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      • 산소와 구리의 공정반응에 의한 구리와 알루미나의 직접접합

        이임렬,유환성 단국대학교 신소재기술연구소 1991 신소재 Vol.1 No.-

        본 연구에서는 구리표면의 구리-산소간의 공정반응에 의하여 형성된 Cu-Cu_2O 공용액상 피막으로 고체 Cu금속과 Al_2O_3세라믹을 압력없이 직접접합시키는 방법을 조사하였으며 접합조건에 따른 접합특성, 파면 및 계면분석을 SEM, EDS, XRD 및 peeling 시험을 통하여 분석하였다. 1.5×10^-1 torr 진공하에서 1015℃의 온도에서 산화시킨 구리시편은 미세한 산화물 Cu_2O가 표면에 잘 형성되었다. 그후 공정온도 1065℃ 이상의 접합온도 1075℃에서 5분간 10^-3 torr의 진공하에서 직접접합시킨 시편은 접합력이 우수한 Cu/Al_2O_3 접합이 되었으며 접합후 구리기니 내에는 Cu2O가 석출된 공융조직을 갖고 있었다. 3분 산화조건에서 충분한 액상이 형성되어 29kg의 최대 접합강도를 보였으며 산회시간이 이보다 짧거나 불충분한 액상의 형성이나 산화물내의 균열 등으로 결합력이 저하하였다. 파단후 Al_2O_3 표면에는 Cu_2O nodule이 존재하였고 Cu족에는 nodule이 빠진홈을 관찰할 수 있었는바 cu2O/Al_2O_3계면 접착력은 Cu.Cu_2O계면보다 강함을 알 수 있었다. 또한 파단면에는 반응 생성물 CuAlO_2가 접합중 형성되었으나 이 반응층 두께는 SEM분해능 이하인 매우 얇은 것으로 생각된다. The direct bonding between Cu and Al_2O_3, utilizing Cu-Cu_2O skin melt formed on Cu surface by eutectic reation of Cu-O, is investigated in this study. The bond strength, fracture surface and interface structure with bonding conditions have been studied using SEM, EDS, XRD and peeling test. A fine Cu_2O is formed on the surface of Cu with oxidation at 1015℃ under 1.5×10^-1torr vacuum. After oxidation, the bonded specimen conducted at 1075℃ in 10^-3torr vacuum for 5minutes, higher temperature than its eutectic temperature of 1065℃, has a good strength having a Cu_2O precipitated structure in Cu matrix upon cooling. It has been found that the maximum bonding force of 29kg is obtatined for 3 minutes of oxidation. However, the adhesion forces are decreased with shorter or longer oxidation than this due to the formation of insufficient liquid skin or crack within oxide. After peeling test, Al_2O_3 surface is covered with Cu_2O nodules which are pulled out of Cu surface indication that Cu_2O/Al_2O_3 adhesion force is stronger than that of Cu/Cu_2O. Moreover a reaction phase of CuAlO_2, thought to be very thin layer below the resolution of SEM, is also formed during the bonding process.

      • 冷間加工의 磨耗에 對한 影響

        李任烈 단국대학교 1986 論文集 Vol.20 No.-

        The wear experiment was conducted on couples consisting of iron, nickel, Fe-36% Ni and 3% silicon steel pins sliding against a tool steel disc. It has been found that the wear rate in air at room temperature lis independent to me hardness. The experimental observations are well related to the oxidation characteristics. However, the rate of oxidative wear is much higher than that for static oxidation due to the difference in the activation energy for oxidative wear. The lower energy for oxidational wear indicates that the rubbing surfaces are mechanically activated and high diffusivity path for diffusion of matrix elements and oxygen are produced during the sliding motion. The higher wear rate for cold-worked samples than for the annealed ones are associated with the higher oxidation rate for the cold-worked specimen.

      • SCIESCOPUS

        Role of protein kinase C-dependent A-kinase anchoring proteins in lysophosphatidic acid-induced cAMP signaling in human diploid fibroblasts

        Rhim, Ji-Heon,Jang, Ik-Soon,Yeo, Eui-Ju,Song, Kye-Yong,Park, Sang Chul BLACKWELL PUBLISHING 2006 AGING CELL Vol.5 No.6

        <P>Summary</P><P>Previously, we reported that lysophosphatidic acid (LPA)-induced adenosine 3′,5′-cyclic monophosphate (cAMP) production by human diploid fibroblasts depends on the age of the fibroblasts. In this study, we examined the role of A-kinase <I>a</I>nchoring proteins (AKAP) in the regulation of LPA-stimulated cAMP production in senescent fibroblasts. We found that levels of protein kinase C (PKC)-dependent AKAPs, such as Gravin and AKAP79, were elevated in senescent cells. Co-immunoprecipitation experiments revealed that Gravin and AKAP79 do not associate with adenylyl cyclase type 2 (AC2) but bind to AC4/6, which interacts with calcium-dependent PKCs α/&bgr; both in young and senescent fibroblasts. When the expression of Gravin and AKAP79 was blocked by small interference RNA transfection, the basal level of cAMP was greatly reduced and the cAMP status after LPA treatment was also reversed. Protein kinase A showed a similar pattern in terms of its basal activity and LPA-dependent modulation. These data suggest that Gravin and to a lesser extent, AKAP79, may play important roles in maintaining the basal AC activity and in coupling the AC systems to inhibitory signals such as Giα in young cells, and to stimulatory signals such as PKCs in senescent cells. This study also demonstrates that Gravin is especially important for the long-term activation of PKC by LPA in senescent cells. We conclude that LPA-dependent increased level of cAMP in senescent human diploid fibroblasts is associated with increases in Gravin levels resulting in its increased binding with and activation of calcium-dependent PKC α/&bgr; and AC4/6.</P>

      • Shear Strength of the Perfobond Connection of a Steel-Concrete Composite Slim Floor System

        Rhim, Hong C.,Lee, Kwang Ho,Jang, Won Seok,Jeong, Seong Hoon,Kim, Dae Jin,Park, Jong Hwan Trans Tech Publications, Ltd. 2015 Applied Mechanics and Materials Vol. No.

