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Jinhong Yu,Wei Wu,Dan Dai,Yingze Song,Chaoyang Li,Nan Jiang 한국고분자학회 2014 Macromolecular Research Vol.22 No.1
Zinc oxide (ZnO) nanorods were synthesized using a modified wet chemical method. Poly(vinylidene fluoride-co-hexafluoropropylene), P(VDF-HFP), nanocomposites with different ZnO nanorods loadings were prepared viaa solution blend route. Field emission scanning electron microscopic (FE-SEM), X-ray diffraction (XRD), Fouriertransform infrared spectroscopy (FTIR) were used to investigate the structure and morphology of the nanocomposites. XRD and FTIR data indicate that the incorporation of ZnO nanorods promote the crystalline structure transformationof P(VDF-HFP). As the content of ZnO nanorods increases, the β phase structure increases while the α phasedecreases. In addition, the dielectric properties of the P(VDF-HFP) and its composites were systematically studied.
Influence of Interface Structure on Dielectric Properties of Epoxy/Alumina Nanocomposites
Jinhong Yu,Genglin Wang,Ruimei Huo,Chao Wu,Xinfeng Wu,Pingkai Jiang 한국고분자학회 2012 Macromolecular Research Vol.20 No.8
Alumina (Al2O3) nanoparticles with three different interface structures have been selected as reinforcement fillers for epoxy nanocomposite, that is surface untreated Al2O3 nanoparticles, γ-aminopropyl-triethoxysilane modified Al2O3 nanoparticles (Al2O3-APS), and hyperbranched aromatic polyamide grafted Al2O3 nanoparticles (Al2O3-HBP). The interface structures of the Al2O3 nanoparticles were characterized by X-ray diffraction and atomic force micrographs. Our studies reported the influence of the interface structure of Al2O3 nanoparticles on the morphology and dielectric properties of epoxy nanocomposites. It was found that the incorporation of the Al2O3-APS and Al2O3-HBP nanoparticles not only improved the dispersion of the nanoparticles in the epoxy matrix, but also enhanced the glass transition temperatures (Tgs) and largely influenced the dielectric properties of the epoxy nanocomposites as compared with the nanocomposites filled with the surface untreated Al2O3 nanoparticles. The improvement of Tgs, volume resistivity, dielectric strength, and the reduction of dielectric loss could be attributed to the good dispersion and special interface structure of the Al2O3 nanoparticles in the epoxy matrix.
( Jesang Yu ),( Jinhong Jung ),( Sang Min Yoon ) 대한간암학회 2020 대한간암학회지 Vol.20 No.1
The optimal treatment strategy for unresectable huge hepatocellular carcinoma (HCC) is yet to be established. Non-surgical monotherapy demonstrated insufficient oncologic outcomes in previously reported studies. To improve the clinical outcomes of unresectable huge HCC, combined locoregional treatments can be considered in selected cases. Here, we report a case of 58-year-old male patient who was treated with combined transarterial chemoembolization (TACE) and external beam radiotherapy for recurrent HCC after a previous hepatic resection. After combined TACE and radiotherapy for the intrahepatic lesion, two metastases were diagnosed in the pelvic bones and lung; each lesion was successfully treated with salvage radiotherapy. During the long-term follow-up period (around 8 years 7 months after combined TACE and radiotherapy for the recurrent huge HCC), no definite viable tumors were observed in any of the treated liver, bone, and lung lesions. (J Liver Cancer 2020;20:90-97)
Zhengkai Yuan,Jinhong Yu,Baolin Rao,Hua Bai,Nan Jiang,Jian Gao,Shaorong Lu 한국고분자학회 2014 Macromolecular Research Vol.22 No.4
In this report, we demonstrate that the thermal conductivity, glass transition temperature, thermal stabilityand dynamical mechanical properties of epoxy composites could all be improved by incorporating hyperbranchedaromatic polyamide grafted silicon carbide (SiC-HBP) whiskers, using a solution method. The morphology andthermal properties of these newly modified epoxy composites were systematically analyzed and studied. Fouriertransform infrared spectroscopy (FTIR), nuclear magnetic resonance spectroscopy (NMR), and thermal gravimetricanalyses (TGA) proved hyperbranched aromatic polyamide grafted SiC whiskers were successfully prepared bysolution polymerization. The thermal conductivity of epoxy composite with 30 wt% of SiC-HBP had 2-fold improvement,compared to that of the neat epoxy. Besides, the glass transition temperatures (Tg) and dynamical mechanicalproperties of the epoxy composites were also raised by the addition of SiC-HBP, which indicates strong interfacialadhesion between SiC-HBP and the epoxy matrix. Most importantly, the incorporation of SiC-HBP in the epoxymatrix could effectively improve the thermal stability of the epoxy composites, according to our thermogravimetricanalysis (TGA).
