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Synthesis and Characterization of KTiNbO5 Nano-particles by Novel Polymerizable Complex Method
Ning-ning Wang,Yun-xiang Lan,Jie He,Rui Dong,Jin-song Hu 대한화학회 2013 Bulletin of the Korean Chemical Society Vol.34 No.9
The layered KTiNbO5 was successfully synthesized with titanium(IV) isopropoxide and niobium oxalate by a novel polymerized complex (PC) method. The morphology and structure of the as-prepared sample was characterized by means of High-Resolution Transmission Electron Microscope, powder X-ray diffraction, and Laser Raman Spectroscopy. The spectral response characteristic was recorded by using UV-vis Diffuse Reflectance Spectroscopy. Results show that KTiNbO5 as-prepared by PC method presents an uniform morphology of nano-particles, the mean particle sizes is ca. 28 nm corresponding to the (002), and the crystal structure can be well indexed to the orthorhombic phase. The sample as-prepared by PC method has higher band gap energy than that of the sample prepared by a solid-state reaction method due to the quantum size effect.
Two Androstane Derivatives from the Cultures of Fungus Marasmiellus ramealis (Bull.) Singer
Ning-Ning Yang,Qing-Yun Ma,Sheng-Zhuo Huang,Hao-Fu Dai,Zhi-Kai Guo,Zhi-Fang Yu,You-Xing Zhao 대한화학회 2014 Bulletin of the Korean Chemical Society Vol.35 No.11
A new androstane derivative, 4β-methyl-15-oxa-14β-androstane-7-ene-4α-carboxylic acid (1) and a known one 4β-methyl-15-oxa-14β-androstane-7-ene-4α-hydroxyl (2) were isolated from the EtOAc extract of the cultures of the fungus Marasmiellus ramealis (Bull.) Singer. Their structures were elucidated on the basis of 1D and 2D NMR as well as MS spectroscopic data analysis. The inhibitory activity of two isolates against acetylcholinesterase (AChE) revealed that compound 1 exhibited definitely inhibitory activity.
Wang, Ning-Ning,Lan, Yun-Xiang,He, Jie,Dong, Rui,Hu, Jin-Song Korean Chemical Society 2013 Bulletin of the Korean Chemical Society Vol.34 No.9
The layered $KTiNbO_5$ was successfully synthesized with titanium(IV) isopropoxide and niobium oxalate by a novel polymerized complex (PC) method. The morphology and structure of the as-prepared sample was characterized by means of High-Resolution Transmission Electron Microscope, powder X-ray diffraction, and Laser Raman Spectroscopy. The spectral response characteristic was recorded by using UV-vis Diffuse Reflectance Spectroscopy. Results show that $KTiNbO_5$ as-prepared by PC method presents an uniform morphology of nano-particles, the mean particle sizes is ca. 28 nm corresponding to the (002), and the crystal structure can be well indexed to the orthorhombic phase. The sample as-prepared by PC method has higher band gap energy than that of the sample prepared by a solid-state reaction method due to the quantum size effect.
Two Androstane Derivatives from the Cultures of Fungus Marasmiellus ramealis (Bull.) Singer
Yang, Ning-Ning,Ma, Qing-Yun,Huang, Sheng-Zhuo,Dai, Hao-Fu,Guo, Zhi-Kai,Yu, Zhi-Fang,Zhao, You-Xing Korean Chemical Society 2014 Bulletin of the Korean Chemical Society Vol.35 No.11
A new androstane derivative, $4{\beta}$-methyl-15-oxa-$14{\beta}$-androstane-7-ene-$4{\alpha}$-carboxylic acid (1) and a known one $4{\beta}$-methyl-15-oxa-$14{\beta}$-androstane-7-ene-$4{\alpha}$-hydroxyl (2) were isolated from the EtOAc extract of the cultures of the fungus Marasmiellus ramealis (Bull.) Singer. Their structures were elucidated on the basis of 1D and 2D NMR as well as MS spectroscopic data analysis. The inhibitory activity of two isolates against acetylcholinesterase (AChE) revealed that compound 1 exhibited definitely inhibitory activity.
