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Xin Yao,CHANGCHANG MA,Hai Huang,Zhi Zhu,Hongjun Dong,Chunxiang Li,Wenli Zhang,Yongsheng Yan,Yang Liu 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2018 NANO Vol.13 No.3
In this paper, the biomass carbon quantum dots (CQDs) modified flower-like BiOI (CQDs/BiOI) composite photocatalyst was synthesized by a facile solvothermal method. Compared with the pristine BiOI, the biomass CQDs/BiOI exhibited outstanding photocatalytic activity for degradation of the typical methylene blue (MB) under visible light irradiation since the biomass CQDs could act as electron acceptors to effectively facilitate the separation efficiency of photon-generated carriers and prolong their lifetime. Furthermore, the mechanism detection experiment showed that the ·O2 - and H+ were major activity species, and the photocatalytic electron transfer mechanism was further investigated. This work provided a new insight into biomass CQDs effects and took an important step toward the development of improving Bi-based semiconductor photocatalyst activity.
Yu Zhao,Yongjun Zhou,Lingling Wu,Changchang Li,Zhongguo John Ma 대한토목학회 2020 KSCE JOURNAL OF CIVIL ENGINEERING Vol.24 No.6
The Longgang Bridge in Shaanxi, China, is a complex continuous hybrid structure composed of two cable-stayed self-anchored suspension parts and one single-pylon cable-stayed part. A 1:20-scaled model was established due to the effect of multiple structural transformation, frequent internal force changes during the construction process, and differences between actual material parameters and theoretical calculation parameters. In this paper, the design, materials, counterweight, experimental instrumentation, and construction stages of the scaled model are introduced. Based on the experimental data, the nonlinear behavior of the self-anchored suspension and cable-stayed hybrid bridge during the structural transformation of the construction process is systematically and comprehensively studied. The evolutions of the hanger force and stayed cable force, the variation in the subcable and back-cable forces, the displacement characteristics of the suspension cable and the deflection of the stiffened girder are analyzed, and the relationships among these variables in different states of the structural system are discussed. This paper will serve as a technical reference for the construction of similar bridges in the future.
Longbao Yu,Zhefei Ye,Jinze Li,Chunhong Ma,CHANGCHANG MA,XINLIN LIU,Huiqin Wang,Lili Tang,Pengwei Huo,Yongsheng Yan 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2018 NANO Vol.13 No.6
A series of hamburger-like Ag@ZnO/C core–shell plasmonic photocatalysts have been synthesized via a simple solvothermal method for degradation of tetracycline (TC) under visible light irradiation, possessing high photocatalytic activity and good stability. The presence of localized surface plasmon resonance (LSPR) in the Ag core has increased the photocatalytic activity over an extended wavelength range. The plasmon-induced resonant energy transfer (PIRET) and direct electron transfer (DET) have facilitated the excitation and separation of photogenerated e-/h+pairs, which has been further confirmed by electrochemical investigations. The presences of hydroxyl radicals ( ·OH), superoxide radicals ( · O-2) and singlet oxygen (1O2) in the photocatalytic reaction system of Ag@ZnO/C photocatalyst have been demonstrated by electron spin resonance (ESR) measurements. All of the experiment results indicate that the ternary structure of Ag@ZnO/C can effectively enhance the photocatalytic activity. Furthermore, the effects of introduced Ag contents and carbon source dosage were researched by comparative photocatalytic experiments, and the potential structures of photodegradation products were studied by HPLC-MS.
