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Large-Pore Apertures in a Series of Metal-Organic Frameworks
Deng, H.,Grunder, S.,Cordova, K. E.,Valente, C.,Furukawa, H.,Hmadeh, M.,Gandara, F.,Whalley, A. C.,Liu, Z.,Asahina, S.,Kazumori, H.,O'Keeffe, M.,Terasaki, O.,Stoddart, J. F.,Yaghi, O. M. American Association for the Advancement of Scienc 2012 Science Vol.336 No.6084
<P>We report a strategy to expand the pore aperture of metal-organic frameworks (MOFs) into a previously unattained size regime (>32 angstroms). Specifically, the systematic expansion of a well-known MOF structure, MOF-74, from its original link of one phenylene ring (I) to two, three, four, five, six, seven, nine, and eleven (II to XI, respectively), afforded an isoreticular series of MOF-74 structures (termed IRMOF-74-I to XI) with pore apertures ranging from 14 to 98 angstroms. All members of this series have noninterpenetrating structures and exhibit robust architectures, as evidenced by their permanent porosity and high thermal stability (up to 300C). The pore apertures of an oligoethylene glycol-functionalized IRMOF-74-VII and IRMOF-74-IX are large enough for natural proteins to enter the pores.</P>
Dynamic PID Gain Changing Control for DC-DC Converter
Y. Furukawa,D. Mitsutake,T. Shirakawa,H. Maruta,F. Kurokawa 전력전자학회 2015 ICPE(ISPE)논문집 Vol.2015 No.6
This paper presents a digital control method where changes PID parameter setting dynamically to improve transient characteristics of dc-dc converters. In the conventional PID control, those control parameters are selected as suitable values to satisfy stable characteristics both in transient state and steady state and keep the stability of system. Therefore, the value of control parameter tends to be a small one. In this paper, we propose the method where the PID parameter setting is changed to the suitable one in the transient state, where the value of control parameter is designed just to improve the transient response and takes larger one compared to the conventional PID control method. Using the proposed method, the transient response can be improved without the loss of stability of dc-dc converter.
Tumor Imaging by Monoclonal Antibodies Labeled with Radioactive Metal Ions
( K. Endo ),( H. Sakahara ),( T. Nakashima ),( M. Koizumi ),( M. Kunimastsu ),( H. Ohta ),( T. Furukawa ),( Y. Ohmomo ),( Y. Arano ),( A. Yokoyama ),( K. Okada ),( O. Yoshida ),( S. Hosoi ),( T’ Nakam 대한핵의학회 1984 핵의학 분자영상 Vol.18 No.2
Nguyen, Nhung T. T.,Lo, Tien N. H.,Kim, Jaheon,Nguyen, Huong T. D.,Le, Toan B.,Cordova, Kyle E.,Furukawa, Hiroyasu American Chemical Society 2016 Inorganic Chemistry Vol.55 No.12
<P>A presynthesized, square planar copper imidazole complex, [Cu(imidazole)(4)](NO3)(2), was utilized as a precursor in the synthesis of a new series of zeolitic imidazolate frameworks, termed ZIF-202, -203, and -204. The structures of all three members were solved by single-crystal X-ray diffraction analysis, which revealed ZIF-203 and -204 having successfully integrated square planar units within the backbones of their respective frameworks. As a result of this unit, the structures of both ZIF-203 and -204 were found to adopt unprecedented three-dimensional nets, namely, ntn and thl, respectively. One member of this series, ZIF-204, was demonstrated to be highly porous, exhibit exceptional stability in water, and selectively capture CO2 over CH4 under both dry and wet conditions without any loss in performance over three cycles. Remarkably, the regeneration of ZIF-204 was performed under the mild conditions of flowing a pure N-2 gas through the material at ambient temperature.</P>