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Erkal, Aslı,Erdox11f,an, Mehmet Selç,uk,Aş,ık, x130,hsan,Ekx15f,i, Haslet,Jeon, Seungwon,Solak, Ali Osman,Ü,stü,ndaf,, Zafer The Electrochemical Society 2014 Journal of the Electrochemical Society Vol.161 No.10
<P>A new electrode was prepared by the electrooxidation of orto-, meta-, and para-substituted nitro phenols on glassy carbon electrode. Electrochemical modification of the electrodes was carried out in 0.01 M HCl using cyclic voltammetry (CV). Then nitro groups in the covalently grafted nitro phenol derivatives on GC electrode were reduced to amine groups in 0.01 M HCl. The electrochemical behavior of the modified electrodes was studied in the presence of electroactive redox probes such as ferrocene and ferricyanide by CV and electrochemical impedance spectroscopy (EIS). X-ray photoelectron spectroscopy (XPS) was employed to characterize the surface structure and composition of the modified substrates. Thickness of the films was measured by using an ellipsometer. Surface topography of the nanofilms and bare GC was characterized via AFM. Graphene oxide (GO) was covalently attached on 4-aminophenyl involved surface through EDC. Simple immersing of the GO covered nanoplatform into a sample solution led to the chemical deposition by means of the interaction with Cd<SUP>2+</SUP> and Pb<SUP>2+</SUP> ions, simultaneously. Various analysis parameters that affect the simultaneous analysis of the ions such as deposition time, pH factor and deposition temperature, were optimized. Calibration curve for the GO grafted electrode surface with Square-wave anodic stripping voltammetry (SWASV) were obtained in the concentration range between 1 × 10<SUP>−8</SUP> M and 1 × 10<SUP>−12</SUP> M for Pb<SUP>2+</SUP> and Cd<SUP>2+</SUP>. The detection limits of the modified electrode for Pb<SUP>2+</SUP> and Cd<SUP>2+</SUP> ions were determined to be about 3.2 (± 0.1) × 10<SUP>−13</SUP> M and 2.4 (± 0.2) × 10<SUP>−13</SUP> M, respectively.</P>
Aguilar, M.,Ali Cavasonza, L.,Ambrosi, G.,Arruda, L.,Attig, N.,Aupetit, S.,Azzarello, P.,Bachlechner, A.,Barao, F.,Barrau, A.,Barrin, L.,Bartoloni, A.,Basara, L.,Baş,ex11f,mez-du Pree, S.,Batta American Physical Society 2018 Physical Review Letters Vol.120 No.2
<P>We report on the observation of new properties of secondary cosmic rays Li, Be, and B measured in the rigidity (momentum per unit charge) range 1.9 GV to 3.3 TV with a total of 5.4 x 10(6) nuclei collected by AMS during the first five years of operation aboard the International Space Station. The Li and B fluxes have an identical rigidity dependence above 7 GV and all three fluxes have an identical rigidity dependence above 30 GV with the Li/Be flux ratio of 2.0 +/- 0.1. The three fluxes deviate from a single power law above 200 GV in an identical way. This behavior of secondary cosmic rays has also been observed in the AMS measurement of primary cosmic rays He, C, and O but the rigidity dependences of primary cosmic rays and of secondary cosmic rays are distinctly different. In particular, above 200 GV, the secondary cosmic rays harden more than the primary cosmic rays.</P>
Aguilar, M.,Ali Cavasonza, L.,Alpat, B.,Ambrosi, G.,Arruda, L.,Attig, N.,Aupetit, S.,Azzarello, P.,Bachlechner, A.,Barao, F.,Barrau, A.,Barrin, L.,Bartoloni, A.,Basara, L.,Baş,ex11f,mez-du Pree American Physical Society 2017 Physical Review Letters Vol.119 No.25
<P>We report the observation of new properties of primary cosmic rays He, C, and O measured in the rigidity (momentum/charge) range 2 GV to 3 TV with 90 x 10(6) helium, 8.4 x 10(6) carbon, and 7.0 x 10(6) oxygen nuclei collected by the Alpha Magnetic Spectrometer ( AMS) during the first five years of operation. Above 60 GV, these three spectra have identical rigidity dependence. They all deviate from a single power law above 200 GV and harden in an identical way.</P>
Functional cortical neurons and astrocytes from human pluripotent stem cells in 3D culture
Paş,ca, Anca M,Sloan, Steven A,Clarke, Laura E,Tian, Yuan,Makinson, Christopher D,Huber, Nina,Kim, Chul Hoon,Park, Jin-Young,O'Rourke, Nancy A,Nguyen, Khoa D,Smith, Stephen J,Huguenard, John R,Ge Nature Publishing Group 2015 NATURE METHODS Vol. No.
The human cerebral cortex develops through an elaborate succession of cellular events that, when disrupted, can lead to neuropsychiatric disease. The ability to reprogram somatic cells into pluripotent cells that can be differentiated in vitro provides a unique opportunity to study normal and abnormal corticogenesis. Here, we present a simple and reproducible 3D culture approach for generating a laminated cerebral cortex–like structure, named human cortical spheroids (hCSs), from pluripotent stem cells. hCSs contain neurons from both deep and superficial cortical layers and map transcriptionally to in vivo fetal development. These neurons are electrophysiologically mature, display spontaneous activity, are surrounded by nonreactive astrocytes and form functional synapses. Experiments in acute hCS slices demonstrate that cortical neurons participate in network activity and produce complex synaptic events. These 3D cultures should allow a detailed interrogation of human cortical development, function and disease, and may prove a versatile platform for generating other neuronal and glial subtypes in vitro.
Aguilar, M.,Ali Cavasonza, L.,Ambrosi, G.,Arruda, L.,Attig, N.,Aupetit, S.,Azzarello, P.,Bachlechner, A.,Barao, F.,Barrau, A.,Barrin, L.,Bartoloni, A.,Basara, L.,Baş,ex11f,mez-du Pree, S.,Batta American Physical Society 2016 Physical review letters Vol.117 No.23
<P>Knowledge of the rigidity dependence of the boron to carbon flux ratio (B/C) is important in understanding the propagation of cosmic rays. The precise measurement of the B/C ratio from 1.9 GV to 2.6 TV, based on 2.3 million boron and 8.3 million carbon nuclei collected by AMS during the first 5 years of operation, is presented. The detailed variation with rigidity of the B/C spectral index is reported for the first time. The B/C ratio does not show any significant structures in contrast to many cosmic ray models that require such structures at high rigidities. Remarkably, above 65 GV, the B/C ratio is well described by a single power law R. with index. Delta = -0.333 +/- 0.014(fit) +/- 0.005(syst), in good agreement with the Kolmogorov theory of turbulence which predicts. Delta = -1/3 asymptotically.</P>
Properties of Cosmic Helium Isotopes Measured by the Alpha Magnetic Spectrometer
Aguilar, M.,Ali Cavasonza, L.,Ambrosi, G.,Arruda, L.,Attig, N.,Bachlechner, A.,Barao, F.,Barrau, A.,Barrin, L.,Bartoloni, A.,Baş,ex11f,mez-du Pree, S.,Battiston, R.,Becker, U.,Behlmann, M.,Beis American Physical Society 2019 Physical Review Letters Vol.123 No.18