Pengwei Huo,Jingru Guan,Mingjun Zhou,CHANGCHANG MA,XINLIN LIU,Yongsheng Yan,Shouqi Yuan 한국공업화학회 2017 Journal of Industrial and Engineering Chemistry Vol.50 No.-
Carbon quantum dots (CQDs)/CdSe/reduced graphene oxide (rGO) was fabricated by hydrothermalmethod. The structures, optical and electronic properties of as-obtained photocatalysts were analyzed bytransmission electron microscopy (TEM), X-ray diffraction (XRD) and photoelectrochemical testing. Thephotocatalytic performances were investigated by degradation of tetracycline hydrochloride (TC HCl). The results showed CQDs modified CdSe loaded rGO could effectively remove TC HCl, the CdSe modifiedwith 7 mL CQDs showed higher photocatalytic degradation rate; the 5 wt% loaded rGO for CQDs/CdSeshowed highest photocatalytic activity. The photocatalytic mechanism exhibited OH, O2and 1O2radicals play key roles
Pengwei Huo,Yanfeng Tang,Mingjun Zhou,Jinze Li,Zhefei Ye,CHANGCHANG MA,Longbao Yu,Yongsheng Yan 한국공업화학회 2016 Journal of Industrial and Engineering Chemistry Vol.37 No.-
ZnWO4-CdS heterostructure photocatalysts have been successfully synthesized by hydrothermalmethod with assembling CdS on the surface of ZnWO4. The obtained composite photocatalysts werecharacterized by X-ray diffraction, transmission electron microscopy, Raman, thermo-gravimetricanalysis, UV–vis diffuse reflectance spectroscopy, photoluminescence and photocurrent measurement. The results show that the interface between ZnWO4 and CdS is well formed, and the CdS nanoparticlesare uniformly distributed onto ZnWO4 nanorods which could facilitate charge transfer and reducerecombination of photo-generated electrons and holes. Compared with pure ZnWO4 and CdS, the aspreparedheterostructure photocatalysts exhibit excellent photostability and photodegradation abilityof ciprofloxacin (CIP) under visible light irradiation.
XINLIN LIU,Yongsheng Yan,Qian Wang,Peng Lv,GUANXIN YAO,CHANGCHANG MA,Yan Yan,Yanfeng Tang 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2014 NANO Vol.9 No.2
A new-type photocatalyst of cadmium sul¯de carbon nanotubes (CdS/CNTs) was prepared bythe hydrothermal method. This as-prepared CdS/CNTs composite photocatalyst was proved toexhibit an excellent photocatalytic activity for degradation of tetracycline (TC). Specially, the95%-CdS – 5%-CNTs composite photocatalyst played the best degradation rate (81.2%) in 60 minunder the visible light irradiation. Moreover, this 95%-CdS – 5%-CNTs composite photocatalystpossessed great stability and could be used at least four cycles with almost no loss of photo-catalytic e±ciency. Furthermore, the as-synthesized CdS/CNTs composite photocatalyst wascharacterized by X-ray di®raction (XRD), transmission electron microscopy (TEM), UV-Visdi®used re°ectance spectra (UV-Vis), Raman and thermal gravimetry (TG). In addition, thepossible mechanism and kinetics of photodegradation of TC with CdS/CNTs photocatalyst wasalso discussed.
Dongyao Wu,Jinze Li,Jingru Guan,Chongyang Liu,Xiaoxu Zhao,Zhi Zhu,CHANGCHANG MA,Pengwei Huo,Chunxiang Li,Yongsheng Yan 한국공업화학회 2018 Journal of Industrial and Engineering Chemistry Vol.64 No.-
An Intercalated heterostructural g-C3N4/TiO2/HNTs supported photocatalyst was successfully prepared via sol–gel and calcination methods. The introduction of HNTs and the g-C3N4-TiO2 heterojunction effectively enhanced the charge transfer and separation efficiency of photogenerated electron–hole pairs, which endued the g-C3N4/TiO2/HNTs hybrid material with an outstanding photoelectric performance and good stability. And an obviously enhanced photocatalytic activity was exhibited by photodegrading ciprofloxacin compared with pure TiO2. Furthermore, the main active species were detected through trapping experiment and ESR spin-trap technique with DMPO, which confirmed that the O2− and the h+ were the main active species in the photocatalytic system.