrations of anthropogenic species were highest at Kangwha among three sites, while contributions from sea salts were highest at Taean during the measurement period due to higher wind speed at Taean. Major chemical components in fine particles were sulfates organic carbon, nitrate, and ammonium. Most of the non-sea-salt (nss) sulfates in PM_(2.5) might be present as ammonium sulfates at these sites. Most air parcels arriving at Kangwha and Taean were from northern China. Therefore, both sites were thought to be affected by the same air parcel. At Kosan, during the measurement period, air parcels were from either northern China or southern China. The nss sulfate concentration in the air parcels from southern China was higher, while the nss calcium nitrate, and ammonium concentrations were higher when the air parcels were from northern China.
고용석,강찬순,최보경,김혜수,홍정희,최명신,김상현,장성재,김길수 식품의약품안전청 2001 식품의약품안전청 연보 Vol.5 No.-
Headspace-GC(딘5-GC)를 이용하여 ICH 잔류웅매 가이드라인 class 1, 2에 속하는 28종의 잔류유기웅매 분석방법을 연군한 결과 SPB-5, BB-WAX column을 동시 이용하여 각각을 확인, 정량할 수 있었다.또한 염의 참가효과, 평형시간,평형온도가 headspace분석에 미치는 영향을 검토한 결과 평형 시간 30분,평형온도 85℃,Na₂SO₄Ig을 첨가하여 시험할 때 최적 부넉조건을 나타내었다. 회수율은 1,1-achloroethene(68.3%)를 제외하고 90.9 ~ 114.5%로 패체적으로 양호하였다. 따로 HS-GCJECD, DB-524 column을 이용하여 9종의 잔류유기용매에 대하여 각각의 검랸선을 작성하고 검출한계를 구하였다. 실제 의약품 원료 10종및 제제 5종에 적용시킨 결과 모두 불검출되었으며 본 시험법은 의약품중의 잔류유기용매 분석에 적용할 수 있는 방법이라고 판단된다. The headspace-fC/FID(HS -GC/FID) method was performed for test method developnlent of residu;31 organic solvents in pfrarmaceuticals. Using SPB-S and BB-WAXcolumn, 28 kinds of solvents iri ICH residual sof)·ents guidetine class 1, 2 couBd be individuallt-identified and quantitated. The foIBowing residoal soIYents were not detected by the headspaceinjection condition : N,N-Cmethylacetamide, N,N-dimeth)rlformamide, ethyfeneglycol, formamide,2-methoryethanot, N-rnethylpyrrolidone, suBforane. The effects of the addition of salts,equilibration time, and equilibration temperature on headspace analt·sis were invesugated. Theoptimum conditions weiFe obtained with addtion of Ifa2s04 19 as a salt, simultaneously. thetime and temperature of equitibration were 30min and 8i'f, respectivety. The recovery havefound between 90.9 and 114.5% except 1,1-dichloroethene(fi8.3%). Using DB-624 column &HS-GC/:ECD method, 9 kinds of residual solvents could be individually identified andfuantitated. This HS-GC method can be applied to test the residua3 organic solvent in thepharmaceuticals.