Compositional homogeneity and X-ray topographic analyses of CdTe_<i>x</i>Se_1−<i>x</i> grown by the vertical Bridgman technique

Roy, U.N.,Bolotnikov, A.E.,Camarda, G.S.,Cui, Y.,Hossain, A.,Lee, K.,Lee, W.,Tappero, R.,Yang, Ge,Cui, Y.,Burger, A.,James, R.B. Elsevier 2015 Journal of crystal growth Vol.411 No.-

<P><B>Abstract</B></P> <P>We grew CdTe<SUB> <I>x</I> </SUB>Se<SUB>1−<I>x</I> </SUB> crystals with nominal Se concentrations of 5%, 7%, and 10% by the vertical Bridgman technique, and evaluated their compositional homogeneity and structural quality at the NSLS’ X-ray fluorescence and white beam X-ray topography beam lines. Both X-ray fluorescence and photoluminescence mapping revealed very high compositional homogeneity of the CdTe<SUB> <I>x</I> </SUB>Se<SUB>1−<I>x</I> </SUB> crystals. We noted that those crystals with higher concentrations of Se were more prone to twinning than those with a lower content. The crystals were fairly free from strains and contained low concentrations of sub-grain boundaries and their networks.</P> <P><B>Highlights</B></P> <P> <UL> <LI> CdTeSe crystals were grown by the vertical Bridgman technique. </LI> <LI> Very high compositional homogeneity. </LI> <LI> Low concentration of sub-grain boundaries. </LI> <LI> Almost free from sub-grain boundary network. </LI> </UL> </P>

Brassica oleracea Extracts Prevent Hyperglycemia in Type 2 Diabetes Mellitus

Sumeet Gupta,Satish Burman,Anroop B. Nair,Samrat Chauhan,Debabrata Sircar,Partha Roy,Meenakshi Dhanwat,Debrupa Lahiri,Dinesh Mehta,Rina Das,Hany Ezzat Khalil 한국식품영양과학회 2022 Preventive Nutrition and Food Science Vol.27 No.1

This study investigated the protective effect of extracts from flowers of Brassica oleracea L. var. italica Plenck on type 2 diabetes mellitus and its associated disorders. Three different doses of each extract (petroleum ether, ethanol, and aqueous) were administered orally for 42 days. Biochemical parameters, behavioral studies, and histological studies were measured at different periods. Mortality was found to be nil up to 2,000 mg/kg. Statistically significant (P<0.001) improvement in serum glucose level was observed in the groups receiving 400 mg/kg of petroleum ether, aqueous, or ethanol extracts compared with the negative control group. Insulin level was decreased by aqueous extracts, whereas lipid profiles were improved by aqueous and ethanol extracts. A reduction in transfer latency was observed in treatments of all three extract types. Ethanol extract treatment (400 mg/kg) showed maximum percentage inhibition in a lipid peroxidation assay. Additionally, the aqueous and ethanol extract treatments markedly reduced tumor necrosis factor-α, interleukin-6, and glycosylated hemoglobin levels. Histological results showed that high doses of extracts alleviated the damages induced by type 2 diabetes mellitus in various organs and bones. Based on the results of this study, it can be concluded that B. oleracea has the potential to alleviate type 2 diabetes mellitus.

Behaviour and strength of back-to-back built-up cold-formed steel unequal angle sections with intermediate stiffeners under axial compression

G. Beulah Gnana Ananthi,Krishanu Roy,James B. P. Lim 국제구조공학회 2022 Steel and Composite Structures, An International J Vol.42 No.1

