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Ha Huu Do,Ha Huu Do,Wenwu Guo,Mahider Tekalne,Quyet Van Le,Thang Phan Nguyen,Jin Hyuk Cho,Sang Hyun Ahn,Soo Young Kim 대한금속·재료학회 2022 ELECTRONIC MATERIALS LETTERS Vol.18 No.1
Reversible metal electrodeposition (RME) windows are a promising material for electrochromic windows and electronic display applications. However, the lifetime of RME devices is a major drawback in the preparation of commercial and practical devices. In this study, we propose a new strategy to prolong the stability and improve the efficiency of RME devices. By using tungsten oxide, a well-known electrochromic material, to modify the surface of a transparent conductive electrode, superior, stable, and highly effective devices were prepared successfully. By applying a low potential of − 0.8 V to 0.5 V, the RME device can quickly switch between a bleached state and colored state with different colors changing from transparent to black and deep blue. The performance improvement of the RME device can be explained by the simultaneous reduction of tungsten oxide and metal ion deposition in the conductive substrate under an applied potential. Furthermore, the lifetime of the device increased significantly (over 1500 cycles) owing to the shielding role of tungsten oxide film in the acid medium, which is an indispensable component of reversible electrochromic devices.
Recent progress of two-dimensional materials and metal–organic framework-based taste sensors
HASANI AMIRHOSSEIN,Do Ha Huu,Tekalgne Mahider,홍성현,장호원,김수영 한국세라믹학회 2020 한국세라믹학회지 Vol.57 No.4
In food industries, the detection of diff erent tastes in low level is required to enhance the quality of products. Recently, 2-D materials and metal–organic framework (MOF) have attracted extensive attention owing to their unique properties, and they can be used in various applications, especially chemical and biochemical sensing. In this review, we investigate the recent progress of the 2-D materials and MOF in the taste sensing applications. From the review, we could conclude that these materials would be promising candidates for taste sensing applications, thereby leading to the development of food industry.
WS2–WC–WO3 nano-hollow spheres as an efficient and durable catalyst for hydrogen evolution reaction
Van Nguyen Tuan,Do Ha Huu,Tekalgne Mahider,Van Le Quyet,Nguyen Thang Phan,Hong Sung Hyun,Cho Jin Hyuk,Van Dao Dung,Ahn Sang Hyun,Kim Soo Young 나노기술연구협의회 2021 Nano Convergence Vol.8 No.28
Transition metal dichalcogenides (TMDs), transition metal carbides (TMCs), and transition metal oxides (TMOs) have been widely investigated for electrocatalytic applications owing to their abundant active sites, high stability, good conductivity, and various other fascinating properties. Therefore, the synthesis of composites of TMDs, TMCs, and TMOs is a new avenue for the preparation of efficient electrocatalysts. Herein, we propose a novel low-cost and facile method to prepare TMD–TMC–TMO nano-hollow spheres (WS 2 –WC–WO 3 NH) as an efficient catalyst for the hydrogen evolution reaction (HER). The crystallinity, morphology, chemical bonding, and composition of the composite material were comprehensively investigated using X-ray diffraction, Raman spectroscopy, field emission scanning electron microscopy, and X-ray photoelectron spectroscopy. The results confirmed the successful synthesis of the WS 2 –WC–WO 3 NH spheres. Interestingly, the presence of nitrogen significantly enhanced the electrical conductivity of the hybrid material, facilitating electron transfer during the catalytic process. As a result, the WS 2 –WC–WO 3 NH hybrid exhibited better HER performance than the pure WS 2 nanoflowers, which can be attributed to the synergistic effect of the W–S, W–C, and W–O bonding in the composite. Remarkably, the Tafel slope of the WS 2 –WC–WO 3 NH spheres was 59 mV dec −1 , which is significantly lower than that of the pure WS 2 NFs (82 mV dec −1 ). The results also confirmed the unprecedented stability and superior electrocatalytic performance of the WS 2 –WC–WO 3 NH spheres toward the HER, which opens new avenues for the preparation of low-cost and highly effective materials for energy conversion and storage applications.
