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Nguyen Van Hung,Bui Thi Minh Nguyet,Nguyen Huu Nghi,Nguyen Minh Luon,Nguyen Ngoc Bich,Le Van Thanh Son,Nguyen Trung Kien,Dao Ngoc Nhiem,Nguyen Thanh Tuoi,Dinh Quang Khieu 대한환경공학회 2024 Environmental Engineering Research Vol.29 No.4
In the present work, ZnO/g-C₃N₄/biochar was prepared, and it was used for visible-light driven photocatalytic degradation of some colorants (methylene blue, rhodamine B, methyl orange) and some antibiotics (doxycycline, ciprofloxacin, amoxicilline). Biochar was prepared by pyrolysing Phragmites australis biomass. The ZnO/g-C₃N₄/biochar composite was synthesized with the alkaline hydrolysis method. The obtained materials were characterized by X-ray diffraction, scanning electron microscopy, transition electron microscopy, energy dispersive X-ray/elemental mapping, ultraviolet-visible-diffuse reflectance spectroscopy, photoluminescence spectroscopy, nitrogen adsorption/desorption isotherms and X-ray photoelectron spectroscopy. The results show that ZnO nanoparticles with a large surface area are highly dispersed on the g-C₃N₄ particle surface and biochar. The composite exhibits superior photocatalytic degradation ability toward doxycycline, a broad-spectrum antibiotic of the tetracycline compared with individual components (ZnO or g-C₃N₄) and satisfies stability after six treatment cycles. The kinetics and degradation mechanisms of doxycyline were also addressed. In addition, the present catalyst also exhibits the photocatalytic degradation of methylene blue, rhodamine B, methyl orange, ciprofloxacin and amoxicillin in visible-light regions.
Nguyen Huu-Manh,Duong The-Khang,Nguyen Van-Khuyen,Nguyen Thi-Khanh-Ly,Dong Thi-Hoang-Yen,Nguyen Canh-Hung,Tung Nguyen-Thach 한국약제학회 2024 Journal of Pharmaceutical Investigation Vol.54 No.2
Purpose A two-step experimental design was used to develop a lornoxicam (LOR)-loaded topical hydrogel patch. We specifically focused on the simultaneous effect of the ion pair formation agent (triethanolamine [TEA]) and the chemical enhancer (cremophor RH40 [RH40]) on flux and conducted physicochemical studies and skin physiology assessments to obtain further information. Methods Drug-in-adhesive patches were fabricated using a micrometer-adjustable film applicator. The applied Design of Experiments (DoE) approach consisted of the Fractional Factorial Resolution V + design and the Central Composite Face design established by the MODDE® 12.0 software. Molecular-level drug-excipient interactions were investigated using infrared (IR) and proton nuclear magnetic resonance (1H NMR) spectroscopy. The effects on skin physiological function was assessed using DermaLab Combo. Results DoE results revealed that TEA enhanced flux by 3.14-fold, whereas RH40 reduced it by 4.62-fold. The addition of RH40 resulted in the disappearance of the proton peak within the region of 12–13 ppm, suggesting competition for hydrogen bonding with LOR between TEA and RH40. The optimized formulation (4% TEA, 0% RH40, and 0.2% Al(OH)3) increased skin hydration by 6.20-fold. Opposing effects of TEA and RH40 on skin elasticity were observed. Conclusion Expected flux and adhesion strength for the optimized formulation were 7.18 μg·cm–2·h–1 and 11.79 mJ, respectively. Our understanding of the conflicting effects of TEA and RH40 has been advanced. The integrated use of the two-step DoE, physicochemical studies, and skin physiology assessments was proven to be effective in elucidating the simultaneous effects of different permeation-modifying strategies on patches, thus having substantial value for the successful execution of future research endeavors.
