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      • KCI등재

        Aspects of Structural and Multiferroic Properties of A- (15% Gd) and B-Site (5–15% Cr) Doped Perovskite BiFeO3 Nanoparticles

        M. N. Hossain,M. A. Matin,M. A. Islam,M. M. Rhaman,M. A. Hakim,M. F. Islam 한국전기전자재료학회 2021 Transactions on Electrical and Electronic Material Vol.22 No.4

        This report focuses on the investigation of multiferroic properties of 15% Gd and (5–15) % Cr co-doped Bismuth Ferrite (BFO) nanoparticles prepared by sol–gel method. The synthesized pure BFO has shown to be R3c rhombohedral crystal structure which partially transforms to Pnma orthorhombic crystal structure with increasing Cr dopant in co-doped samples. The crystallite size was found to vary from 68 to 22 nm depending on doping level. SEM images exhibited uniform nanoparticles and the average size of particles was shown to vary from 263 to 114 nm which is comparatively higher than that obtained from XRD results due to agglomeration eff ects. Ferroelectric tests exhibited a signifi cant reduction in polarization in doped BFO under an applied fi eld of ± 15 kV/cm. In contrast, the magnetic measurement showed a substantial improvement in ferromagnetic properties of the synthesized samples compared to un-doped one. A prominent exchange anisotropy eff ect was also observed in all the samples at room temperature. In addition, co-doped BFO samples demonstrated a signifi cant reduction in band gap energy from 1.88 to 1.68 eV.

      • KCI등재

        Structure-based magnetic, electrical and transport properties of Ni–Zn–Co ferrite by V5+ substitution

        Hossain M.D.,Khan M.N.I.,Hossain Md Sarowar,Ahned S.J.,Alam M.K.,Liba S.I.,Hakim M.A.,Jamil A.T.M.K. 한국물리학회 2022 Current Applied Physics Vol.43 No.-

        This article presents the modification of structure-based magnetic, electronic and transport properties along with the conduction mechanism and its relaxation process in a Ni–Zn–Co ferrite tailored by V5+ substitution at B-site replacing Fe3+ ions. The composition Ni0.7Zn0.2Co0.1Fe2-xVxO4 (0≤ x≤ 0.12) was synthesized by standard solid-state reaction method and all samples were crystallized with a single-phase cubic spinel structure belonging to the Fd3m space group. The lattice constants decreased gradually from 8.3673≽A to 8.3602≽A and the average grain sizes (DSEM) are also decreased from 6.92 μm to 1.99 μm due to V5+ ions substitution at Fe3+ of B-site. However, more than 25% of Fe3+ ions migrate to A-site from B-site due to V5+ substitution at Fe3+ of B-site. In all samples θD does not strictly follow the Anderson’s prediction, rather it monotonically decreases to a low value until x = 0.12. Magnetic phase transition temperature shifted to the lower temperature and the net magnetization (ηeB) decreases due to V5+ substitution in Ni–Zn–Co ferrite. Apart this, during conduction charge carriers should require more energy to jump from one cationic site to other for V5+ substitution in the Ni–Zn–Co ferrite and the activation energy (Ea) is much more higher in V5+ substituted sample. Moreover, long-range interaction with localized relaxation mechanism is observed in V5+ doped samples. The resistance at the grain (Rg) is maximum (243.09 Ω) for the sample x = 0.10 while grain boundary resistance (Rgb) is maximum (5.98×105 Ω) for the sample x = 0.07. However, the higher value of ρdC for x = 0.12 sample ensures to be suitable for electromagnets, transformers, electronic inductors, and at high-frequency applications. Moreover, x = 0.07 sample displays high value of TCR ( -8.6%/K at 418 K) which may be utilized as an infrared detector for night vision bolometer material.

