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도가니 구조 변경을 통한 6H-SiC 단결정의 직경 확장에 관한 연구
김정규,견명옥,서정두,안준호,김정곤,구갑렬,이원재,김일수,신병철,Kim, Jung-Gyu,Kyun, Myung-Ok,Seo, Jung-Doo,An, Joon-Ho,Kim, Jung-Gon,Ku, Kap-Ryeol,Lee, Won-Jae,Kim, Il-Soo,Shin, Byoung-Chul 한국전기전자재료학회 2006 전기전자재료학회논문지 Vol.19 No.7
A sublimation method using the SiC seed crystal and SiC powder as the source material is commonly adopted to grow SiC bulk single crystal. However, it has proved to be difficult to achieve the high quality crystal and the process reliability because SiC single crystal should be grown at very high temperature in closed system. In this study, SiC crystal boules were prepared with different angles in trapezoid-shaped graphite seed holders using sublimation physical vapor transport technique (PVT) and then their crystal quality was systematically investigated. The temperature distribution in the growth system and the crystal shape were varied with angles in trapezoid-shaped graphite seed holders, which was successfully simulated using 'Virtual Reactor'. The SiC polytype proved to be the n-type 6H-SiC from the typical absorption spectrum of SiC crystal. The micropipe densities of SiC wafers in this study were measured to be < $100/cm^2$. Consequently, SiC single crystal with large diameter was successfully achieved with changing angle in trapezoid-shaped graphite seed holders.