Song, Xiao-Yun,Zhou, Shi-Jie,Xiao, Ning,Li, Yun-Song,Zhen, De-Zhi,Su, Chong-Yu,Liu, Zhi-Dong Asian Pacific Journal of Cancer Prevention 2013 Asian Pacific journal of cancer prevention Vol.14 No.8
Aims: This study was conducted to evaluate the levels of TNF-${\alpha}$, IL-6, IL-8 and VEGF in serum of patients with non- small cell lung cancer, for assessing their possible diagnostic and prognostic roles. Methods: We enrolled 48 patients newly diagnosed with non-small cell lung cancer and 40 healthy controls. TNF- ${\alpha}$, IL-6 and IL-8 levels were measured in the serum of all the subjects with specific radioimmunoassay kits, while EGF was analyzed by sandwich enzyme immunoassay techniques. Results: A statistically significant difference was observed between lung cancer patients and the control group regarding the values of TNF-${\alpha}$, IL-6, IL-8 and VEGF in serum. Moreover, TNF-${\alpha}$, IL-8 and VEGF levels were higher in patients with advanced stages compared to early stages. In addition, higher serum levels of TNF-${\alpha}$, IL-6, IL-8 and VEGF were found in smokers than in non-smokers, both in patients and controls. Conclusion: Serum levels of TNF-${\alpha}$, IL-6, IL-8 and VEGF were all elevated in lung cancer patients, suggesting that inflammatory cytokines could be jointly used as a screening tool. Though TNF-${\alpha}$, IL-8 and VEGF levels were related to advanced disease, long-term survival studies of NSCLC patients should be performed to confirm whether they can act as biomarkers of advanced disease. In addition, smoking would be an important contributor to the processes of inflammation and lung cancer.
Yun-Bong Kim,Jeong-Ig Song,Han Ning,Jae-Moung Kim 통신위성ㆍ우주산업연구회 2007 한국위성정보통신학회논문지 Vol.2 No.2
위성통신시스템은 넓은 커버리지를 바탕으로 광범위한 지역에 통신을 가능하게 하는 장점을 가지고 있다. 그러나 위성통신 시스템에 할당된 주파수 대역의 사용률은 셀룰러 시스템과 같은 다른 무선통신시스템과 비교할 때 상당히 낮은 효율을 보인다. 그러므로 할당된 주파수를 이용하여 부가적인 서비스를 제공하고, 주파수 효율을 높이기 위한 방법들이 연구되고 있다. 본 논문에서는 허가 대역에서 새로운 서비스를 적용할 수 있는지에 관하여 분석해보고, 새로운 서비스를 적용하기 위하여 가장 중요한 부분인 위성 터미널의 신호를 정확하게 검출하는 방법을 제안한다. 제안하는 방법은 간섭을 회피하기 위하여 Spectrum Sensing과 Eigenvalue 검출하고, 결론을 통하여 터미널의 신호를 검출하고 성능을 분석한다. The Satellite Mobile Communication System holds several advantages, such as wide coverage that guarantees the communication in a huge area. It is suitable in the ocean and forest and especially in emergency situation. However, the licensed frequency is not always occupied within all coverage and all the time. The actual utilization rate is relatively low compared to other wireless communications such as cellular systems. There are a large amount of white spaces in its coverage. Therefore, it is necessary to consider introducing additional services such as data communication, in order to increase the spectrum utilization as well as the revenue of the Satellite service provider. In this paper, we first analyze the possibility to implement new services in the licensed band of satellite mobile phone by its provider. Then we address the most significant issue for the implementation of current service, which is how to accurately detect the satellite mobile terminals. Finally, we suggest two new possible solutions namely, eigenvalue detection based methods to find out the existence of transmitted signal from the satellite mobile terminals.
Characterization method of rolling bearing operation state based on feature information fusion
Ning Li,Xianghe Yun,Qingkai Han,Baogang Wen,Jingyu Zhai 대한기계학회 2023 JOURNAL OF MECHANICAL SCIENCE AND TECHNOLOGY Vol.37 No.3
Aiming at the problem of incomplete information covered by the bearing state discrimination using a single physical quantity as the data source, a characterization method based on the feature information fusion of multi-physical quantities including acceleration RMS and stiffness that are sensitive to the bearing operating state is proposed. The accelerated life test of the bearing is carried out through the bearing experiment bench, and the effect of different feature information fusion schemes to characterize the bearing state is compared, and the effectiveness of the method is verified. This paper also analyzes the different characteristics of the state evolution law between the bearing early failure caused by specific factors and the bearing reaching normal fatigue life, which provides a new method and idea for the maintenance strategy of rolling bearing such as condition-based maintenance.
Contributed Mini Review : Role of Wnt signaling in fracture healing
( Hui Yun Xu ),( Jing Duan ),( Dan Dan Ning ),( Jing Bao Li ),( Ruo Fei Liu ),( Rui Xin Yang ),( Jean X Jiang ),( Peng Shang ) 생화학분자생물학회(구 한국생화학분자생물학회) 2014 BMB Reports Vol.47 No.12
The Wnt signaling pathway is well known to play major roles in skeletal development and homeostasis. In certain aspects, fracture repair mimics the process of bone embryonic development. Thus, the importance of Wnt signaling in fracture healing has become more apparent in recent years. Here, we summarize recent research progress in the area, which may be conducive to the development of Wnt-based therapeutic strategies for bone repair.