      • KCI등재

        Effect of Preparation Routes on the Crystal Purity and Properties of BiFeO3 Nanoparticles

        M. A. Matin,M. M. Rhaman,M. N. Hossain,F. A. Mozahid,M. A. Hakim,M. H. Rizvi,M. F. Islam 한국전기전자재료학회 2019 Transactions on Electrical and Electronic Material Vol.20 No.6

        Sol–gel as a chemical solution deposition technique is compatible with functional device fabrication technology. Single-phase bismuth ferrite (BiFeO3) mutiferroic with its multi-functionality has extensively been studied for a variety of prospective novel device applications. However, the synthesis of BiFeO3 is confronted with a challenge to produce pure state without any secondary phase. Scarcity of unified process parameters impede justifi cation of best synthesis techniques. In this work, sol–gel methods with and without auto-combustion reactions were used to synthesize bismuth ferrite (BiFeO3) nanoparticles. Different techniques UV–Vis–NIR spectroscopy, XRD, EDS, and SEM were used to investigate the effect of preparation routes on the crystal purity and properties of prepared samples. Synthesized nanoparticles were calcined at temperature between 400 and 800 ◦ C and an optimal calcination temperature was found to be 600 ◦ C. Band-gap was determined by UV–Vis–NIR spectroscopy and found to vary from 1.93 to 2.07 eV. X-ray diff raction (XRD) has confi rmed single phase rhombohedral crystal structure with R3c symmetry. Avg crystallite size was found to be higher (40–68 nm) in auto-combustion reaction compared to that of 23–42 nm obtained in sol–gel method without auto-combustion reaction. The band-gap energy was found to reduce with decreasing crystallite size (above the critical size of 10 nm) following Brus’s eff ective mass model. Induced strain was found to exhibit an inverse relation with crystallite size and displayed substantial reduction in auto-combustion reaction route. The microstructural features were investigated by fi eld emission scanning electronic microscopy and avgparticle size was shown to vary from 107 to 197 nm depending on adopted synthesis route. A low reaction temperature (70 ◦ C–80 ◦ C) without auto-combustion and calcination temperature at 600◦ C were found to be optimal conditions for the preparation of low impurity un-doped bismuth ferrite nanaoparticles.

      • SCIESCOPUSKCI등재

        EFFECT OF FEEDING STRAW SUPPLEMENTING WITH UREA MOLASSES BLOCK LICK ON THE PERFORMANCE OF SHEEP

        Hossain, K.B.,Sarker, N.R.,Saadullah, M.,Beg, M.A.H.,Khan, T.M. Asian Australasian Association of Animal Productio 1995 Animal Bioscience Vol.8 No.3

        The experiment was conducted to study the effect of supplementary urea molasses block lick with rice straw based diet on the performance of sheep. Six indigenous sheep of about two years of age with an average body weight of 12.88 kg, were selected for this experiment They grouped into two by stratified randomization, and the experiment was conducted for a period of 90 days. Sheep of group A was fed rice straw and group B was feed rice straw with urea molasses block lick, beside this both the groups received 66 g wheat bran and 167 g of Ipil-Ipil leaf meat. The study revealed that the average daily gain of live weight per sheep per day was 41 gm and 70 gm in group-A and group-B respectively. From the analysis of variance it was evident that live weight gain in sheep of group B, supplemented with urea molasses block lick was highly significant (p < 0.01). It was also estimated that group A required 8.12 kg DM to gain 1 kg live weight, whereas group B receiving urea molasses block lick required 5.30 kg DM to gain 1 kg live weight. Therefore, feeding rice straw with urea molasses block lick able to utilize more crop-residues efficiently.

      • KCI등재

        Optical and Ferroelectric Properties of Bi0.95Gd0.05Fe1−xCrxO3

        M. A. Matin,M. N. Hossain,M. M. Islam,M. A. Hakim,M. F. Islam 한국전기전자재료학회 2021 Transactions on Electrical and Electronic Material Vol.22 No.3

        In this paper, optical and ferroelectric properties were investigated for gadolinium, Gd3+ (5 at.%) and chromium, Cr3+ (0–8at.%) co-doped of BiFeO3 . Chemical solution deposition (CSD) method was employed as compatible device fabrication technology to synthesize Gd and Cr co-doped multiferroic BiFeO3 (Bi0.95Gd0.05Fe1−xCrxO3 with x = 0–0.08). X-ray diffraction (XRD) analysis confirmed a well-defined crystalline phase with a tendency towards structural change from rhombohedral to orthorhombic symmetry. Crystallite size was found to reduce substantially from 34 to 13.5 nm with increasing the doping concentration of Cr3+ . The field emission scanning electron microscopy (FESEM) demonstrated a significant reduction in grain size of doped BiFeO3 compared to un-doped one following the trend obtained from XRD results. Ferroelectric nature of samples was obtained from polarization versus electric field measurements. Improved ferroelectric order was displayed in co-doped BiFeO3 with a maximum remnant polarization of 0.23 μ C∕cm2 . Diffuse reflectance measurement by UV–Vis–NIR spectroscopy of Gd 3+ and Cr3+ co-doped BiFeO3 has shown a significant reduction in the optical band-gap energy (Eg) to 1.71 eV compared to 2.03 eV of pure BiFeO 3 counterpart.

