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김광호(Gwang-Ho Kim),이민구(Min-Ku Lee),김경호(Kyeong-Ho Kim),김흥회(Whung-Whoe Kim),이창규(Chang-Kyu Rhee),김길무(Gil-Mu Kim) 한국표면공학회 2006 한국표면공학회지 Vol.39 No.2
In this study, the movable flame hardening process of 12Cr steel for a uniform hardness and desirable residual stress have been investigated. For this, the temperature cycles have been controlled accurately as a function of the three processing variables, the flame intensity If, the scanning velocity Vs and the initial flame holding time th, where the standard surface temperature Ts, max was maintained at 960°C. The optimized conditions were Vs = 0.68 ㎜/s and th = 67 sec for the C₃H?:O₂ = 5:20 l/min, Vs = 0.80 ㎜/s and th= 56 sec for the C₃H?:O₂ = 6:24 l/min, Vs = 1.01 ㎜/s and th= 48 sec for the C₃H?:O₂= 7:28 l/min, and Vs = 1.15 ㎜/s and th= 39 sec for the C₃H?:O₂= 8:32 l/min. The optimally flame-hardened surface exhibited uniform distributions of the hardness and residual compressive stress over the treated area with moderate levels of 470~490HV0.2 in hardness and ?300~?450 MPa in residual stress, which were acceptable on the basis of the acceptance criteria of Siemens AG-KWU and GE Power Generation Engineering.
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김봉구,황성식,양명승,김길무,김종집,Kim, Bong-Gu,Hwang, Seong-Sik,Yang, Myeong-Seung,Kim, Gil-Mu,Kim, Jong-Jip 한국재료학회 1994 한국재료학회지 Vol.4 No.6
합금원소(Cr, V, Si. Mo, Nb)가 첨가된 TiAi 금속간화합물의 고온 산화거동을 대기중의 900~$1100^{\circ}C$에서 관찰하였다. 산화반응물은 XRD, SEM, WDX을 이용하여 분석하였다. 등온 산화에 있어서 Cr과 V이 각각 첨가된 시편은 무게증가가 많았으나, Si, Mo, Vb가 각각 첨가된 시편은 상대적으로 무게증가각 적었아. 그리고, Cr과 V이 각각 첨가된 시편의 산화속도는 TiAi의 그것보다 항상 크게 나타났으며, Si, Mo, Vb가 각각 첨가된 시편의 산화속도는 TiAi의 그것보다 향상되지 않고, Si, Mo또는 Nb 첨가는 내산화성을 향상시킨다. Si, Mo, Nb이 각각 첨가된 TiAI합금표면에 형성된 산화물은 보호막 역할을 함으로 산소와 합금원소의 확산을 감소시키는 역할을 하였다. 특히, Nb는 산화의 초기단계에서는 $AI_{2}O_{3}$를 형성하려는 경향이 강하기 때문에 연속적인 $AI_{2}O_{3}$층과 조밀한 $Tio_{2}+AI_{2}O_{3}$ 혼합층이 형성되었다. Nb가 첨가된 합금의 백금 marker 실험결과에 따르면, 산소가 주로 합금내부로 확산하여 합금표면에서 산화물을 형성하였다. $900^{\circ}C$에서의 열반복주기(thermal cyclic)산화실험 결과, 다른 합금원소와 비교해 볼 때 Cr또는 Nb첨가가 금속기지와 산화층간의 접착력을 향상시키는 것으로 나타났다. Oxidation behaviour of TiAl intermetallic compounds with the addition of Cr, V, Si, Mo, or Nb was investigated at 900~$1100^{\circ}C$ under the atmospheric environment. The reaction products were examined by XRD, SEM equipped with WDX. The weight gain by continuous oxidation increased with the addition of Cr or V, but there was less weight gain when Mo, Si or Nb was added individually. he oxidation rate of Cr- or V-added TiAl was always larger than that of TiAI. However, oxidation rate of Si-, Mo- or Nb-added TiAl was almost same or smaller than that of TiAI. Thus, it is concluded that the addition of Cr or V did not improve the oxidation resistance, whereas the addition of Si, Mo or Nb improved the oxidation resistance. Oxides formed on TiAl with Mo, Si, and Nb were found to be more protective, resulting from the decrease in diffusion rate of the alloying elements and oxygen. Nb strengthened the tendency to form $AI_{2}O_{3}$ in the early stage of oxidation, due to the continuous $AI_{2}O_{3}$ layer formation and dense $Tio_{2}+AI_{2}O_{3}$ layer. According to the Pt-marker test of TiAI- 5wt%Nb, oxygen diffused mainly inward while oxides were formed on the substrate surface. Upon thermal cyclic oxidation at $900^{\circ}C$, it is shown that the addition of Cr or Nb improved the adherence of oxide scale to the substrate.
