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Shuai Ji,Yujie Wang,Shikai Gao,Xian Shao,Wei Cui,Yan Du,Mengzhe Guo,Daoquan Tang 한국공업화학회 2019 Journal of Industrial and Engineering Chemistry Vol.80 No.-
Lots of minor constituents in herbal medicines have shown great potential to devolve into leadcompounds, and their extraction is attracting more and more attention in pharmaceutical industry. Thisstudy provided an example that showed efficient and selective extraction of minor bioactive naturalproducts (prenylatedflavonoids with anti-cancer activities) from an herbal medicine (licorice) using pureionic liquids as green solvents. After investigation of a variety of hydrophobic ionic liquids withultrasonic-assisted extraction, we found that [C8MIM]BF4 (1-octyl-3-methylimidazolium tetrafluor-oborate) was the most effective one for extraction offive representative compounds (isoangustone A,glycycoumarin, licoisoflavanone, licoricidin and glabridin), and solvent to solid ratio, extraction time,extraction temperature and soaking time were then optimized through single-factor experiments andresponse surface methodology. As a result, the established method had significantly higher extractionselectivity than conventional organic solvents, which could be attributed to significant physical change oflicorice microstructures after extraction, as well as strong interactions (especially hydrogen bondinteractions) between [C8MIM]BF4 and prenylatedflavonoids by mechanism study. In addition, 78.92% ofthe extracted prenylatedflavonoids could be readily recovered from [C8MIM]BF4 by using reversed-phasesolid phase extraction, and the recyclability of [C8MIM]BF4 was also confirmed.
Qianli Liu,Kaikai Cao,Shikai Qi,You Yang,Shuheng Liang,Huihui Gao,Chen Yang,Dazhe Li,Mengjin Jiang 한국섬유공학회 2020 Fibers and polymers Vol.21 No.7
The spinnability of semi-dilute poly(m-phenylene isophalamide) (PMIA) spinning dope was regulated by a smallamount of surfactants to make it suitable for dry-jet wet spinning. OP-10 shows the best effect of lowering the surface tensionof PMIA spinning dope among the selected surfactants. The effects of different amounts of OP-10 on surface tension andrheological behavior of PMIA spinning dope were investigated. Results show that when the content of OP-10 reaches0.5 wt.%, the surface tension of the PMIA dope reduces to a minimum. The apparent viscosity of the PMIA dope increaseswith the increment of OP-10 contents. The dynamic viscoelasticity study shows that OP-10 also enhances the elasticity of thePMIA spinning dope. The spinning dope with 0.5 wt.% OP-10 can be smoothly spun by dry-jet wet spinning, and theobtained PMIA filament shows excellent mechanical performance.
Chaochen Ma,Jianbing Gao,Shikai Xing,Liwei Sun,Jiangquan Liu 한국화학공학회 2016 Korean Journal of Chemical Engineering Vol.33 No.12
Non-road diesel engines are important polycyclic aromatic hydrocarbon (PAH) sources in the environment due to their high emission concentration compared to on-road diesel engines. Particle- and gas-phase PAH concentrations of a non-road diesel engine were investigated. Non-thermal plasma (NTP) as an effective after-treatment technology was used to reduce PAH emissions. The results showed that particle-phase PAH concentrations were 329.7 μg/m3, 3,206.7 μg/m3, and 1,185.7 μg/m3 without the action of NTP at three different engine loads respectively. Relatively low concentrations were measured for gas-phase PAHs. Excellent linearity was shown for particle-phase with total PAH concentrations both with, and without, NTP. The gas-phase PAH concentrations linearly increased with engine load without NTP. The five most abundant compounds of PAHs were among low molecular weight (LMW) and medium molecular weight (MMW) compounds. Total PAH cleaning efficiency was beyond 50% when treated with NTP at the three different engine loads. We hypothesized that naphthalene (Nap) concentrations increased greatly at 60% and 80% engine loads because it was produced within the plasma zone by decomposition of high molecular weight (HMW) PAHs. The PAHs content of particulate matter (PM) aggregation at 60% load was approximately three times higher than at 40% and 80% loads. High correlation values were observed for MMW PAHs with total PAH concentrations. Correlations of PAH concentration reduction could be important to clarify the PAH reduction mechanism with NTP technology.