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홍인권,김상철,김원일,이승범 단국대학교 1998 論文集 Vol.33 No.-
Adsorption characteristics of activated carbon were affected by raw materials and operating conditions. Coal based activated carbons were prepared in a rotary kiln type furnace and the pretreatment effect of raw materials for preparing activated carbon was investigated. Steam was employed in manufacturing process as an activation agent. Activation temperature affected the properties of activated carbon. The adsorption capacity, or iodine value was increased in te activation temperature range of 800 to 900℃, yet decreased at higher temperatures than 900℃. Then, the activation effect was analyzed in terms of the activated carbon(AC) yield. It was found that the optimum heating rate and steam amount were 2.9℃/min, and 1g steam/g coalㆍhr, respectively. Effect of coal blends on the preparation of activated carbon was examined. The developing patterns of pore structure were varied with mixing ratio. As the amount of anthracite coal was increased, AC yield increased but adsorption capacity decreased. Pore size and pore size distribution were examined by BET specific surface area analyzer. In the AC yield range of 30∼40%, prepared activated carbon has micropores of sizes below 30Å and iodine value was above 1,000㎡/g in the temperature range of 850∼900℃. Benzene adsorption capacity was similar to those of mixed and Fushun coal but MEK adsorption capacity was superior to that of functions mixed coal. We found that the activated carbon based on coal has comparable to those of commericial products.