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RISS 인기검색어
- 검색키워드
- 저자 : Zhiping Du (검색결과 4 건)
- 무료
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- 유료
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Spontaneous vesicle formation from trisiloxane-tailed gemini surfactant
Guoyong Wang,Zhiping Du,Dianlong Zhang,Ping Li 한국공업화학회 2014 Journal of Industrial and Engineering Chemistry Vol.20 No.4
The spontaneous vesicle formation from a novel trisiloxane-tailed gemini surfactant were reported. The surface tension measurements revealed that aggregates are formed, and dynamic light scattering (DLS) measurements suggested the aggregates are vesicles. The size and morphology were observed by transmission electron microscopy (TEM). The vesicle formation was further confirmed by dye entrapment studies.
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Recovery of Bisphenol A by pH-Triggered Magnetic Nanoparticles
Yongsheng Jia,Enze Li,Zhiping Du,Jianfeng Li,Fangqin Cheng 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2019 NANO Vol.14 No.5
Bisphenol A is not only one of the frequent contaminants of industrial wastewater, but also one of the main ingredients in polycarbonate and epoxy resins. This study synthesizes a pH-triggered Fe3O4@mSiO2@DPDES adsorbent for recycling Bisphenol A through adsorption–desorption process. Due to the strong π–π interaction between the phenyl groups in diphenyldiethoxysilane modified magnetic nanoparticles (MNPs) and Bisphenol A, absorbance reached 120.17 mg/g at pH 7, allowing the bisphenol A adsorbed to Fe3O4@mSiO2@DPDES to be trivially separated from aqueous solutions with a magnet. Desorption of the adsorbed bisphenol A in aqueous solution occurred at pH 2, allowing an impressive 95% recovery rate. The durability of the Fe3O4@mSiO2@DPDES adsorbent was tested by repeated separation of bisphenol A from an aqueous solution, with the recovery efficiency remaining greater than 85% after five cycles.
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Qiwen Yin,Wanxu Wang,Wei Xue,Yanyun Bai,Xiaoyuan Ma,Zhiping Du,Guoyong Wang 한국공업화학회 2016 Journal of Industrial and Engineering Chemistry Vol.42 No.-
Sodium perfluoropolyether carboxylate (PFPE-Na) was synthesized via hydrolyzing the correspondinghexafluoropropylene oxide oligomer (PFPF). The structure of PFPE-Na was characterized by FT-IR and 19FNMR. The micellization and aggregation properties of PFPE-Na surfactant in aqueous solution werestudied systematically using equilibrium surface tension, electrical conductivity, dynamic surfacetension, steady-statefluorescence, transmission electron microscopy (TEM) and contact anglemethodologies. The results of equilibrium surface tension at 25 C showed that the critical micelleconcentration (CMC) and the surface tension at CMC (gCMC) of PFPE-Na aqueous solution are lower thansodium perfluorooctanoate [NaPFO, C7F15COONa], which revealing that as a kind of environment-friendly surfactant, PFPE-Na is a perfect substitute of NaPFO. Electrical conductivity measurementsimplied that the micellization of PFPE-Na in aqueous solution was an exothermic and entropy-drivenprocess in the range of temperature investigated. Steady-statefluorescence and transmission electronmicroscopy (TEM) may indicate that PFPE-Na self-assemble in aqueous solution to form larger sphericalaggregates with the increase of concentration. In addition, dynamic surface tension measurements ofPFPE-Na solution showed an extremely efficient adsorption at concentrations above CMC while thedetermination of contact angle of PFPE-Na showed the wetting ability was general.
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Guoyong Wang,Yanyan Zhu,Yunhui Zhai,Wanxu Wang,Zhiping Du,Jieqiong Qin 한국공업화학회 2017 Journal of Industrial and Engineering Chemistry Vol.47 No.-
A simple process to synthesize polyglycerol modified polysiloxane surfactants has been carried outapplying a “grafting-to” approach. After formation of allyl polyglycerol ether (APGE) from diglycerol(DGY) and allyl glycidyl ether (AGE), polysiloxane modified by designed number of polyglycerol groups(PHMS-APGE) were obtained by connecting the APGE structure to different Si H functionalizedpolyhydromethyl siloxane (PHMS). The synthesized APGE-PHMS were characterized by IR and 1H NMR. Solubility measurements showed that the solubility of the as-prepared polymers increased in polarsolvents with the increasing of the amount of hydrophilic APGE groups. Furthermore, the surface activity,surface adsorption, aggregation and spreading behaviors of APGE-PHMS were investigated utilizingsurface tension measurements, dynamic light scattering (DLS), transmission electron microscopy (TEM)and contact angle measurements. The results showed that critical aggregation concentration (CAC) andthe time needed to reach adsorption equilibrium on water surface decrease systematically with theincrease in the number of APGE groups. These polymers in aqueous solutions could aggregate to formspherical assemblies. Moreover, the spreading behavior of these polymers on low energy surface wasfound to be influenced by the number of hydrophilic APGE groups.
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