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최선희,김종미,홍상황,Choi, Sun-Hee,Kim, Jong-Mee,Hong, Sang-Hwang 한국초등상담교육학회 2011 초등상담연구 Vol.10 No.2
본 연구는 아동청소년 교우관계문제검사(KIPR)에 잠재되어 있는 요인구조를 밝히고 검증하여 이 검사의 심리적 특성을 밝히고 해석적 유용성을 높이는데 목적이 있다. 이를 위해 경남지역 3개 초등학교 4~6학년 아동 616명을 대상으로 아동청소년 교우관계문제검사를 실시하였고 그 중 578명의 자료를 분석하였다. 연구결과를 요약하면 다음과 같다. 첫째, 3요인과 4요인 모형을 설정하여 탐색적 요인분석을 실시한 결과 3요인 모형이 적합한 것으로 나타났다. 3요인 모형에서 요인 1은 아동청소년 교우관계문제검사의 비주장성(C5), 사회적 억제(C4), 냉담(C3), 과순응성(C6) 원형척도의 문항들로 구성되어 있어서 "자신감 결여와 사회적 위축", 요인 2는 통제지배(C1), 자기중심성(C2) 원형척도의 문항들로 구성되어 있어서 "공격성과 타인조종", 요인 3은 자기희생(C7), 과관여(C8), 과순응성(C6) 원형척도의 문항들로 구성되어 있어서 "과잉배려"로 명명하였다. 둘째, 확인적 요인분석을 실시한 결과 3요인 모형은 4요인 모형보다 수집된 자료를 잘 반영하고 있었고(RMSEA=.054), 적합도는 만족할 수준은 아니지만 수용할 수 있는 수준이었고(CFI=.786), 모형의 간명성 또한 적합한 것으로 나타났다(PCFI=.733). 본 연구에서는 교우관계원형에서 상관계수가 높은 인접한 척도끼리는 동일한 요인으로 묶여지는 것을 확인하였고 이를 통해 8개의 원형척도를 망라하는 상위의 대표적인 요인척도를 구성하는데 필요한 근거를 제공하여, 이 검사의 해석적 유용성을 높였다는 점에서 의의가 있다고 생각된다. The purpose of this study is to reveal and confirm the factor structure inherent in the Korean inventory of peer relationships(KIPR; Sang-Hwang Hong, et al., 2009) in order to strengthen the interpretive usefulness of the test. For this purpose, the inventory was administered to the total of 616 children in the fourth through sixth grades in three elementary schools located in Gyungnam area, and the data from 578 of them were analyzed. The results of the study can be summarized as follows. First, as a result of the exploratory factor analysis of 3-factor and 4-factor models, the 3-factor model was found to be more appropriate. In the 3-factor model, the factor 1 is named "Lack of Self-Confidence and Social Withdrawal" as it consists of such circumplex scale items as Non-Assertiveness (C5), Social Avoidance (C4), the Cold (C3), and Too Submissive (C6). The factor 2 is named "Too Aggressive and Controlling" and consists of items Too Controlling (C1) and Hard to be Supportive (C2). The factor 3 is named "Too Caring" and consists of items Too Responsible (C7), Over Involvement (C8), and Too Submissive (C6). Second, as a result of the confirmatory factor analysis, the 3-factor model, in comparison to the 4-factor model, was found to better reflect the collected data(RMSEA=.054), its goodness of fit was not satisfactory but within the acceptable range(CFI=.786), and its power of simplicity and clarity was also adequate(PCFI=.733). In the current study, through the exploratory and confirmatory factor analyses of scores from the Korean inventory of peer relationships circumplex scales, scales within the peer relationship circumplex model that are near each other and are highly correlated were confirmed to be grouped together as same factors. I believe the main merit of the study lies in the above result having provided the necessary foundation for forming the superordinate and representative scale that encompasses the eight circumplex scales, which enhances the test's interpretive usefulness.