Phuc Nguyen Thien,Giang Nguyen Thi Huong,An Vu Nguyen Thien Truong,Nam Nguyen Thanh Hoai,Anh Ly Duc,Nguyen Huynh Cam,An Hoang,Phong Mai Thanh,Hieu Nguyen Huu 한국탄소학회 2023 Carbon Letters Vol.33 No.2
In this study, graphene oxide (GO) was synthesized by the improved Hummers’ method. The degree of oxidation from graphite (Gi) to GO was determined through interlayer spacing calculated from X–ray diffraction. Besides, the effect of KMnO4:Gi ratios (X1), H2SO4 volume (X2), oxidation temperature (X3), oxidation time of stage 1 (X4), and oxidation time of stage 2 (X5) was screened by the Plackett–Burman model. The simultaneous impact of three factors that influenced the degree of oxidation (X1, X2, and X3) was studied by the Box–Behnken experimental model of response surface methodology to achieve suitable conditions for the GO synthesis process. The characterization of GO product was investigated via the modern analytical methods: X-ray diffraction, Raman spectroscopy, Fourier transform infrared spectroscopy, UV–Vis spectroscopy, field emission scanning electron microscopy, transmission electron microscopy, and atomic force microscopy. In addition, the study was also carried out on a pilot scale for orientation in industrial application with the yield of 14 g/batch.
Anti-inflammatory tirucallane saponins from Paramignya scandens.
Phan, Nguyen Huu Toan,Thuan, Nguyen Thi Dieu,Ngoc, Ninh Thi,Thao, Nguyen Phuong,Kim, Sohyun,Koh, Young Sang,Thanh, Nguyen Van,Cuong, Nguyen Xuan,Nam, Nguyen Hoai,Kiem, Phan Van,Kim, Young Ho,Minh, Cha Pharmaceutical Society of Japan 2015 Chemical & pharmaceutical bulletin Vol.63 No.7
<P>Five new tirucallane saponins, paramignyosides A-E (1-5), were isolated from the water fraction of the Paramignya scandens stem and leaves. Their structures were elucidated on the basis of spectroscopic evidence including high-resolution electrospray ionization mass spectrometry (HR-ESI-MS) and one dimensional (1D)- and 2D-NMR. The effects of isolated compounds on pro-inflammatory cytokines were evaluated by measuring the production of interleukin (IL)-12 p40, IL-6, and tumor necrosis factor-α (TNF-α) in lipopolysaccharide (LPS)-stimulated bone marrow-derived dendritic cells (BMDCs). Paramignyoside C (3) exhibited selective and potent inhibitory effect (IC50=5.030.19??M) on the production of IL-12 p40 comparable to that of the positive control, SB203580 (IC50=5.000.16??M). Further studies are required to confirm efficacy in vivo and the mechanism of anti-inflammatory effects.</P>
Two New C-Glucosyl Benzoic Acids and Flavonoids from Mallotus nanus and Their Antioxidant Activity
Phan Van Kiem,Nguyen Thi Mai,Chau Van Minh,Nguyen Huu Khoi,Nguyen Hai Dang,Nguyen Phuong Thao,Nguyen Xuan Cuong,Nguyen Hoai Nam,Nguyen Xuan Nhiem,Yvan Vander Heyden,Joëlle Quetin-Leclercq,김교남,장해동,김영호 대한약학회 2010 Archives of Pharmacal Research Vol.33 No.2
Two new 2-C-β-D-glucopyranosyl benzoic acid derivatives named mallonanosides A (1) and B (2) were isolated from the methanolic extract of the leaves of Mallotus nanus along with five known flavonoids, kaempferin (3), juglanin (4), quercitrin (5), myricitrin (6), and rhoifolin (7). Their structures were established on the basis of spectral and chemical evidence. Their antioxidant activities were shown to depend on the number of hydroxyl groups, and the location and species of sugar moiety.
Advanced Magnetic Materials Produced by Using Rapid Quenching Technology
Nguyen Hoang Nghi,Nguyen Van Dung,Trinh Thi Thanh Nga,Bui Thi Khanh Nhung,Mai Thanh Tung,Nguyen Huu Tinh,Hoang Nhat Hieu,Bui Xuan Chien,Nguyen Thi Hong Tam 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.6
Amorphous alloys produced by using a rapid quenching technique are considered to be a precursor for producing nanosized and multiphase structures by precipitation (the top-down method). By using this technique, several new magnetic materials with different magnetic properties based on different physical mechanisms have been manufactured and investigated. Three new magnetic materials, a nanocrystalline soft magnetic material, a soft-hard permanent magnet and a Me-3d granular alloy with a GMR effect, what were prepared under local conditions, are presented and discussed in the experimental point of view. Amorphous alloys produced by using a rapid quenching technique are considered to be a precursor for producing nanosized and multiphase structures by precipitation (the top-down method). By using this technique, several new magnetic materials with different magnetic properties based on different physical mechanisms have been manufactured and investigated. Three new magnetic materials, a nanocrystalline soft magnetic material, a soft-hard permanent magnet and a Me-3d granular alloy with a GMR effect, what were prepared under local conditions, are presented and discussed in the experimental point of view.
