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이재범,김선태,Lee Jaebum,Kim Seontai 한국재료학회 2005 한국재료학회지 Vol.15 No.5
Gallium oxyhydroxide (GaOOH) powders were heat-treated in a flowing ammonia gas to form GaN, and the reaction kinetics of the oxide to nitride was quantitatively determined by X-ray diffraction analysis. GaOOH turned into intermediate mixed phases of $\alpha-\;and\;\beta-Ga_2O_3$, and then single phase of GaN. The reaction time for full conversion $(t_c)$ decreased as the temperature increased. There were two-types of rapid reaction processes with the reaction temperature in the initial stage of nitridation at below $t_c$, and a relatively slow processes followed over $t_c$ does not depends on temperatures. The nitridation process was found to be limited by the rate of an interfacial reaction with the reaction order n value of 1 at $800^{\circ}C$ and by the diffusion-limited reaction with the n of 2 at above $1000^{\circ}C$, respectively, at below $t_c$. The activation energy for the reaction was calculated to be 1.84 eV in the temperature of below $830^{\circ}C$, and decreased to 0.38 eV above $830^{\circ}C$. From the comparative analysis of data, it strongly suggest the rate-controlling step changed from chemical reaction to mass transport above $830^{\circ}C$.
고체 입자가 부상된 충돌제트에서의 입자 거동에 관한 수치해석적 연구
이재범,서영섭,이정희,최영기,Lee, Jae-Beom,Seo, Yeong-Seop,Lee, Jeong-Hui,Choe, Yeong-Gi 대한기계학회 2001 大韓機械學會論文集B Vol.25 No.12
The purpose of this study is to analyze numerically the movement of particles included in turbulent fluid flow characteristics of metallic surfaces. To describe fluid flew, the incompressible Navier-Stokes equation discretized by the finite volume method were solved on the non-orthogonal coordinates with non-staggered variable arrangement, and the k-$\xi$ turbulence model was adapted. After fluid flow was calculated, particle movement was predicted from the Lagrangian approaches. Non-essential complexities were avoided by assuming that the particles had spherical shapes and the Stoke's drag formula only consisted of external farces acting upon them. In order to validate the numerical calculations, the results were compared with the experimental data reported in literature and agreed well with them. The drag force coefficient equation showed better agreement with the experimental data in the prediction of particle movement than the correction factor equation. Impact velocity and impact angle increased as inlet turbulence intensity decreased, relative jet height was lower. or the Reynolds number was larger.