In cold-formed steel (CFS) structures, such as trusses, transmission towers and portal frames, the use of back-toback built-up CFS unequal angle sections are becoming increasingly popular. In such an arrangement, intermediate welds or screw fasteners are required at discrete points along the length, preventing the angle sections from buckling independently. Limited research is available in the literature on axial strength of back-to-back built-up CFS unequal angle sections. The issue is addressed herein. This paper presents an experimental investigation reported by the authors on back-to-back built-up CFS unequal angle sections with intermediate stiffeners under axial compression. The load-axial shortening behaviour along with the deformed shapes at failure are reported. A nonlinear finite element (FE) model was then developed, which includes material non-linearity, geometric imperfections and modelling of intermediate fasteners. The FE model was validated against the experimental test results, which showed good agreement, both in terms of failure loads and deformed shapes at failure. The validated finite element model was then used for the purpose of a parametric study comprising 96 models to investigate the effect of longer to shorter leg ratios, stiffener provided in the longer leg, thicknesses and lengths on axial strength of back-toback built-up CFS unequal angle sections. Four different thicknesses and seven different lengths (stub to slender columns) with three overall widths to the overall depth (B/D) ratios were investigated in the parametric study. Axial strengths obtained from the experimental tests and FE analyses were used to assess the performance of the current design guidelines as per the Direct Strength Method (DSM); obtained comparisons show that the current DSM is conservative by only 7% and 5% on average, while predicting the axial strengths of back-to-back built-up CFS unequal angle sections with and without the stiffener, respectively.

Graphene-wrapped Ag 3 PO 4 /LaCO 3 OH heterostructures for water purification under visible light

Patil, Santosh S.,Mali, Mukund G.,Roy, Animesh,Tamboli, Mohaseen S.,Deonikar, Virendrakumar G.,Patil, Deepak R.,Kulkarni, Milind V.,Al-Deyab, Salem S.,Yoon, Sam S.,Kolekar, Sanjay S.,Kale, Bharat B. Elsevier 2016 Journal of energy chemistry Vol.25 No.5

<P>We demonstrated a unique synthesis approach of graphene (GR)-wrapped Ag3PO4/LaCO3OH (APO/LCO) heterostructures by an in-situ wet chemical method. FESEM analysis reveals the formation of rhombic dodecahedrons of APO decorated with LCO and later wrapped with GR flakes. Optical studies shows two absorption edges corresponding to the band gap energies of APO (2.41 eV) and LCO (4.1 eV). Considering the absorption edge of the heterostructures in the visible region, the photocatalytic activities of photocatalysts containing different APO/LCO mass ratios were evaluated by the degradation of MB. GR-decorated composite with 20% LCO (APO/LCO20/GR) exhibited the highest photocatalytic activity for MB degradation, with a rate constant, k of 0.541 min(-1). The photocatalytic activity of APO/LCO20/GR more greatly enhanced than those of the individual constituents (APO, LCO, APO/LCO20). The enhanced photocatalytic activity of the heterostructure can be attributed to the co-catalytic effect of LCO as well as intriguing physicochemical properties of GR. To understand the enhanced photocatalytic activity of the heterostructures the photocatalytic reaction mechanism is proposed in detail. The recyclability of the APO/LCO/GR composite photocatalyst is further evaluated by reusing the catalyst in replicate photocatalytic experiments which shows consistent photocatalytic activity thereby confirms the stability and reusability of heterostructure photocatalyst. (C) 2016 Science Press and Dalian Institute of Chemical Physics, Chinese Academy of Sciences. Published by Elsevier B.V. and Science Press. All rights reserved.</P>

Finite-element analysis and design of aluminum alloy RHSs and SHSs with through-openings in bending

Ran Feng,Tao Yang,Zhenming Chen,Krishanu Roy,Boshan Chen,James B. P. Lim 국제구조공학회 2023 Steel and Composite Structures, An International J Vol.46 No.3

