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      • SCOPUSKCI등재

        Synthesis, Characterization and Antimicrobial Activities of Hydrazone Ligands Derived from 2-(phenylamino)acetohydrazide and Their Metal Complexes

        EL-Saied, F.A.,Shakdofa, M.M.E.,Al-Hakimi, A.N. Korean Chemical Society 2011 대한화학회지 Vol.55 No.3

        N'-(2-hydroxybenzyl)-2-(phenylamino)acetohydrazide ($H_2L^1$, 1) 및 N'-((3-hydroxy-naphthalen-2-yl)methylene)-2-(phenylamino)acetohydrazide ($H_2L^2$, 13)에 대한 VO(II), ZrO(II), Hf(IV), $UO_2$(II), Sn(II), V(V)$O_3$, Ru(III), Cd(II), Ho(III) 및 Yb(III) 착물을 합성하여 원소분석, $^1H$ NMR, IR, UV-Vis, 전기전도도 및 열분석 (DTA 및 TG)을 통해 특성을 조사하였다. 이들 리간드는 분광학적 결과에 의하면 중성 이배위, 일염기성 이배위, 일열기성 삼배위 또는 이염기성 삼배위 리간드로 행동한다. 그 결과 azomethine 질소원자, 양성자화 되어있거나 또는 탈양성자화 된 형태의 페놀 하이드록시 그룹 그리고 에놀 또는 케톤형 카드보닐 그룹을 통해 금속이온에 결합한다. 이들 리간드와 그 금속 착물들은 모체 리간드 및 금속이온 용액에 비해 높은 항균 및 항박테리아 저해효과를 보인다. 대부분의 금속 착물은 표준 항균성 시약 (amphotricene B) 보다 더 높은 항균 활동성을 보인다. 또한 이들 리간드와 착물은 항박테리아 활성도보다는 항균활성도에서 더 높은 수치를 보인다. VO(II), ZrO(II), Hf(IV), $UO_2$(II), Sn(II), V(V)$O_3$, Ru(III), Cd(II), Ho(III) and Yb(III) complexes of N'-(2-hydroxybenzyl)-2-(phenylamino)acetohydrazide ($H_2L^1$, 1) and N'-((3-hydroxy-naphthalen-2-yl)methylene)-2-(phenylamino)-acetohydrazide ($H_2L^2$, 13) have been synthesized and characterized by elemental analyses, $^1H$ NMR, IR, UV-Vis, conductance, thermal analyses (DTA and TG). The spectral data showed that the ligands behave as neutral bidentate, monobasic bidentate, monobasic tridentate or bibasic tridentate ligand bonded to the metal ions through the azomethine nitrogen atoms, phenolic hydroxyl group in protonated or deprotonated form and enolic or ketonic carbonyl group. The ligands and their metal complexes exhibit higher antifungal and antibacterial inhibitory effects than parent ligands and the solution of metal ions. Most of metal complexes exhibit higher antifungal activity than standard antifungal drug (amphotricene B). It is also clear that the ligands and their metal complexes have higher antifungal activity than antibacterial activity.

      • KCI등재

        Production of Smart Cotton-nickel Blend Fibers Using Functional Polymers Comprising Ammonium Polyphosphate and Silicone Rubber

        Mehrez E. El-Naggar,Ola A. Abu Ali,Dalia I. Saleh,K. M. Abu-alnja,Abd-allah M. Mnsour,Mohammed A. Abu-Saied,Tawfik A. Khattab 한국섬유공학회 2022 Fibers and polymers Vol.23 No.6

        Despite the fact that Pyrovatex is widely used as a commercial flame-retardant, the release of toxic formaldehyderemains a serious problem. Fluorine-based compounds, on the other hand, have been employed to impart hydrophobic textilesurfaces, although they are exceedingly costly and poisonous. Based on those difficulties, we describe a simple one-stepmethod for coating electrically conductive cotton-nickel (Cot-Ni) blend fabric providing flame-retardant and water-repellentcharacteristics. A nickel ribbon was firstly bent around a cotton yarn as a core, and then woven into an electrically conductiveCot-Ni blend fabric, which was created by weaving the cotton-nikel hybrid threads with regular cotton yarns. The conductivefabric was coated with a composite consisting of silicone rubber (RTV) and ammonium polyphosphate (APP). The strongbinding of RTV with both APP and cotton fibres increased the flame-retardant action of cotton, according to the findings. Asa result, varied concentrations of APP were used in the composite to show that only 100 g/l of APP combined with RTVimproved the fire-retardancy. Depending on the concentration of APP, distinct hierarchical morphologies appeared on thesurface of the coated Cot-Ni fabrics. RTV also improved the hydrophobic character of the blend surface. Measurements of airpermeability, surface roughness, and stiffness were used to investigate the comfort qualities of the coated Cot-Ni blends. Eventually, those multifunctional (Cot-Ni)/RTV-APP textiles might be used in a variety of applications, such as grain storagecontainers, car seat mats, and firefighters' uniforms.