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고속 중성자 조사에 의한 원자로 용기재료내의 결함생성이 자기적 특성변화에 미치는 영향
정명모,김길수,장기상,유근배,박덕근,김길무,윤인섭,홍치유,Jeong, Myeong-Mo,Kim, Gil-Su,Jang, Gi-Sang,Yu, Geun-Bae,Park, Deok-Geun,Kim, Gil-Mu,Yun, In-Seop,Hong, Chi-Yu 한국재료학회 1999 한국재료학회지 Vol.9 No.12
In order to assess the effects on the magnetic properties due to the defect in the material irradiated by fast neutron ranging $10^0-10^{18}n/cm^2$, the magnetic properties such as maximum magnetic induction, coercivity, remanence, Barkhausen Noise Amplitude(BNA), Barkhausen Noise Energy(BNE) and hardness were measured. It is shown that the magnetic properties and hardness do not change by the fast neutron irradiation under $10^{17}n/cm^2$. Therefore, in this experiment, it is understood that the magnetic properties decrease by the increase of hardness. This measurement method can be used to evaluate the neutron irradiation embrittlement nondestructively since the magnetic properties and hardness do change by the neutron irradiation over $10^{17}n/cm^2$ consistently. 고속중성자가 조사된 재료내에 생성된 결함이 자기적 특성에 미치는 영향을 평가하기 위해서, 대기압, $70^{\circ}C$에서 고속 중성자(조사량 : $10^0-10^{18}n/cm^2$, E>1 MeV)가 조사된 원자로 용기강재의 자기적 성질(최대 자기유도, 보자력, 잔류자기, Barkhausen noise amplitude (BNA), Barkhausen noise energy (BNE)) 및 경도를 측정하였다. $10^{17}n/cm^2$ 이하의 고속 중성자 조사에서 자기적 특성 및 경도의 변화는 없는 것으로 나타났으나, $10^{17}n/cm^2$ 이상 조사에서는 최대 자기유도, 보자력, 잔류자기, BNA, BNE는 감소하고, 경도는 증가하는 것으로 나타났다. 따라서 경도 증가에 따라 자기적 특성은 감소하는 것을 알 수 있었으며, 측정된 요소들이 전부 $10^{17}n/cm^2$ 이상에서 변화를 보이고 있어 실험결과는 일관성이 있어, 이 방법을 이용하여 중성자 조사취화를 비파괴적으로 평가할 수 있음을 알 수 있었다.
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12Cr 강의 화염경화 표면처리 층의 초음속 물방울 충격에 의한 손상 거동
김광호,이민구,김경호,김흥회,김길무 대한금속재료학회 2005 대한금속·재료학회지 Vol.43 No.1
Water drop impact erosion properties of the 12Cr steel, currently used as nuclear steam turbine blade material, surface-hardened by the flame hardening process have been characterized. For this, variations of both the maximum erosion depth de,,,,ax and volume loss V with the cumulative impacts n at the supersonic impact velocity (~350 m/s) have been investigated for the as-received and flame-hardened 12Cr steels with different hardnesses. Typically all the samples showed an erosion-time characteristic involving the incubation period initially followed by the steady state period. It is also found that the d_(e,max) increases stepwise-like with the number of impacts n, which results from a sudden formation of craters by crack propagation. Compared to those for the as-received 12Cr steel, the flame-hardened ones showed an excellent resistance to water drop impact erosion with 2.2~2.8 times higher incubation time n, and 115~1/8 times lower erosion rate a. In the incubation period the as-received 12Cr steel was damaged by ductile depression and ploughing, while the flame-hardened 12Cr steel by fatigue cracks and brittle platelet deformation. Erosion in the steady state period was developed by the cleavage fracture commonly. (Received July 22, 2004)
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