This paper presents a finite-element analysis (FEA) of aluminum alloy rectangular hollow sections (RHSs) and square hollow sections (SHSs) with circular through-openings under three-point and four-point bending. First, a finite-element model (FEM) was developed and validated against the corresponding test results available in the literature. Next, using the validated FE models, a parametric study comprising 180 FE models was conducted. The cross-section width-to-thickness ratio (b/t) ranged from 2 to 5, the hole size ratio (d/h) ranged from 0.2 to 0.8 and the quantity of holes (n) ranged from 2 to 6, respectively. Third, results obtained from laboratory test and FEA were compared with current design strengths calculated in accordance with the North American Specifications (NAS), the modified direct strength method (DSM) and the modified Continuous strength method (CSM). The comparison shows that the modified CSM are conservative by 15% on average for aluminum alloy RHSs and SHSs with circular through-openings subject to bending. Finally, a new design equation is proposed based on the modified CSM after being validated with results obtained from laboratory test and FEA. The proposed design equation can provide accurate predictions of flexural capacities for aluminum alloy RHSs and SHSs with circular throughopenings.

Rule-based Machine Vision System on Clear Empty Glass Base Inspection of Foreign Materials for Philippine MSMEs

James Roy B. Santos,Raymund M. Lozada,Mark Joseph B. Enojas ASCONS 2019 IJASC Vol.1 No.3

Background/Objectives: The Philippine government through the Department of Science and Technology (DOST) helps the micro, small, and medium enterprises (MSMEs) to support and sustain growth and address their needs on availing cost-effective solutions. Methods/Statistical analysis: Most of the MSMEs which apply clear bottles for their products use manual inspection. These are prone to human error that leads to poor product qualities and rejects. Findings: To address these problems, this study presents a cost-effective solution by a rule-based machine vision system for clear empty glass base inspection. A method on proper setup for the inspection is presented and validated through an in-line loop on a wedge conveyor machine prototype. A minimal setup time was achieved by experimenting different lighting techniques. Improvements/Applications: The use of back light illumination is suggested for good image processing quality with minimal cost. The implementation of a rule-based inspection in this setup results to a high speed of 9000-18000 bottles per hour (bph) with consistent repeatability and superior accuracy.

Absence of P53 Gene Mutations in Exons 5 - 7 Among Breast Cancer Patients of Bengalee Hindu Caste Females, West Bengal, India

Roy, Abhishikta Ghosh,Sarkar, B.N.,Roy, Rakesh,Rao, V.R.,Bandyopadhyay, A.R. Asian Pacific Journal of Cancer Prevention 2012 Asian Pacific journal of cancer prevention Vol.13 No.9

Background: The high incidence and relatively good prognosis of breast cancer has made it the most prevalent cancer in the world today. A large number of distinct mutations and polymorphisms in the p53 gene have been reported worldwide, but there is no report regarding the role of this inherited susceptibility gene in breast cancer risk among the Bengalee Hindu Caste females of West Bengal, India. Aim of the Study: We investigated the distribution and the nature of p53 gene mutations and polymorphisms in exons 5-7 in a cohort of 110 Bengalee Hindu breast cancer patients and 127 age, sex and caste matched controls by direct sequencing. Results: We did not observe any mutations and polymorphisms in our studied individuals. Conclusion: We therefore conclude that mutations in exons 5-7 of p53 gene are rare causes of breast cancer among Bengalee Hindu caste females, and therefore of little help for genetic counseling and diagnostic purposes.

The Effect of Soil Physico-chemical Properties on Rhizome Rot and Wilt Disease Complex Incidence of Ginger Under Hill Agro-climatic Region of West Bengal

B. R. Sharma,S. Roy,A. Debnath,M. De Roy,S. Dutta 한국식물병리학회 2010 Plant Pathology Journal Vol.26 No.2

A study was conducted to find out the relationship of physico-chemical properties (viz. organic carbon(OC),pH, electrical conductivity, nitrogen, phosphorus and potassium content) of ginger growing soil with incidence percentage of rhizome rot and wilt disease complex of ginger. Organic carbon content and pH of the ginger soil contributed significantly (93%) in the prediction of ginger rhizome rot and wilt disease complex incidence with negative correlation. Soil having weak acidic reaction with OC percent greater than 2.25 was observed to have the lower average incidence of the disease.