      • KCI등재

        Reproductive performance comparison between local and crossbred sows reared under backyard and farming condition in Rangamati district of Bangladesh

        Hossain, M.I.,Momin, M.M.,Fakhrul Islam, K.M.,Quader, M.N.,Miah, G. The Korean Society of Embryo Transfer 2016 한국동물생명공학회지 Vol.31 No.3

        It is imperious to know the reproductive parameters of the subsisting swine breed for profitable farming in Bangladesh. This study was designed to compare the reproductive parameters of sows at hilly areas between the local and crossbred at farm and backyard level. A total of 116 breedable sows were included. The data on age at puberty, litter size, birth weight, weaning weight, gestation length, interval between farrowing and number of piglets born per sow in local and crossbred sows were determined and direct questionnaire method was used for data collection. The present study revealed that age at puberty between farm and backyard system of crossbred sows was $8.88{\pm}0.153$ and $9.85{\pm}0.221$ months, respectively. The farrowing interval was shorter in crossbred sows which were kept in farming system rather than backyard system. The interval between farrowing and onset of estrus was shorter in crossbred sows. The gestation length was almost similar between backyard and farm condition. The number of litter size per sow per farrowing was $8.45{\pm}0.41$ in crossbred and $7.17{\pm}0.250$ in local pigs at backyard system. The birth weight and weaning weight were more in farm conditions than backyard system. The age at puberty in local breed was lower than the crossbred and litter size was $8.45{\pm}0.407$ in crossbred which was higher than local breed $7.17{\pm}0.250$ in backyard system. These results suggest that reproductive parameters of local sow need to be improved for better production and crossbred sows should be reared for obtaining desired productivity.

      • KCI등재후보

        Experimental Pathogenesis of Pullorum Disease with the Local Isolate of Salmonella enterica serovar. enterica subspecies Pullorum in Pullets in Bangladesh

        M. G. Haider,E. H. Chowdhury,M. A. H. N. A. Khan,M. T. Hossain,M. S. Rahman,송희종,M. M. Hossain 한국가금학회 2008 韓國家禽學會誌 Vol.35 No.4

