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Huang Sheng-Jian,Lee Hoi-Kwan,Kang Won-Ho,Wu Qing The Korean Microelectronics and Packaging Society 2004 마이크로전자 및 패키징학회지 Vol.11 No.4
A series of $H_3PO_4$-doped composite membranes based on poly(vinyl alcohol)(PVA) and silica have been prepared by sol-gel process. The proton conductivity, as well as properties of swelling, methanol permeation, was measured in this study. The proton conductivity increased with the molar ratio of $H_3PO_4$ to silica. With the silica content increasing, swelling degree decreased and methanol permeability showed a slight increase. It suggested that the former was mainly determined by hydrophilicity of the membrane, while the latter was dominated by the interconnectivity of matrix. According to the value of on, the optimal conformations of these composite membranes were 60, 70, 80 wt.$\%$ of PS-x in membranes, where x were 1.5, 1.0, and 0.5, respectively. These composite membranes were thermal stability up to $200^{\circ}C$.
Huang, Sheng-Jian,Lee, Hoi-Kwan,Kang, Won-Ho Korean Chemical Society 2005 Bulletin of the Korean Chemical Society Vol.26 No.2
A series of proton conductive inorganic-organic hybrid membranes doped with phosphoric acid ($H_3PO_4$) and/or triethylphosphate (PO(OEt)$_3$) have been prepared by sol-gel process with 3-glycidoxypropyltrimethoxysilane (GPTMS), 3-aminopropyltriethoxysilane (APTES) and tetraethoxysilane (TEOS) as precursors. High proton conductivity of 3.0 ${\times}$ $10^{-3}$ S/cm with composition of 50TEOS-30GPTMS-20APTES-50$H_3PO_4$ was obtained at 120 ${^{\circ}C}$ under 50% relative humidity. Thermal stability of membrane was significantly enhanced by the presence of SiO$_2$ framework up to 250 ${^{\circ}C}$. XRD revealed that the gels are amorphous. IR spectra showed a good complexation of $H_3PO_4$ in the matrix. The conductivity under 75% relative humidity was significantly improved by addition of APTES due to the increase in concentration of defected site in hybrid matrix. The effect of PO(OEt)$_3$, humidifying time, and heat-treatment were also investigated. PO(OEt)$_3$ had no improvement on conductivity and conductivity increased with humidifying time, however, decreased with heating temperature.
Sheng-Jian Huang,Hoi-Kwan Lee,Won-Ho Kang* 대한화학회 2005 Bulletin of the Korean Chemical Society Vol.26 No.2
A series of proton conductive inorganic-organic hybrid membranes doped with phosphoric acid (H3PO4 ) and/or triethylphosphate (PO(OEt)3) have been prepared by sol-gel process with 3-glycidoxypropyltrimethoxy- silane (GPTMS), 3-aminopropyltriethoxysilane (APTES) and tetraethoxysilane (TEOS) as precursors. High proton conductivity of 3.0´103 S/cm with composition of 50TEOS- 0GPTMS-20APTES-50H3PO4 was obtained at 120 ºC under 50% relative humidity. Thermal stability of membrane was significantly enhanced by the presence of SiO2 framework up to 250 ºC. XRD revealed that the gels are amorphous. IR spectra showed a good complexation of H3PO4 in the matrix. The conductivity under 75% relative humidity was significantly improved by addition of APTES due to the increase in concentration of defected site in hybrid matrix. The effect of PO(OEt)3, humidifying time, and heat-treatment were also investigated. PO(OEt)3 had no improvement on conductivity and conductivity increased with humidifying time, however, decreased with heating temperature.
Proton Conducting Behavior of a Novel Composite Based on Phosphosilicate/Poly(Vinyl Alcohol)
Huang, Sheng-Jian,Lee, Hoi-Kwan,Kang, Won-Ho The Korean Ceramic Society 2005 한국세라믹학회지 Vol.42 No.2
A series of proton conductive composite membranes based on poly(vinyl alcohol) and phosphosilicate gels powders were successfully prepared. The proton conductivity of these composite was attributed to the phosphosilicate gel, which derived from tetraethoxysilane and phosphoric acid by sol-gel process at a molar ratio of P/Si = 1.5. The proton conductivity increased with increasing both the content of phosphosilicate gel and relative humidity. Temperature dependence of conductivity showed a Vogel-Tamman-Fulcher type behavior, indicating that proton was transferred through a liquidlike phase formed in micropores of phosphosilicate gel. The high conductivity of 0.065 S/cm with a membrane containing 60 wt$\%$ of the gel was obtained at $60^{\circ}C$ at $90\%$ relative humidity.
Proton Conducting Behavior of a Novel Composite Based on Phosphosilicate/Poly(Vinyl Alcohol)
Sheng-Jian Huang,강원호,Hoi-Kwan Lee 한국세라믹학회 2005 한국세라믹학회지 Vol.42 No.2
A series of proton conductive composite membranes based on poly(vinyl alcohol) and phosphosilicate gels powders were successfully prepared. The proton conductivity of these composite was attributed to the phosphosilicate gel, which derived from tetraethoxysilane and phosphoric acid by sol-gel process at a molar ratio of P/Si=1.5. The proton conductivity increased with increasing both the content of phosphosilicate gel and relative humidity. Temperature dependence of conductivity showed a Vogel-Tamman-Fulcher type behavior, indicating that proton was transferred through a liquidlike phase formed in micropores of phosphosilicate gel. The high conductivity of 0.065 S/cm with a membrane containing 60wt% of the gel was obtained at 60oC at 90% relative humidity.
