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위인희,신동욱,한규성,김진호,조우석,황광택,Wi, In-Hee,Shin, Dong-Wook,Han, Kyu-Sung,Kim, Jin-Ho,Cho, Woo-Seok,Hwang, Kwang-Taek 한국세라믹학회 2014 한국세라믹학회지 Vol.51 No.4
A single layer ultrafiltration(UF) ceramic membrane was prepared using boehmite sol. Boehmite was synthesized using a typical sol-gel process with optimization of the viscosity, pH, molar ratio of aluminum isopropoxide(AIP) and $HNO_3$. Boehmite sol was coated on a microfiltration(MF) support using the dip-coating method. MF support was dipped into the boehmite sol with a withdrawal speed of 5 mm/s and was maintained for 10 s in the boehmite sol, resulting in a uniform UF membrane layer of $10{\mu}m$ thickness. The porosity of the obtained membrane was measured and found to be 41.2%; the pore size was found to range from 80~100 nm, corresponding to the pore size of the UF membrane. The flux of the obtained membrane was initially 540 $L/m^2h$ and approximately 85% of the initial flux was recovered using a periodic back-flushing process.
위인희,신동욱,한규성,김진호,조우석,황광택,Wi, In-Hee,Shin, Dong-Wook,Han, Kyu-Sung,Kim, Jin-Ho,Cho, Woo-Seok,Hwang, Kwang-Taek 한국세라믹학회 2014 한국세라믹학회지 Vol.51 No.4
A non-electric water purification system using the Korean traditional ceramic ware Onggi, was demonstrated as an appropriate technology to solve water shortages in under developed regions. Generally, Onggi is produced using large size raw materials that are sintered at low temperature, resulting in a porous body that shows air and water permeability. An Onggi filter was prepared using a spinning wheel with the addition of rice bran to the body to increase porosity. The porosity of the obtained Onggi filter was 25.1%; the water permeability was 85.1 $L/m^2h$. Turbidity and TDS of the purified water using Onggi filter were decreased by 97.7% and 29.1%, respectively.
박영수,위인희,조우석,김진호,황광택,Park, Young-Soo,Wui, In-Hee,Cho, Woo-Seok,Kim, Jin-Ho,Hwang, Kwang-Taek 한국결정성장학회 2012 한국결정성장학회지 Vol.22 No.6
알루미늄 에칭 폐액으로부터 boehmite(AlOOH) 분말을 합성하였다. 폐액에서 침전되어 있는 결정상은 gibbsite ($Al(OH)_3$)였으며, 산을 이용하여 pH를 조절한 결과 pH가 7~8 영역에서 boehmite 결정상이 얻어졌다. 침전 분말에 남아 있는 Na 이온을 제거하고자 세척공정을 진행하여 boehmite 분말을 얻었다. 합성한 분말의 평균입경은 약 40 nm이었다. 또한 열처리 온도가 증가함에 따라 boehmite는 ${\gamma}-Al_2O_3$와 ${\delta}-Al_2O_3$, ${\Theta}-Al_2O_3$를 거쳐 ${\alpha}-Al_2O_3$ 결정상으로 상전이가 일어났다. Boehmite (AlOOH) powder was synthesized using waste aluminium etching solution. In waste solution, precipitated phase was gibbsite ($Al(OH)_3$), and boehmite (AlOOH) phase was obtained at pH of 7 and 8 controlled by addition of acid. Boehmite powder was obtained by washing process to remove the Na ion in precipitated solution. Mean particle size of obtained powder was 40 nm. Boehmite phase transformed to ${\alpha}-Al_2O_3$ phase via ${\gamma}-Al_2O_3$, ${\delta}-Al_2O_3$, and ${\Theta}-Al_2O_3$.