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보통 포틀랜드 시멘트 물성에 미치는 시멘트 입도의 영향
변승호,김형철,김재영,최현국,송종택,Byun, Seung-Ho,Kim, Hyeong-Cheol,Kim, Jae-Young,Choi, Hyun-Kuk,Song, Jong-Taek 한국세라믹학회 2010 한국세라믹학회지 Vol.47 No.5
This study examined the effects of particle size on characteristics of cement by controlling the particle size of commercial cement. Through a size adjustment, the cement has increasing more of particles that are less than $10{\mu}m$ in size so the initial reaction time has been shortened as a result of improvement in the early hydration reaction. Additionally, it showed a great characteristics of strength from the early age and the initial hydration heat has been increased as well. In the upper and middle parts cements, the initial hydration reaction rate contribution is high with the $10{\mu}m$ compared to original cement. So the initial hydration reaction rate is improved and as a result, it also showed relatively high hydration heat as well. Additionally, adiabatic temperature also showed an increase rate in the results.
파이넥스 슬래그 미분말을 혼합한 시멘트 페이스트의 유동특성
이근재,변승호,송종택,Lee, Keun-Jae,Byun, Seung-Ho,Song, Jong-Taek 한국세라믹학회 2009 한국세라믹학회지 Vol.46 No.6
In this study, rheological properties of cement pastes containing ground Finex-slag (4000, 6000, 7000 c$m^2$/g) were investigated bymini-flow test and coaxial cylinder viscometer. And also blast furnace slag(4000, 6000, 7000 c$m^2$/g) were used for comparison. According to the experimental results, Finex-slag and blast furnace slag showed very similar trend in the rheological properties of the cement pastes. The fluidity of cement pastes blended Finex-slag and blast furnace slag powder were improved by high replacement ratio. In the relationship of plastic viscosity and yield stress appeared the tendency of the proportion greatly. And in the relationship of plastic viscosity, yield stress and mini-flow appeared the tendency of the inverse proportion.
박효상,유동우,변승호,송종택,Park, Hyo-Sang,Yoo, Dong-Woo,Byun, Seung-Ho,Song, Jong-Taek 한국세라믹학회 2009 한국세라믹학회지 Vol.46 No.1
In this study, rheological properties of ternary system cement containing ground fly ash(F3, Blaine specific surface area $8,100\;cm^2/g$) were investigated using mini slump, coaxial cylinder viscometer and conduction calorimeter. In the results, the segregation resistance was observed at high W/B and PC area while the replacement ratio of F3 was increasing. The 2:5:3 system was shown in higher fluidity and lower hydration heat than 3:4:3 system. The segregation range of cement pastes occurred over 175 mm in average diameter by mini slump and below $10\;dynesec/cm^2$ of the plastic viscosity or below 50 cP of the yield stress by coaxial cylinder viscometer. It was observed that even if BFS and FA blended together admixture properties would remaine as they were separately. The properties of admixture would not be changed. On the above results, the decreased replacement ratio of OPC and increased replacement ratio of admixtures would be possible.
고로슬래그 및 플라이 애시 분말을 혼합한 시멘트 페이스트의 유동특성
송종택,박효상,변승호,유동우,Song, Jong-Taek,Park, Hyo-Sang,Byun, Seung-Ho,Yoo, Dong-Woo 한국세라믹학회 2008 한국세라믹학회지 Vol.45 No.6
Rheological properties of cement pastes containing blast furnace slag (BFS: 3,900, $7,910\;cm^2/g$) or fly ash powder (FA: 4,120, $8,100\;cm^2/g$) according to the ratio of water/binder (W/B) and the dosage of polycarboxylate type superplasticizer (PC) were investigated by a mini slump and a coaxial cylinder viscometer. In this experiment, the ratio of replacing OPC with BFS or FA was 30 wt%, the W/B was from 30 to 70 wt%. As a result, the fluidity of cement paste containing BFS or FA was improved with increasing W/B and the dosage of PC. BFS or FA replaced cement paste with W/B 70% and PC 0.3% showed the highest fluidity. The segregation range of cement paste was occurred below $10\;d/cm^2$ of the yield stress and below 50 cPs of the plastic viscosity by the coaxial cylinder viscometer. And also it was formed that the plastic viscosity and the yield stress of FA replaced cement paste were higher than them of BFS replaced cement paste.
김재영(Kim Jae Young),변승호(Byun Seung Ho) 대한토목학회 2008 대한토목학회논문집 A Vol.28 No.2A
콘크리트의 균열이 수밀성을 떨어트리고 내구성을 악화시키는 것은 이미 잘 알려진 사실이다. 균열에 의한 이러한 성능저하는, 콘크리트에 균열이 발생하면 물 뿐만이 아니라 염화물, 이산화탄소, 황산염과 같이 유해한 물질들의 침투가 용이해지기 때문이다. 하지만 균열이 물과 접촉하는 경우 일부는 폐쇄 된다. 이러한 현상을 self-healing이라고 하며, self-healing은 균열면에서 새로이 생성되는 수화물과 밀접한 관련이 있다. 콘크리트의 self-healing과 관련한 상당수의 연구에서 공통적으로 균열면 표면에서 CSH겔이 관찰됨을 확인하였다. 그러나 self-healing에 관한 일부 연구에서는 CSH겔 뿐만 아니라 수산화칼슘 및 에트링자이트가 균열 표면에서 관찰되었다고 보고하였다. 본 연구에서는 self-healing에 의한 수화생성물을 확인하고자 하였으며, 또한 구체방수재가 self-healing에 미치는 영향을 평가하고자 하였다. 균열 표면에 대하여 XRD, DSC, SEM, EDX 분석을 실시한 결과 시멘트계에서 self-healing은 CSH겔, 수산화칼슘, 에트링자이트와 연관이 있음을 확인하였다. 또한 구체방수재가 섬유상(또는 침상)의 수화물의 생성을 촉진하고 이들 수화물이 망목구조 형태를 이루는 것을 확인하였다. 이러한 섬유상의 수화물이 시멘트 계의 self-healing에 매우 효과적인 것으로 판단된다. It is well known that cracks in concrete decrease permeability and durability of concrete because cracks enhance the penetration of water or corrosive chemicals like as chlorides, carbon dioxides, sulfates and some others. But some of cracks in hardened cements may be sealed in case of contacting water. This phenomenon is called "self healing" and it has a close relation to hydration products newly formed on surfaces of cracks. Many studies on self healing in concretes commonly showed that CSH gel has been observed on crack surfaces. And some studies have reported that calcium hydroxides and ettringite were observed as well as CSH gel on crack surfaces. This study was carried out to investigate hydration products formed by self healing process and also examine the influence of waterproof admixture for concretes on self healing of cement. As a result of XRD, DSC, SEM and EDX analysis of crack surfaces, it was found that self healing of cement was related to CSH gel, calcium hydroxides and ettringite. And waterproof admixture increased fibrous (needle-like) hydration products which were in network form. It is estimated that such fibrous products are effective for self healing process of cement system.