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Duan, Mengying,Liu, Yidong,Ao, Jun,Xue, Lu,Luo, Shilong,Tan, Yu,Qin, Wenling,Song, Choong Eui,Yan, Hailong American Chemical Society 2017 ORGANIC LETTERS Vol.19 No.9
<P>A chiral, fluoride-catalyzed asymmetric cascade sulfaMichael/aldol condensation reaction of 1,4-dithiane-2,5-diol and a series of alpha,beta-unsaturated ketones is described to access chiral trisubstituted tetrahydrothiophene derivatives. The target products, including the spiro tetrahydrothiophene derivatives bearing a five-, six-, and seven-membered ring, were highly functionalized and showed high ee value. This established protocol realized a highly enantioselective reaction with a catalytic amount of KF and Song's chiral oligoEG via in situ generated chiral fluoride to construct useful heterocyclic skeletons with great complexity.</P>
Yijiong Liu,Juanqin Xue,Yinli Duan,Liang-Sheng Qiang,Jing Ma 한국섬유공학회 2019 Fibers and polymers Vol.20 No.9
In this study, Layer-by-layer (LbL) self-assembly technique was used to fabricate TiO2 films onto glass slides. Polyurethane (PU) was used as a substrate for the immobilization of TiO2, to increase the adsorption ability of thephotocatalyst. The LBL sequence was (PU/TiO2 NPs)n (n is the number of bilayers). These LbL hybrid films werecharacterized by Raman spectra, which confirmed the formation of TiO2 nanoparticles (TiO2 NPs) in the anatase phase withaverage size around 30 nm. The thickness of the film estimated around 1.1±0.2 μm as determined by scanning electronmicroscopy (SEM). UV-vis spectra confirmed the linear and regular growth of the films with the number of bilayers. Thephotocatalytic property of the films was investigated by the decomposition of methyl blue (MB) under UV-light irradiation. Furthermore, the reusability studies revealed that the fabricated film could be repeatedly used for up to six times withoutaffecting the photocatalytic activity. In addition, the corresponding mechanism of enhanced photocatalytic activity wasproposed on the basis of the investigated results from reactive species scavenging of (PU/TiO2 NPs)10. The active species h+played the most important role in the photocatalytic reaction. This work manifested that the LbL films can be handled moreeasily than TiO2 NPs in suspension form. Therefore, as-synthesized film is a promising candidate in wastewater treatmentapplication.
Yinli Duan,Jing Ma,Jiao Liu,Liang-Sheng Qiang,Juanqin Xue 한국섬유공학회 2020 Fibers and polymers Vol.21 No.4
In this paper, a facile and efficient method was performed to prepare the thermo-responsive Poly(Nisopropylacrylamide)/TiO2 (TiO2/PNIPAM) with the dispersing of TiO2 nanoparticles into PNIPAM. The structures ofnanoparticles and the grafted polymer were confirmed by X-ray diffraction (XRD), Raman spectra, Fourier transforminfrared spectra (FT-IR) and Dynamic Light Scattering (DLS). The interactions between the two components were studied byX-ray photoelectron spectroscopy (XPS), and the morphology of TiO2/PNIPAM was observed by scanning electronmicroscopy (SEM). The results showed that TiO2 exhibited homogeneous dispersion, without sacrificing the properties ofTiO2. Furthermore, The composite was used to photocatalytic degradation of Methylene blue (MB). The highest MB removalefficiency is 86.3 %. The photocatalytic activities above or below the lower critical solution temperature (LCST) of PNIPAMwas also investigated. The experiment results show that the existence of PNIPAM contributed not only the thermo-responsiveabilities to TiO2, but also the enhanced photocatalytic activities to TiO2. In addition, the corresponding mechanism ofenhanced photocatalytic activity was proposed. The results manifest that the well-designed TiO2/PNIPAM is a promisingcandidate in wastewater treatment application.
Vector Quantization Method Based on Satellite Cloud Image
Xumin Liu,Zilong Duan,Xue Yang,Weixiang Xu 보안공학연구지원센터 2015 International Journal of Signal Processing, Image Vol.8 No.11
Automatic vectorization in the field of image processing and recognition is one of development direction. This paper does some relevant researches on satellite cloud image preprocessing, image segmentation, image vector quantization. To improve the effect of noise reduction and preserving image details, this paper puts forward an improved adaptive median filter algorithm; For increasing the speed of image segmentation, this paper puts forward automatic layering algorithm combined with color information. Finally, this paper puts forward automatic vector quantization algorithm based on satellite cloud images and we developed an automatic vector quantization prototype system of satellite cloud images. The research results suggest that our automatic vector quantization algorithm has satellite cloud information automatic extraction function, identification function and vector quantization function.
Effects of Tissue Factor, PAR-2 and MMP-9 Expression on Human Breast Cancer Cell Line MCF-7 Invasion
Lin, Zeng-Mao,Zhao, Jian-Xin,Duan, Xue-Ning,Zhang, Lan-Bo,Ye, Jing-Ming,Xu, Ling,Liu, Yin-Hua Asian Pacific Journal of Cancer Prevention 2014 Asian Pacific journal of cancer prevention Vol.15 No.2
Objective: This study aimed to explore the expression of tissue factor (TF), protease activated receptor-2 (PAR-2), and matrix metalloproteinase-9 (MMP-9) in the MCF-7 breast cancer cell line and influence on invasiveness. Methods: Stable MCF-7 cells transfected with TF cDNA and with TF ShRNA were established. TF, PAR-2, and MMP-9 protein expression was analyzed using indirect immunofluorescence and invasiveness was evaluated using a cell invasion test. Effects of an exogenous PAR-2 agonist were also examined. Results: TF protein expression significantly differed between the TF cDNA and TF ShRNA groups. MMP-9 protein expression was significantly correlated with TF protein expression, but PAR-2 protein expression was unaffected. The PAR-2 agonist significantly enhanced MMP-9 expression and slightly increased TF and PAR-2 expression in the TF ShRNA group, but did not significantly affect protein expression in MCF-7 cells transfected with TF cDNA. TF and MMP-9 expression was positively correlated with the invasiveness of tumor cells. Conclusion: TF, PAR-2, and MMP-9 affect invasiveness of MCF-7 cells. TF may increase MMP-9 expression by activating PAR-2.
Jin-cheng Zhou,Qian-jin Dong,Tong-shu Zhang,Li-jia Duan,Su-fang Ning,Quanquan Liu,Yuan-yuan Li,Chun-xue Li,Hui Dong 한국응용곤충학회 2019 Journal of Asia-Pacific Entomology Vol.22 No.3
The efficacy of Trichogramma against pests basically depends on the dispersal capacity of the wasps. A releaserecapture method was used in this study to evaluate the effect of relative wind speed (RWS) during the nighttime and the daytime on the dispersal capacity of postrelease population of Trichogramma dendrolimi Matsumura. Two repeated measurements were carried out, using sentinel cards with the host eggs and yellow sticky card traps on the third and the sixth day after wasp release. The results showed that: (1) both the number of recaptured wasps and parasitized eggs increased with the RWS in the daytime during the first three days. The number of parasitized eggs also increased with the RWS in the daytime over the latter three days. The distances that encompassed 98% recaptured T. dendrolimi adults (X 98 ) at the first three days was quadratically increased by the RWS of the daytime. (2) The number of wasps recaptured decreased with the distance from the releasing point during the first three days, but it was not influenced by the distance from the releasing point during the latter three days. (3) The average dispersal radius of the wasps during the first three days was shorter than during the latter three days. The present results will be helpful to improve release techniques based on the wind effects at different times.