Preparation and Electrical Properties of Manganese-incorporated Neodymium Oxide System
Jong Sik Park,Keu Hong Kim,Chul Hyun Yo,Sung Han Lee Korean Chemical Society 1994 Bulletin of the Korean Chemical Society Vol.15 No.9
Manganese-incorporated neodymium oxide systems with a variety of Mn mol% were prepared to investigate the effect of doping on the electrical properties of neodymium oxide. XRD, XPS, SEM, DSC, and TG techniques were used to analyze the specimens. The systems containing 2, 5, 8, and 10 mol% Mn were found to be solid solutions by X-ray diffraction analysis and the lattice parameters were obtained for the single-phase hexagonal structure by the Nelson-Riley method. The lattice parameters, a and c, decreased with increasing Mn mol%. Scanning electron photomicrographs of the specimens showed that the grain size decreased with increasing Mn mol%. The curves of log conductivity plotted as a function of 1/T in the temperature range from 500 to 1000$^{\circ}C$ at $PO_2$'s of $10^{-5}$ to $10^{-1}$ atm for the specimens were divided into high-and low-temperature regions with inflection points near 820-890$^{\circ}C$. The activation energies obtained from the slopes were 0.53-0.87 eV for low-temperature region and 1.40-1.91 eV for high-temperature region. The electrical conductivities increased with increasing Mn mol% and $PO_2$, indicating that all the specimens were p-type semiconductors. At $PO_2$'s below $10^{-3}$ atm, the electrical conductivity was affected by the chemisorption of oxygen molecule in the temperature range of 660 to 850$^{\circ}C$. It is suggested that electron holes generated by oxygen incorporation into the oxide are charge carriers for the electrical conduction in the high-temperature region and the system includes ionic conduction owing to the diffusion of oxygen atoms in the low-temperature region.
Hong, Yong Pyo,Lee, Sung-Hong,Choi, Jong-Ha,Kashima, Ayana,Nakamura, Go,Suzuki, Takayoshi Korean Chemical Society 2014 Bulletin of the Korean Chemical Society Vol.35 No.8
Two diastereoisomers of cyclo(Pro-Tyr) have been synthesized simultaneously. The crystal structures and conformations of both cyclo($\small{L}$-Pro-$\small{L}$-Tyr) and a racemic mixture of cyclo($\small{D}$-Pro-$\small{L}$-Tyr) and cyclo($\small{L}$-Pro-$\small{D}$-Tyr), abbreviated as rac-cyclo($\small{D}$-Pro-$\small{L}$-Tyr/$\small{L}$-Pro-$\small{D}$-Tyr), have been determined by a single-crystal X-ray diffraction study at low temperature. The crystals of rac-cyclo($\small{D}$-Pro-$\small{L}$-Tyr/$\small{L}$-Pro-$\small{D}$-Tyr) belong to orthorhombic space group $Pna2_1$ with a = 10.755 (1), b = 12.699 (1), c = 9.600 (1) ${\AA}$ and Z = 4. The tyrosine side chain is folded towards the diketopiperazine (DKP) ring. The DKP ring adopts a twist boat conformation with pseudo symmetry $C_{2v}$. The pyrrolidine ring has an envelope conformation with the N5, C4, C7 and C8 atoms in a plane. The crystal of rac-cyclo($\small{D}$-Pro-$\small{L}$-Tyr/$\small{L}$-Pro-$\small{D}$-Tyr) is stabilized by hydrogen bonds between amide N2-H2 and carbonyl oxygen O2 in the neighbor. The hydroxyl group of tyrosine residue is also hydrogen bonded to the oxygen of the carbonyl group of the DKP ring in the next molecule. The spectroscopic properties of both isomers are also described.
Jong-Yun Kim,Sang-Eun Bae,Tae-Hong Park,Seung woo Paek,Tack-Jin Kim,Sung-Jai Lee 한국공업화학회 2020 Journal of Industrial and Engineering Chemistry Vol.82 No.-
We have developed a liquid level measurement system using the dynamic bubbler technique. Based onour previous methodology, herein, we established afield-applicable wireless measurement system tosimultaneously monitor the liquid level and density of corrosive molten salts at high temperatures. Theaccuracy and precision of the present technique were suitable for applications in harshfield processes. Regardless of the base pressure under the present experimental conditions, percentage differencescompared with reliable reference values in the literature were less than 10% in the temperature range773–1123 K using KNO3 as a molten salt. Our dynamic bubbler technique produces an average percentagedifference ca. 5–8% with a standard deviation of less than ca. 0.04 g cm 3 between measured andliterature density values in all experiments, whereas the standard deviations in all liquid levelmeasurements were less than 0.3 mm (0.07% relative standard deviation). The present technique is anexcellent alternative to many conventional liquid level and density measurement techniques used underextreme environmental conditions characteristic of common industrial processes.