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IBS 법으로 제작한 Bi 계 초전도 박막의 동시 증착 특성
박용필,이준웅 한국전기전자재료학회 1997 電氣電子材料學會誌 Vol.10 No.5
BSCCO thin films have been fabricated by co-deposition at an ultralow growth rate using ion beam sputtering(IBS) method. The growth rates of the films was set in the region from 0.17 to 0.27 nm/min. MgO(100) was used as a substrate. In order to appreciate stable existing region of Bi 2212 phase with temperature and ozone pressure, the substrate temperature was varied between 655 and 82$0^{\circ}C$ and the highly condensed ozone gas pressure(PO$_3$) in vacuum chamber was varied between 2.0$\times$10$^{-6}$ and 2.3$\times$10$^{-5}$ Torr. Bi 2212 phase appeared in the temperature range of 750 and 795$^{\circ}C$ and single phase of Bi 2201 existed in the lower region than 785$^{\circ}C$. Whereas, PO$_3$dependance on structural formation was scarcely observed regardless of the pressure variation. And high quality of c-axis oriented Bi 2212 thin film with T$_{c}$(onset) of about 90 K and T$_{c}$(zero) of about 45 K is obtained. Only a small amount of CuO in some films was observed as impurity, and no impurity phase such as CaCuO$_2$was observed in all of the obtained films.lms.
박용필,김영천,황석영 한국전기전자재료학회 1996 電氣電子材料學會誌 Vol.9 No.1
We investigated the effects of doping elements on the Bi-Sr-Ca-Cu-O ceramics. The doping elements can be classified into four groups depending on their supeconducting characteristics in the Bi-Sr-Ca-Cu-O structure. The first group of doping elements(Co, Fe, Ni and Zn) substitute into the copper site and can reduce the critical temperatures of the 2223 and 2212 phases. The second group of doping elements(Y and La) substitute into the Ca site and cause the disappearance of the 2223 phase and increase the critical temperatures in the 2212 phase. The third group of doping elements(P and K) have a tendency to decompose the superconducting phase and reduce the optimal sintering temperature. The fourth group of doping elements(B, Si, Sn and Ba) almost unaffected the superconductivity of the 2223 and 2212 phase.
소결 후 열처리 조건이 Bi(Pb)SrCaCuO계 초전도 특성에 미치는 영향
박용필,이성우,이준웅 한국전기전자재료학회 1991 電氣電子材料學會誌 Vol.4 No.4
소결 후 냉각 및 Annealing이 Bi(Pb)SrCaCuO계 초전도체의 특성에 미치는 영향에 대해 연구하였다. 소결 후 시편을 500[.deg.C]에서 5[hr] Annealing함으로써 1)미세조직이 치밀화 되었으며 고온상의 체적비가 증가하였다. 2)임계온도 및 전류밀도 특성이 향상되었다.