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Azido Boronate와 산소 기체를 이용한 D-glucal로부터 β-D-Mannopyranosyl Azide의 전합성과 구조 결정
김진연 ( Jin Yeon Kim ),안태호 ( Tae Ho Ahn ),김정우 ( Jung Woo Kim ) 한국키틴키토산학회 2015 한국키틴키토산학회지 Vol.20 No.1
Treatment of 4,6-O-protected D-glucal derivatives with azido boronate and molecular oxygen in THF afforded 4,6-protected β-D-mannopyranosyl azide. Transformation and probable mechanism of this azidohydroxylation method were discussed and the application of this methodology. We obtained β-D-mannopyranosyl azide and It``s structure was determined by 1 H-NMR and Xray crystallography