CePO4:Tb Nanoparticles: Preparation, Structure and Optical Properties
Nguyen Vu Thanh,Tran Kim Anh,Nguyen Quang Liem,Nguyen Huu Quan,Nguyen The Khoi 한국물리학회 2008 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.52 No.5
Nanocrystals of CePO4:Tb were prepared by reacting the corresponding metal chlorides, phos- phoric acid and trioctylamine at 200℃ in tris(2-ethylhexyl) phosphate (TEHP). The samples were characterized by X-ray diffraction and scanning electron microscopy (SEM). The photoluminescence (PL) and the absorption spectra of CePO4:Tb nanoparticles will be presented. The PL spectra are described by using the well-known 5D4 - 7FJ transitions (J = 6, 5, 4, 3 ···) of Tb3+ ions with the strongest emission at 543 nm for J = 5. The dependence of PL intensity on Tb3+ concentration has been investigated. Nanocrystals of CePO4:Tb were prepared by reacting the corresponding metal chlorides, phos- phoric acid and trioctylamine at 200℃ in tris(2-ethylhexyl) phosphate (TEHP). The samples were characterized by X-ray diffraction and scanning electron microscopy (SEM). The photoluminescence (PL) and the absorption spectra of CePO4:Tb nanoparticles will be presented. The PL spectra are described by using the well-known 5D4 - 7FJ transitions (J = 6, 5, 4, 3 ···) of Tb3+ ions with the strongest emission at 543 nm for J = 5. The dependence of PL intensity on Tb3+ concentration has been investigated.
A Simple SVM Technique to Eliminate Common-mode Voltage for Matrix Converters
Huu-Nhan Nguyen,Tuyen D. Nguyen,Thanh-Luan Nguyen,Hong-Hee Lee 전력전자학회 2019 ICPE(ISPE)논문집 Vol.2019 No.5
In a matrix-converter (MC) system, commonmode voltage (CMV) causes damage to the motor bearings and other equipment. When the MC is controlled by means of space vector modulation (SVM), zero-CMV can be achieved by using only rotating-vector states to drive the MC. However, as the computation becomes quite complicated, it is not easy to apply the rotating-vector states in practice. This paper presents a simple SVM technique using rotating-vector states to eliminate the CMV for MCs. Based on the conventional SVM method, the proposed SVM technique achieves the zero CMV for MCs within a few simple steps by considering the relationship between active-vector and rotating-vector states. The performance and effectiveness of the proposed technique are verified by simulation results.
Nguyen Huu Nghia,Nguyen Thi Nguyen,Phan Trong Binh,Le Thi May,Tong Tran Huy,Pham Thai Giang,Sophie St-Hilaire,Phan Thi Van 한국수산과학회 2022 Fisheries and Aquatic Sciences Vol.25 No.8
This study assessed the effects of oxygen and ozone nanobubbles on gill morphology, weight gain, and mortality of Pacific white shrimp (Penaeus vannamei), as well as the level of Vibrio parahaemolyticus and water quality of shrimp culture tanks under lab conditions. Two experiments were carried out with oxygen macrobubble, ozone macrobubble, oxygen nanobubble, ozone nanobubble, and control treatments (air-stone macrobubble). Experiments were done in triplicate in 100 L tanks with 15‰ saline water, and 20 shrimp per tank. Tanks in Experiment 1 were not inoculated with bacteria; tanks in Experiment 2 were inoculated with V. parahaemolyticus at a concentration of 106 CFU/mL. The results revealed that short treatments with ozone nanobubbles had minimal impact on shrimp gills, mortality, and growth rates, reduced V. parahaemolyticus concentration in water compared to the other groups, and improve water quality. These laboratory results indicate that ozone nanobubble treatment may be useful for controlling V. parahaemolyticus. More work is needed to find the best protocol to apply the technology on a commercial scale.