        <P>The use of steel-concrete composite members has been significantly increased as they have the advantages of the reduction of cross sectional areas, excellent ductility against earthquake loadings and a longer life span than typical steel frame members. In this paper, push-out tests were performed on six specimens to investigate the structural behavior and shear strength of perfobond connection of a steel-concrete composite slim floor system. An equation to theoretically estimate the shear strength of the perfobond connection is proposed, and its accuracy is examined by comparing its predictions with the test results. A finite element analysis model is also developed and used to confirm the effectiveness of the proposed strength equation.</P>

      • Cryopreservation induces macrophage colony stimulating factor from human periodontal ligament cells in vitro

        Rhim, E.M.,Ahn, S.J.,Kim, J.Y.,Chang, Y.R.,Kim, K.H.,Lee, H.W.,Jung, S.H.,Kim, E.C.,Park, S.H. Academic Press 2013 Cryobiology Vol.67 No.2

        Cryopreservation is used to protect vital periodontal ligaments during the transplantation of teeth. We investigated which gene products implicated in root resorption are upregulated in human periodontal ligament cells by cryopreservation, and whether cryopreservation affects the expression of macrophage-colony stimulating factor (M-CSF) in human periodontal ligament cells. We used customized microarrays to compare gene expression in human periodontal ligament cells cultured from teeth immediately after extraction and from cryopreserved teeth. Based on the result of these assays, we examined M-CSF expression in periodontal ligament cells from the immediately extracted tooth and cryopreserved teeth by real-time PCR, enzyme-linked immunosorbent assay (ELISA), Western blot analysis, and immunofluorescence. We also investigated whether human bone marrow cells differentiate into tartrate-resistant acid phosphatase (TRAP) positive osteoclasts when stimulated with RANKL (Receptor Activator for Nuclear Factor κ B Ligand) together with any secreted M-CSF present in the supernatants of the periodontal ligament cells cultured from the various groups of teeth. M-CSF was twofold higher in the periodontal ligament cells from the rapid freezing teeth than in those from the immediately extracted group (p<0.05). Cryopreservation increased M-CSF expression in the periodontal ligament cells when analyzed by real time PCR, ELISA, Western blotting, and immunofluorescence (p<0.05). TRAP positive osteoclasts were formed in response to RANKL and the secreted M-CSF present in the supernatants of all the experimental groups except negative control. These results demonstrate that cryopreservation promotes the production of M-CSF, which plays an important role in root resorption by periodontal ligament cells.

      • SCOPUSKCI등재

        Aging Effect of Poly(vinyl alcohol) Membranes Crosslinked with Poly(acrylic acid-co-maleic acid)

        Rhim Ji Won,Hwang Ho Sang,Kim Dae Sik,Park Ho Bum,Lee Chang Hyun,Lee Young Moo,Moon Go Young,Nam Sang Yong The Polymer Society of Korea 2005 Macromolecular Research Vol.13 No.2

        Poly(vinyl alcohol) (PVA) membranes crosslinked with poly(acrylic acid-co-maleic acid) (PAM) were prepared to investigate the effect of aging on their morphology by swelling them for up to 7 days. PAM was used both as a crosslinking agent and as a donor of the hydrophilic-COOH group. A $30 wt\%$ weight loss of the dry membrane was observed in the swelling test after 6 days. The surface of the membrane was dramatically changed after the swelling test. The surface roughness of the PVA/PAM membrane was increased, as determined by atomic force microscopy (AFM). The swelling loosened the polymer structure, due to the release of the unreacted polymer and the decomposition of the ester bond, thereby resulting in an increase in the free volume capable of containing water molecules. The water molecules present in the form of free water were determined by differential scanning calorimetry (DSC). The fraction of free water increased with increasing swelling time. The swelling of the membrane may provide space for the transport of protons and increase the mobility of the protonic charge carriers. The proton conductivity of the membranes measured at T= 30 and $50^{\circ}C$ was in the range of $10^{-3} to 10^{-2} S/cm$, and slightly increased with increasing swelling time and temperature.

      • KCI등재

        Characteristics of Breeding Bird Communities in Mt. Namsan, Seoul, Korea

        Rhim, Shin-Jae,Lee, Ju-Young,Kang, Jeong-Hoon Korean Society of Forest Science 2006 한국산림과학회지 Vol.95 No.5

        This study was conducted to clarify the characteristics of breeding bird communities between deciduous and coniferous forests from April to June 2005 in Mt. Namsan, Seoul, Korea. Two 10ha areas were selected for territory mapping of breeding bird communities. Number of breeding bird species, pairs,density and bird species diversity index were higher in deciduous forest with increasing amount of foliage in the forest profile or as forest structures developed compared with coniferous forest. The number of in coniferous forest. The differences in habitat structure between both study areas are very likely to have influenced how breeding birds used the available habitat. Forest structure and its interactions with birds should be consideration in forest management for birds and their habitat.

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