SCN1A Gene Mutation and Adaptive Functioning in 18 Vietnamese Children with Dravet Syndrome
Thi Thu Hang Do,Diem My Vu,Thi Thuy Kieu Huynh,Thi Khanh Van Le,손은화,Thieu Mai Thao Le,Huu Hao Ha,Chi Bao Bui 대한신경과학회 2017 Journal of Clinical Neurology Vol.13 No.1
Background and Purpose Dravet syndrome is a rare and severe type of epilepsy in infants. The heterogeneity in the overall intellectual disability that these patients suffer from has been attributed to differences in genetic background and epilepsy severity. Methods Eighteen Vietnamese children diagnosed with Dravet syndrome were included in this study. SCN1A variants were screened by direct sequencing and multiplex ligation-dependent probe amplification. Adaptive functioning was assessed in all patients using the Vietnamese version of the Vineland Adaptive Behavior Scales, and the results were analyzed relative to the SCN1A variants and epilepsy severity. Results We identified 13 pathogenic or likely pathogenic variants, including 6 that have not been reported previously. We found no correlations between the presence or type of SCN1A variants and the level of adaptive functioning impairment or severity of epilepsy. Only two of nine patients aged at least 5 years had an adaptive functioning score higher than 50. Both of these patients had a low frequency of convulsive seizures and no history of status epilepticus or prolonged seizures. The remaining seven had very low adaptive functioning scores (39 or less) despite the variability in the severity of their epilepsy confirming the involvement of factors other than the severity of epilepsy in determining the developmental outcome. Conclusions Our study expands the spectrum of known SCN1A variants and confirms the current understanding of the role of the genetic background and epilepsy severity in determining the developmental outcome of Dravet syndrome patients.
Van Nguyen Tuan,Do Ha Huu,Tekalgne Mahider,Van Le Quyet,Nguyen Thang Phan,Hong Sung Hyun,Cho Jin Hyuk,Van Dao Dung,Ahn Sang Hyun,Kim Soo Young 나노기술연구협의회 2021 Nano Convergence Vol.8 No.33
Following publication of the original article [1], the affiliation of the authors was incorrectly published in the article. The affiliation which was shown in supplementary information is correct. This has been corrected with this erratum.
Yan Ding,Enqi Wu,Jianbo Chen,Huu Tung Nguyen,Thi Ha Do,Kyung Lae Park,KiHwan Ba,Young Ho Kim,강종성 대한화학회 2009 Bulletin of the Korean Chemical Society Vol.30 No.10
A simple high performance liquid chromatographic method was developed to evaluate the quality of Moutan Cortex Radicis based on chromatographic fingerprints that characterize eight pharmacological compounds, namely, gallic acid, paeoniflorin, galloyl paeoniflorin, benzoic acid, quercetin, benzoylpaeoniflorin, paeoniflorigenone, and paeonol. These compounds were identified by their characteristic UV profiles and the mass spectroscopy data, and their contents were determined by HPLC. The chromatographic separation was performed on a C18 column by gradient elution with 0.05% formic acid in water and acetonitrile. The methodological validation gave acceptable linearities (r = 0.9996) and recoveries (ranging from 99.4∼103.1%). The limits of detection (LOD) of these compounds ranged from 10 to 30 μg/mL. The representative chromatographic fingerprints of Moutan Cortex Radicis were obtained by analyzing 20 batches of samples collected from markets in Korea and China. For the efficient evaluation of quality for the commercial Moutan Cortex Radicis it is recommended that the total content of the six characteristic compounds should contain more than a minimum of 2% and that the content of total paeoniflorin and paeonol should exceed a minimum of 1.5% of dry weight of Moutan Cortex Radicis.
Ding, Yan,Wu, Enqi,Chen, Jianbo,Nguyen, Huu-Tung,Do, Thi-Ha,Park, Kyung-Lae,Bae, Ki-Hwan,Kim, Young-Ho,Kang, Jong-Seong Korean Chemical Society 2009 Bulletin of the Korean Chemical Society Vol.30 No.10
A simple high performance liquid chromatographic method was developed to evaluate the quality of Moutan Cortex Radicis based on chromatographic fingerprints that characterize eight pharmacological compounds, namely, gallic acid, paeoniflorin, galloyl paeoniflorin, benzoic acid, quercetin, benzoylpaeoniflorin, paeoniflorigenone, and paeonol. These compounds were identified by their characteristic UV profiles and the mass spectroscopy data, and their contents were determined by HPLC. The chromatographic separation was performed on a $C_{18}$ column by gradient elution with 0.05% formic acid in water and acetonitrile. The methodological validation gave acceptable linearities (r = 0.9996) and recoveries (ranging from 99.4∼103.1%). The limits of detection (LOD) of these compounds ranged from 10 to 30 $\mu$g/mL. The representative chromatographic fingerprints of Moutan Cortex Radicis were obtained by analyzing 20 batches of samples collected from markets in Korea and China. For the efficient evaluation of quality for the commercial Moutan Cortex Radicis it is recommended that the total content of the six characteristic compounds should contain more than a minimum of 2% and that the content of total paeoniflorin and paeonol should exceed a minimum of 1.5% of dry weight of Moutan Cortex Radicis.