Inorganic-organic Hybrid Proton Conductive Membranes Doped with Phosphoric Acid
Sheng-Jian Huang,Yong Su Lee,Hoi Kwan Lee,Won Ho Kang 한국산학기술학회 2004 한국산학기술학회 학술대회 Vol.- No.-
A new proton conductive inorganic-organic hybrid membrane doped with H₃P0₄ was fabricated via sol-gel process wit 3-glycidoxypropyltrimethoxysilane(GPTMS), 3-aminopropyltriethoxysilane(APIES)andtetraethoxysilane(TEOS)asprecursors. Theproto conductivity of about 3.0 x 10¯³ S/cm was obtained at 120°C under 50% relative humidity (R.H). DTA curves showed that the thermal stability of the membrane is significantly enhanced by the presence of SiO₂ framework up to 250°C. SEM and XRD revealed that the gel is microporou and amorphous. The addition of APTES improved the conductivity of the membranes and the effect of the APIES on the conductivity was also discussed in this paper.
Yuan, Sheng-Guang,Liao, Wei-Jia,Yang, Jian-Jun,Huang, Guo-Jin,Huang, Zhao-Quan Asian Pacific Journal of Cancer Prevention 2014 Asian Pacific journal of cancer prevention Vol.15 No.24
Background: This study was conducted to determine DEPDC1 expression in hepatocelluar carcinomas (HCCs) and to reveal its potential role in diagnosis and prognosis of affected patients. Materials and Methods: DEPDC1 expression at the mRNA level was detected by quantitative real-time PCR (qRT-PCR) in 205 cases of HCC and paired adjacent normal liver tissues, and by semi-quantitative RT-PCR in 20 cases. Survival curves were obtained by using Kaplan-Meier method and Log-rank test. Independent predictors associated with regard to disease free survival (DFS) and overall survival (OS) were identified using the Cox proportional hazard model. Results: High DEPDC1 mRNA levels were detected in 144 out of 205 cases (70.24%) of HCC, significantly associated with clinicopathological parameters, including tumor size (${\geq}4cm$), alpha-fetoprotein (${\geq}100ng/ml$), B-C of BCLC stage and recurrence. Kaplan-Meier survival analysis revealed that HCC patients with high DEPDC1 expression had poor OS and DFS. Multivariate analysis demonstrated that high DEPDC1 expression was an independent predictor for OS (HR=1.651; 95% 95%CI, 1.041-2.617; p=0.033) and DFS (HR=1.583; 95%CI, 1.01-2.483; p=0.045). Conclusions: Our results indicate DEPDC1 might be a novel diagnostic marker and an independent prognostic predictor for HCC patients.
Yu Jian,Li Wen,Hou Guo-jun,Sun Da-peng,Yang Yuan,Yuan Sheng-xian,Dai Zhi-hui,Yin Hao-zan,Sun Shu-han,Huang Gang,Zhou Wei-ping,Yang Fu 생화학분자생물학회 2023 Experimental and molecular medicine Vol.55 No.-
Hepatitis B protein x (HBx) has been reported to promote tumorigenesis in hepatitis B virus (HBV)-related hepatocellular carcinoma (HCC), but the mechanism awaits further investigation. In this study, we found that cFAM210A (a circular RNA derived from the third exon of transcript NM_001098801 of the FAM210A gene; CircBase ID: hsa_circ_0003979) can be silenced by HBx. cFAM210A expression was downregulated and negatively correlated with tumorigenesis in patients with HBV-related HCC. Furthermore, cFAM210A reduced the proliferation, stemness, and tumorigenicity of HCC cells. Mechanistically, HBx increased the N6-methyladenosine (m6A) level of cFAM210A by promoting the expression of RBM15 (an m6A methyltransferase), thus inducing the degradation of cFAM210A via the YTHDF2-HRSP12-RNase P/MRP pathway. cFAM210A bound to YBX1 and inhibited its phosphorylation, suppressing its transactivation function toward MET. These findings suggest the important role of circular RNAs in HBx-induced hepatocarcinogenesis and identify cFAM210A a potential target in the prevention and treatment of HBV-related HCC.
Yan-sheng Huang,Yue-Ling Long,Jian Cai 국제구조공학회 2008 Steel and Composite Structures, An International J Vol.8 No.2
A method is proposed to estimate the ultimate strength of rectangular concrete-filled steel tubular (CFT) stub columns under axial compression. The ultimate strength of concrete core is determined by using the conception of the effective lateral confining pressure and a failure criterion of concrete under true triaxial compression, which takes into account the difference between the lateral confining pressure provided by the broad faces of the steel tube and that provided by the narrow faces of the steel tube. The longitudinal steel strength of broad faces and that of the narrow faces of the steel tube are calculated respectively due to that buckling tends to occur earlier and more extensively on the broader faces. Finally, the proposed method is verified with experimental results. Corresponding values of ultimate strength calculated by ACI (2005), AISC (1999) and GJB4142-2000 are given respectively for comparison. It is found from comparison that the proposed method shows a good agreement with the experimental results.