        The research work was carried out to study the pathogenesis covering the clinical signs, gross and histopathological lesions in different organs, and reisolation and identification of the organisms after experimental infection with the local isolate of Salmonella enterica serovar. enterica subspecies (S.) Pullorum at different time interval of the experiment during the period February 2006 to December 2006. One hundred pullets (seronegative to S. Pullorum of 12 weeks age were purchased and divided into 5 (A, B, C, D and E) groups and each group consisted of 20 birds. Four groups (A, B, C and D) were infected orally with a dose of 106 CFU, 107 CFU, 2 × 107 CFU, 108 CFU of S. Pullorum, respectively, and one group (E) was treated as uninfected control. The used methods were necropsy and histopathology, culture of bacteria, staining and biochemical test of Salmonella. Five birds from each group were randomly selected and sacrificed 1st week, 2nd, 3rd and 4th weeks of post infection (PI). From all the groups, the bacteriological samples (crop, liver, lung, heart, spleen, bile duodenum, ceca and blood) were collected with pre enriched in buffered peptone water in sterile poly bags. Liver, lungs, heart, spleen, intestine, etc. were collected in 10% buffered-formalin for histopathological examination. No clinical signs, gross and histopathological lesions were found in control group and no S. Pullorum was reisolated. Clinical sign of experimentally infected with S. Pullorum in pullets were loss of appetite (100%), slight depression (75%), ruffled feathers (85%), diarrhea (60%) and loss of weight (100%) in chickens. The feed intake and body weight at different weeks after PI differed significantly (p<0.01) among the groups. Grossly, the highest recorded lesion was button-like ulcer in the ceca (80%) and the lowest was white nodules in lungs (1.25%). S. Pullorum were reisolated from crop (91.25%), liver (91.25%), lung (83.75%), heart (71.25%), spleen (87.75%), bile (33.25%), duodenum (92.50%), ceca (97.50%) and from different group of infection (61.25%). The highest microscopic findings were intestinal and cecal mucosa and submucosa exhibited infiltration of mononuclear cells and congestion (96.25%), and the lowest finding was nodule formation in the lungs (3.75%). The pattern of the disease production by local isolate of S. Pullorum in Bangladesh is almost similar with other isolates in different countries. The research work was carried out to study the pathogenesis covering the clinical signs, gross and histopathological lesions in different organs, and reisolation and identification of the organisms after experimental infection with the local isolate of Salmonella enterica serovar. enterica subspecies (S.) Pullorum at different time interval of the experiment during the period February 2006 to December 2006. One hundred pullets (seronegative to S. Pullorum of 12 weeks age were purchased and divided into 5 (A, B, C, D and E) groups and each group consisted of 20 birds. Four groups (A, B, C and D) were infected orally with a dose of 106 CFU, 107 CFU, 2 × 107 CFU, 108 CFU of S. Pullorum, respectively, and one group (E) was treated as uninfected control. The used methods were necropsy and histopathology, culture of bacteria, staining and biochemical test of Salmonella. Five birds from each group were randomly selected and sacrificed 1st week, 2nd, 3rd and 4th weeks of post infection (PI). From all the groups, the bacteriological samples (crop, liver, lung, heart, spleen, bile duodenum, ceca and blood) were collected with pre enriched in buffered peptone water in sterile poly bags. Liver, lungs, heart, spleen, intestine, etc. were collected in 10% buffered-formalin for histopathological examination. No clinical signs, gross and histopathological lesions were found in control group and no S. Pullorum was reisolated. Clinical sign of experimentally infected with S. Pullorum in pullets were loss of appetite (100%), slight depression (75%), ruffled feathers (85%), diarrhea (60%) and loss of weight (100%) in chickens. The feed intake and body weight at different weeks after PI differed significantly (p<0.01) among the groups. Grossly, the highest recorded lesion was button-like ulcer in the ceca (80%) and the lowest was white nodules in lungs (1.25%). S. Pullorum were reisolated from crop (91.25%), liver (91.25%), lung (83.75%), heart (71.25%), spleen (87.75%), bile (33.25%), duodenum (92.50%), ceca (97.50%) and from different group of infection (61.25%). The highest microscopic findings were intestinal and cecal mucosa and submucosa exhibited infiltration of mononuclear cells and congestion (96.25%), and the lowest finding was nodule formation in the lungs (3.75%). The pattern of the disease production by local isolate of S. Pullorum in Bangladesh is almost similar with other isolates in different countries.

      • KCI등재

        Reproductive performance comparison between local and crossbred sows reared under backyard and farming condition in Rangamati district of Bangladesh

        M.I. Hossain,M.M. Momin,K.M. Fakhrul Islam,M.N. Quader,G. Miah 한국수정란이식학회 2016 한국동물생명공학회지 Vol.31 No.3

        It is imperious to know the reproductive parameters of the subsisting swine breed for profitable farming in Bangladesh. This study was designed to compare the reproductive parameters of sows at hilly areas between the local and crossbred at farm and backyard level. A total of 116 breedable sows were included. The data on age at puberty, litter size, birth weight, weaning weight, gestation length, interval between farrowing and number of piglets born per sow in local and crossbred sows were determined and direct questionnaire method was used for data collection. The present study revealed that age at puberty between farm and backyard system of crossbred sows was 8.88±0.153 and 9.85±0.221 months, respectively. The farrowing interval was shorter in crossbred sows which were kept in farming system rather than backyard system. The interval between farrowing and onset of estrus was shorter in crossbred sows. The gestation length was almost similar between backyard and farm condition. The number of litter size per sow per farrowing was 8.45±0.41 in crossbred and 7.17±0.250 in local pigs at backyard system. The birth weight and weaning weight were more in farm conditions than backyard system. The age at puberty in local breed was lower than the crossbred and litter size was 8.45±0.407 in crossbred which was higher than local breed 7.17±0.250 in backyard system. These results suggest that reproductive parameters of local sow need to be improved for better production and crossbred sows should be reared for obtaining desired productivity.

      • KCI등재

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