      • SCIESCOPUSKCI등재
      • KCI등재

        Regenerative Strategies in Treatment of Peripheral Nerve Injuries in Different Animal Models

        Khaled Mona M,Ibrahium Asmaa M,Abdelgalil Ahmed I,El-Saied Mohamed A.,El-Bably Samah H 한국조직공학과 재생의학회 2023 조직공학과 재생의학 Vol.20 No.6

        BACKGROUND: Peripheral nerve damage mainly resulted from traumatic or infectious causes; the main signs of a damaged nerve are the loss of sensory and/or motor functions. The injured nerve has limited regenerative capacity and is recovered by the body itself, the recovery process depends on the severity of damage to the nerve, nowadays the use of stem cells is one of the new and advanced methods for treatment of these problems. METHOD: Following our review, data are collected from different databases ‘‘Google scholar, Springer, Elsevier, Egyptian Knowledge Bank, and PubMed’’ using different keywords such as Peripheral nerve damage, Radial Nerve, Sciatic Nerve, Animals, Nerve regeneration, and Stem cell to investigate the different methods taken in consideration for regeneration of PNI. RESULT: This review contains tables illustrating all forms and types of regenerative medicine used in treatment of peripheral nerve injuries (PNI) including different types of stem cells ‘‘ adipose-derived stem cells, bone marrow stem cells, Human umbilical cord stem cells, embryonic stem cells’’ and their effect on re-constitution and functional recovery of the damaged nerve which evaluated by physical, histological, Immuno-histochemical, biochemical evaluation, and the review illuminated the best regenerative strategies help in rapid peripheral nerve regeneration in different animal models included horse, dog, cat, sheep, monkey, pig, mice and rat. CONCLUSION: Old surgical attempts such as neurorrhaphy, autogenic nerve transplantation, and Schwann cell implantation have a limited power of recovery in cases of large nerve defects. Stem cell therapy including mesenchymal stromal cells has a high potential differentiation capacity to renew and form a new nerve and also restore its function.

      • KCI등재

        Optimization of Reservoir Operation using New Hybrid Algorithm

        Zaher Mundher Yaseen,Hojat Karami,Mohammad Ehteram,Nuruol Syuhadaa Mohd,Sayed Farhad Mousavi,Lai Sai Hin,Ozgur Kisi,Saeed Farzin,김성원,Ahmed El-Shafie 대한토목학회 2018 KSCE JOURNAL OF CIVIL ENGINEERING Vol.22 No.11

        Due to the scarcity of fresh water resources, exploiting dams’ reservoirs, based on their optimal operation, obviates construction of extra dams and high costs and satisfies downstream consumers’ water needs with high reliability. In this research, a new hybrid approach of Artificial Fish Swarm Algorithm (AFSA) and Particle Swarm Optimization Algorithm (PSOA) is used to optimize Karun-4 reservoir, increase energy production and minimize downstream water shortages. This Hybrid Algorithm (HA) brings about diversity of responses in PSOA, prevents entrapment of AFSA in local optimum traps and increases convergence speed and balances between the abilities to scan and make profit in the AFSA. This method was assessed based on reliability, vulnerability and resilience indices. In addition, based on a multi-criteria decision-making model, it was evaluated by comparing it with other evolutionary algorithms. To verify the HA, it was tested on few mathematical functions. Results indicated that the HA features performed higher reliability, lower vulnerability and resiliency, as compared with AFSA and PSOA. In addition, HA is ranked first according to the multi criteria decision making model. Further, among all the tested evolutionary methods, this new algorithm yielded the best answer for dam power plant’s objective function.

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