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비수용성 매질로부터 Ni(OH)<sub>2</sub> 반응슬러리의 환원반응에 의한 니켈 분말의 제조
최은영,이윤복,윤석영,김광호,김진천,임영목,김형국,김양도,Choi Eun Young,Lee Yoon Bok,Yoon Suk Young,Kim Kwang Ho,Kim Jin Chun,Rhyim Young Mok,Kim Hyong Kuk,Kim Yang Do 한국재료학회 2005 한국재료학회지 Vol.15 No.5
Nickel Powders were synthesized by the reduction of $Ni(OH)_2$ reactant slurries from nonaqueous media, and the morphological characteristics of nickel powders with the addition of NaOH, the composition of mixed solvents, reaction temperature and reaction time were investigated. The NaOH addition changed the structure of agglomeration in the submicron range. As the volume ratio of TEA to DEA increased, the powders slightly suppressed the agglomeration between particles and their size increased. The reaction temperature on size and shape of nickel powders was significant. As reaction time was shortened from 40 min to 0.3 min at $220^{\circ}C$, size distribution of nickel powders was transferred to a narrow size distribution owing to the presence of smaller particles with below $1.0\;{\mu}m$.
DEA 용액으로부터 히드라진의 환원 반응에 의한 니켈 분말 제조
최은영,이윤복,윤석영,김광호,김진천,임영목,김형국,김양도,Choi, Eun-Young,Lee, Yoon-Bok,Yoon, Suk-Young,Kim, Kwang-Ho,Kim, Sin-Chun,Rhyim, Yaung-Mok,Kim, Hyong-Kuk,Kim, Ynng-Do 한국세라믹학회 2005 한국세라믹학회지 Vol.42 No.6
Nickel powders synthesized by the reduction of hydrazine of nickel salts fiom diethanolamine(DEA) solution, and investigated the morphological characteristics of nickel powders with the addition of hydrazine, reaction temperature, the composition of mixed solvents. The addition of hydrazine in DEA solution largely affected on size control of nickel powders. Under $N_2H_4/Ni^{2+}$ molar ratio= 1.5 and 2.0 conditions, spherical nickel powders in the submicron range obtained, owing to higher the reduction rate. An increase of temperature increased the size of nickel particles. At $220^{\circ}C$ for 40 min, the nickel powders composed of polyhedral particles with high crystalline in the submicron range. The mixed volume ratio of TEA to DEA affected on the increase of particle size and the inhibition of agglomerate between particles.
DEA 용액에서 암모니아를 함유한 염화니켈 수용액으로부터 니켈 분말의 입경 제어
최은영,이윤복,윤석영,김광호,김진천,임영목,김형국,김양도,Choi Eun Young,Lee Yoon Bok,Yoon Suk Young,Kim Kwang Ho,Kim Jin Chun,Rhyim Young Mok,Kim Hyong Kuk,Kim Yang Do 한국분말야금학회 2005 한국분말재료학회지 (KPMI) Vol.12 No.3
Nickel powders were synthesized by the hydrazine reduction of nickel chloride solution containing ammonia in DEA solutions. The size distribution of nickel powders were investigated as a function of ammonia concentration, hydrazine concentration and the mixed composition ratio of diethanolammine (DEA) and triethanolammine (TEA). Nickel powders with the size in submicron range were obtained at $185^{\circ}C$ for 45 minutes by hydrazine reduction of nickel chloride solution in DEA solutions. The hydrazine concentrations showed significant effects on the particle size and shape distribution of nickel powders under $NH_3/Ni^{2+}$ molar ratio of 2.0 condition. As the mixed volume ratio of TEA and DEA increased, nickel powders with relatively larger particle size and low agglomeration were obtained. Nickel powders with particle size in the ranged from 0.4 to $0.9\;{\mu}m$ were obtained at the 50 $vol.%$ of TEA.
강소라(Gang, So-Ra),윤석영(Yoon, Suk-Young),장덕례(Chang, Duk-Rye) 한국신재생에너지학회 2009 한국신재생에너지학회 학술대회논문집 Vol.2009 No.11
투과증발은 저 에너지 분리기술로서 공비혼합물의 분리 및 유기화화물을 선택적으로 분리하는 공정에 활용되고 있다. 투과증발공정을 위한 막으로 쓰이는 대표적인 고분자 재료인 친수성 고분자 PVA(Poly(vinyl alcohol)는 하이드로실 그룹을 포함하고 있어 물에 대한 선택도가 뛰어난 장점을 가지고 있다. 그러나 PVA는 물에 대한 친화력이 높아 투과증발막으로 적용하기 위해서는 내수성을 향상시키기 위하여 가교시킨후 투과증발막으로 사용가능하다. 본 연구에서는 PVA 분리막을 투과증발막으로 적용하기 위하여 PVA를 전기방사에 의해 나노섬유로 제조하고 제조된 나노섬유가 수용액에서 내수성을 갖게 하기 위해 10-70%의 KOH수용액에 가교화 하여 특성을 알아보았다.