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HPLC-ICP/MS 와 ICP/MS를 이용한 FAPAS 07187 쌀의 총비소, 무기비소, 카드뮴 측정
노현명 ( Hyun Myung Noh ),김지영 ( Ji Young Kim ),김원일 ( Won Il Kim ),( Anitha Kunhikrishnan ),김민지 ( Min Ji Kim12 ),김경진 ( Gyeong Jin Kim ),박기문 ( Ki Moon Park ),류지혁 ( Ji Hyock Yoo ),김두호 ( Doo Ho Kim ),이영자 ( Y 한국환경농학회 2013 한국환경농학회 학술대회집 Vol.2013 No.-
Metal (loid)s such as environmental contaminants affect food safety. Metal (loid)s exist trace extremely in agriculture products. Therefore it is important to analyze accurately about trace these metals. High resolution techniques and quality controls are needed to analyze these materials. In order to achieve quality results, standardized methods and techniques are required. So ISO(International Organization for Standardization) of laboratory proficiency testing is determination of laboratory testing performance by means of inter-laboratory comparison. The values have been derived as a consensus of a number of laboratories using a variety of methods. Proficiency tests were applied to analyze the metal(loid)s [inorganic arsenic (As), total As and cadmium (Cd)] in powdered rice FAPAS 07187 (Food Analysis Performance Assessment Scheme; February-April 2013). The rice powder sample was extracted with 1% HNO3 for inorganic As for microwave-assisted extraction using water at 95℃ for 90 min and their analysis by HPLC/ICPMS. Also, HNO3 for total As and Cd using microwave-assisted extraction using at 200℃ for 50 mins and analysis by ICP/MS. Validation check was performed for accuracy using CRM (NMIJ CRM 7503-a) for inorganic As, and CRM (IRMM-Rice CRM) for total arsenic and cadmium. The result were satisfactory. FAPAS 07187 the z-scores of inorganic As, total As and Cd in powdered rice were-1.8,-0.9 and 0.2(lzl<2, respectively).
친환경농산물과 GAP농산물 인증제도의 올바른 이해 - 'GAP' 인식부족으로 혼돈 '농법 선택'은 소비자 몫
김두호,Kim, Du-Ho 한국작물보호협회 2009 자연과 농업 Vol.246 No.-
1997년에 '친환경농업육성법'을 제정, 시행하고 2001년부터 친환경 농산물 인증제도를 도입, 운영해 오고 있으나 69%가 저농약농산물로 유기 무농약농산물의 보편화는 이루어 지지 않고 있다. 또 2006년에는 농산물품질관리법에 GAP 제도를 반영시켜 시행, 운영해오고 있으나 인증농산물은 아직 초보단계에 머물고 있는 실정이다.
단열재가 극저온 용기의 내부지지대 구조설계에 미치는 영향
김두호,지현진,김기열,조성백,Kim, Doo-Ho,Ji, Hyun-Jin,Kim, Ki-Youl,Cho, Sung-Baek 한국군사과학기술학회 2011 한국군사과학기술학회지 Vol.14 No.3
The cryogenic vessel, storing a liquified solutions as LOX and $LN_2$, consists of a external vessel, internal vessel, thermal insulator and internal support. The internal support should be satisfied with mechanical strength not only to support weight of internal tank but also to maintain uniform space between external and internal tank in spite of external mechanical shock. However, excessive structure design of internal supports is able to increase the amount of heat conduction and the rate of vaporization. The thermal insulator, filled with space between a external and internal vessel, reduces the rate of heat transfer and guarantees the standing time of cryogenic vessel. Especially powder type of insulator has low thermal conductivity and reduce the specification of structure design. In order to evaluate the effect of insulator on structure design, the experiment set-up simulated cryogenic vessel was tested in shock environment according to thermal insulator. As a result, the behavior of internal support under external shock was understood and the design criteria was able to be suggested.