Enhanced Thermal and Mechanical Properties of Polyimide/Graphene Composites
Wen Dai,Jinhong Yu,Yi Wang,Yingze Song,Hua Bai,Kazuhito Nishimura,Huiwei Liao,Nan Jiang 한국고분자학회 2014 Macromolecular Research Vol.22 No.9
Polyimide (PI)/graphene sheets (GSs) composites were prepared by solution blending. The incorporationof GSs into PI increased the thermal conductivity, thermal stability and mechanical properties of PI. The thermal conductivityof PI/GSs composites was significantly improved compared with that of neat PI from 0.254 to 1.002 W/mK; this can be attributed to the homogeneous dispersion of graphene and the formation of heat conduction pathway. Furthermore, the Young modulus of PI/GSs was raised up to 4.04 GPa, approximately two-fold enhancement incomparison with that of neat PI. In addition, the incorportation of GSs in PI indicated excellent optical transparencyat the lowest weight fractions of GSs and modified wettability of PI films.
Xu Xu,Jinhong Yu,Zihai He,Shaorong Lu,Dong Guo 한국고분자학회 2014 Macromolecular Research Vol.22 No.10
A reactive compatibilizer containing flexible segment (RCFS) was synthesized and characterized by Fouriertransform infrared spectroscopy (FTIR) and gel permeation chromatography (GPC). The RCFS was used as acompatibilizer for the preparation of lignin/polypropylene (PP) wood plastic composites, and the effect of the RCFSon the properties of composites (e.g., mechanical properties, thermal properties, crystal structure, and morphology)were investigated in detail. Experimental results indicated that the lignin/PP composite displayed the best performancewith the addition of 2 wt% RCFS. Its impact strength, flexural strength, and modulus were 56.8%, 37.3%,and 20.6%, respectively, which are higher than those of the untreated composites. Moreover, RCFS treatment couldalso increase the thermal stability, crystallization rate, and degree of crystallinity of lignin/PP composites.
Xinfeng Wu,Bo Tang,Jinhong Yu,Xiao Cao,Chongyin Zhang,Yonggen Lv 한국섬유공학회 2018 Fibers and polymers Vol.19 No.1
Graphite reinforced hollow epoxy macrospheres (GR-HEMS) and hollow glass microspheres (HGMS) were used to prepare three phase epoxy syntactic foam (ESF) using “molding method”, and the physical and mechanical properties of ESF were also studied and investigated. An innovative “rolling ball method” was implemented in the GR-HEMS preparationprocess. The performance tests show that higher GR-HEMS stacking volume fraction, lower GR-HEMS thickness, higher GR-HEMS diameter, higher HGMS volume fraction, lower HGMS density are beneficial to reducing the density of ESF, but the effects of the five factors on the strength of ESF are the opposite. Therefore, in order to obtain “high strength and low density” ESF composites, the various factors should be considered to achieve a balance of the strength and the density. Scanning electron microscope (SEM) shows that the “rolling ball method” can make graphite form a graphite spherical x-y network throughout the macrosphere wall, which can make GR-HEMS and ESF have great compressive strength. The ESF (450 kg/m3, 20.75 MPa) can withstand the 2075 meters water pressure and provide 550 kg/m3 buoyancy, which can givesome advice to the preparation of buoyancy material used in deepwater oil exploration.