Microstructural comparison of Zr_73.5Nb₉Cu₇Ni₁Al_9.5 nanostructure-dendrite composites produced by different casting techniques

Kim, K.B.,Das, J.,Lö,ser, W.,Lee, M.H.,Kim, D.H.,Roy, S.K.,Eckert, J. Elsevier 2007 Materials science & engineering. properties, micro Vol.449 No.-

<P><B>Abstract</B></P><P>Zr<SUB>73.5</SUB>Nb<SUB>9</SUB>Cu<SUB>7</SUB>Ni<SUB>1</SUB>Al<SUB>9.5</SUB> (numbers indicate at.%) nanostructure-dendrite composites were fabricated using three different casting techniques: suction casting, centrifugal casting and arc-melting. The microstructure of the suction casting sample consists of micrometer-scale dendrites in a nanostructured matrix. However, some areas in the matrix contain nano-scale crystals together with an amorphous phase revealing an inhomogeneity of the specimen. On the contrary, the microstructures of the centrifugally-cast and the arc-melted samples are overall homogeneous, consisting of micrometer-scale dendrites that are homogeneously distributed in a nanostructured matrix. The dendrites correspond to a body centered cubic (bcc) β-Zr phase, whereas the nanostructured matrix consists of body centered tetragonal (bct) Zr<SUB>2</SUB>Cu-type and hexagonal close-packed (hcp) MgZn<SUB>2</SUB>-type phases. The comparison of the microstructures of these two alloys reveals that the formation of nano-scale twins and a disordered ω-phase in the β-Zr dendrites only happens in the centrifugally-cast sample. The differences in the phases and the microstructures between the differently prepared samples significantly influence the corresponding mechanical properties of the specimens.</P>

Influence of Milk Yield, Parity, Stage of Lactation and Body Weight on Urea and Protein Concentration in Milk of Murrah Buffaloes

Roy, B.,Mehla, R.K.,Sirohi, S.K. Asian Australasian Association of Animal Productio 2003 Animal Bioscience Vol.16 No.9

The present study was carried out to investigate the effect of test day milk yield, test day evening milk yield, parity, stage of lactation and body weight on milk urea and milk protein concentration. A total of 319 milk samples was collected from buffaloes over four month's period and subjected to urea and protein analysis. Milk urea concentration (mg/dl) was significantly (p<0.01) increased with increasing test day milk yield. The lowest value ($57.03{\pm}1.13$) was observed in the milk yield group ${\leq}4.5kg/day$ and the highest value ($64.15{\pm}1.13$) in the group 7.7-10.7 kg/day. However, test day evening milk yield had no significant effect on milk urea concentration. Milk protein did not vary significantly with the test day milk yield as well as test day evening milk yield. A clear decreasing trend of milk urea concentration (mg/dl) was found with the increasing parity. The highest MU concentration ($64.03{\pm}1.14$) was found in the first parity and the lowest ($55.67{\pm}1.22$) was found in the sixth and above parity. Whereas, stage of lactation had no effect on milk urea concentration. Moreover, parity and stage of lactation did not have any significant effect on milk protein concentration. Body weight (kg) was also found negatively (p<0.05) related with urea content (mg/dl) in milk. The highest mean MU concentration ($64.34{\pm}0.88$) was found when body weight was between 532 and 598 kg and lower mean values ($59.24{\pm}0.94$ and $59.33{\pm}1.23$) were observed in 599 to 665 kg and ${\geq}666kg$ group. Body weight also had significant (p<0.05) effect on milk protein content. The highest milk protein content (%) was found in ${\geq}666kg$ group and the lowest in <531 kg group. In conclusion, for proper interpretation of milk urea values to monitor protein nutrition status of the buffaloes parity, milk yield and body weight should be considered.