전해수를 이용한 들깻잎 중 Salmonella Typhimurium과 Staphylococcus aureus의 저감화 효과 분석
김세리(Se-Ri Kim),류경열(Kyoung Yul Ryu),이명희(Myoung-Hee Lee),정찬식(Chan-Sik Jung),윤요한(Yohan Yoon),심현보(Won-Bo Shim),김주희(Ju-Hee Kim),김병석(Byung-Seok Kim),유순영(Soon-Young Yoo),김두호(Doo-Ho Kim),윤종철(Jong-Chul Yun),정덕 한국식품과학회 2012 한국식품과학회지 Vol.44 No.4
본 연구는 들깻잎에 존재하는 Salmonella Typhimurium, Staphylococcus aureus에 대한 전해수의 저감효과를 분석하고 전해수로의 유기물의 유입과 들깻잎과 전해수의 비율이 전해수의 효과에 미치는 영향을 분석하고자 수행하였다. 들깻잎에 S. Typhimurium과 S. aureus을 7.0 log10CFU/g 정도로 접종 한 후 25, 50, 75, 100 ppm에서 1, 3, 5분 동안 각각 처리하여 시간과 농도에 따른 전해수 효과를 분석하였다. 또한 유기물이 전해수의 효과에 미치는 영향을 분석하기 위해 전해수에 첨가한 유기물 농도는 150, 300, 450, 600 μg/L 수준이었고, 들깻잎과 전해수의 처리비율은 1:10, 1:25, 1:50이었다. 그 결과, S. Typhimurium과 S. aureus 모두 유효 염소 농도가 증가할수록 미생물 저감효과도 높아지는 경향을 보였으며(p<0.05) 두 균주 모두 100 ppm 처리에서 25 ppm 처리에서 보다 전해수의 저감효과가 약 0.7 log10CFU/g 정도 높게 나타났다(p<0.05). 하지만 처리 시간에 따른 효과는 없었다 (p>0.05). 또한 전해수 중 유기물 함량이 증가할수록 S. Typhimurium과 S. aureus의 제어효과는 감소하였다(p<0.05). 유기물 600 μg/L 첨가시 유기물 첨가를 하지 않았을 때에 비하여 S. Typhimurium은 1.10 log<SUB>10</SUB>CFU/g, S. aureus는 0.8 log10CFU/g의 전해수 효과가 감소하였다. 들깻잎과 전해수의 처리비율은 1:10으로 처리하였을 때 미생물 저감효과는 S. Typhimurium 0.57 log10CFU/g, S. aureus 0.79 log10CFU/g로 전해수에 의한 미생물저감 효과를 기대하기 어려웠다. 따라서 들깻잎에서 S. Typhimurium과 S.aureus의 효과적인 제어를 위해서는 전해수 처리전에 물 세척을 통하여 흙과 먼지를 제거하고 전해수 농도 100 ppm에서 1분 이상 처리해야한다. 또한 들깻잎과 전해수 비율은 1:25 이상 유지 하는 것이 바람직할 것으로 사료된다. This study was conducted to evaluate the bactericidal activity of weakly alkalic electrolyzed water (WEW)against Salmonella Typhimurium and Staphylococcus aureus on perilla leaves. The influences of organic matter, inform of bovine serum, and the ratio of WEW to perilla leaves on bactericidal activity of WEW were also examined. Treatment of these organisms with 25, 50, 75, and 100 ppm WEW was performed for 1 min, 3 min and 5 min, respectively. Higher bactericidal activity was observed after a treatment with 100 ppm WEW compared to a treatment with 25 ppm WEW by 0.7 log<SUB>10</SUB>CFU/g. The bactericidal activity of WEW also decreased with increasing bovine serum concentration. At the ratio of 10:1 (WEW: perilla leave), levels of Salmonella Typhimurium and Staphylococcus aureus were only reduced by 0.57 and 0.79 log10CFU/g, respectively. It is suggested that the removal of organic debris prior to application of sanitizers and treatment above the ratio of 25:1 (WEW: perilla leave) is needed in order to improve WEW activity.
농산물과 토양에 대한 퍼클로레이트 함량 평가 및 생물농축계수 산출
김지영 ( Ji Young Kim ),김민지 ( Min Ji Kim ),이정미 ( Jeong Mi Lee ),김두호 ( Doo Ho Kim ),박기문 ( Ki Moon Park ),김원일 ( Won Il Kim ) 한국환경농학회 2013 한국환경농학회지 Vol.32 No.3
BACKGROUND: Perchlorate(ClO4 -) is an anion that is extremely water-soluble and environmentally stable. It mostly exists in the form of sodium perchlorate, ammonium perchlorate and potassium perchlorate which are used in rocket fuels, propellants, ignitable sources, air bag inflation systems and explosives. Perchlorate can be taken into the thyroid glands and interfere with iodide uptake. The determination of perchlorate in agricultural products is important due to its potential health impact on humans. The objective of this study was to determine the perchlorate concentrations in the samples of various agricultural products and soils. METHODS AND RESULTS: In this study, samples of cereal(Rice, Barley, Corn, Bean), vegetable(Spinach, Lettuce, Sesame, Chives, Chili, Pumpkin, Tomato), fruit(Apple, Pear, Tangerine, Grape) were analyzed for perchlorate contents. Perchlorate concentrations were analyzed by liquid chromatography-tandem mass spectrometry. The results showed that agricultural products respectively contained perchlorate concentrations in the range of : cereals N.D.∼7.46 μg/kg, vegetables 0.52∼23.06 μg/kg, fruits 0.19∼2.66 μg/kg. Bioconcentration factor was in the order of : vegetables > cereals > fruits. Bioconcentration factor was highest follwed by Sesame 37.88, Corn 21.51, Spinach 10.57, Tangerine 4.39, Chives 2.89 and Lettuce 1.90. The recoveries of perchlorate from spiked agricultural products and soils ranged from 87.72∼111.26% and 102.09∼111.23%. CONCLUSION(S): The health risk assessment results obtained in this study are lower than the RfD(Reference Dose, 0.0007 mg/kg/body weight/day) value as suggested by the Integrated Risk Information System(US IRIS). Our results indicate that, people currently exposed to perchlorate from agricultural products consumption are considered as safe.