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X. J. Chen,J. C. Xu,H. X. Jin,D. F. Jin,B. Hong,H. L. Ge,X. Q. Wang 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2017 NANO Vol.12 No.5
In this paper, ordered mesoporous SBA-15 silica was synthesized by the hydrothermal method, and then a series of CoFe2O4/SBA-15 nanocomposites were synthesized by a facile impregnation method. X-ray diffraction and N2 adsorption–desorption isotherms were used to characterize the microstructure and morphology of SBA-15 and CoFe2O4/SBA-15 nanocomposites. CoFe2O4 nanoparticles presented spinel phase structure and existed in the mesopores of SBA-15. The magnetic response of CoFe2O4/SBA-15 nanocomposites was characterized with vibrating sample magnetometer (VSM). The adsorption efficiency of CoFe2O4/SBA-15 nanocomposites for methylene blue increased firstly with the increasing CoFe2O4 content, and then decreased. Sample-2 (SBA-15: CoFe2O4 = 1: 0.1 in the precursor) not only presented the best adsorptive performance, but also could be separated and retrieved effectively by magnetic separation technique.
Q. Zhang,S. Zhou,S. F. Fu,X. Z. Wang 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2017 NANO Vol.12 No.10
"2,9,16,23-tetranitrophthalocyanine zinc (TNZnPc)/TiO2 organic–inorganic heterostructures were successfully fabricated by a simple combination method of electrospinning technique and solvothermal processing. These photocatalysts were characterized by X-ray diffraction, scanning electron microscope, transmission electron microscope, UV–Vis, energy dispersive X-ray and X-ray photoelectron spectroscopy. The photocatalytic studies revealed that the TNZnPc/TiO2 organic–inorganic heterostructures exhibited enhanced photocatalytic efficiency of photo-degradation of rhodamine B compared with pure TiO2 nanofibers under visible-light irradiation. Further studies indicate that the photosynergistic effect of organic–inorganic heterostructures can remarkably enhance the photoinduced interfacial charge transfer, thereby increasing the charge separation during the photocatalytic reaction."
Wang, T. G.,Dong, Y.,Gebrekidan, B. A.,Liu, Y. M.,Fan, Q. X.,Kim, K. H. Springer Science + Business Media 2017 Acta metallurgica sinica Vol.30 No.7
<P>The Cr-Si-N coatings were prepared by combining system of high-power impulse magnetron sputtering and pulsed DC magnetron sputtering. The Si content in the coating was adjusted by changing the sputtering power of the Si target. By virtue of electron-probe microanalysis, X-ray diffraction analysis and scanning electron microscopy, the influence of the Si content on the coating composition, phase constituents, deposition rate, surface morphology and microstructure was investigated systematically. In addition, the change rules of micro-hardness, internal stress, adhesion, friction coefficient and wear rate with increasing Si content were also obtained. In this work, the precipitation of silicon in the coating was found. With increasing Si content, the coating microstructure gradually evolved from continuous columnar to discontinuous columnar and quasi-equiaxed crystals; accordingly, the coating inner stress first declined sharply and then kept almost constant. Both the coating hardness and the friction coefficient have the same change tendency with the increase of the Si content, namely increasing at first and then decreasing. The Cr-Si-N coating presented the highest hardness and average friction coefficient for an Si content of about 9.7 at.%, but the wear resistance decreased slightly due to the high brittleness. The above phenomenon was attributed to a microstructural evolution of the Cr-Si-N coatings induced by the silicon addition.</P>
Chen, P.,Tian, Q.,Baek, S.J.,Shang, X.L.,Park, A.,Liu, Z.C.,Yao, X.Q.,Wang, J.Z.,Wang, X.H.,Cheng, Y.,Peng, J.,Shen, A.G.,Hu, J.M. WILEY‐VCH Verlag 2011 Laser physics letters Vol.8 No.7
<P><B>Abstract</B></P><P>Early and differential diagnosis of Alzheimer's disease (AD) is a problem that puzzled many doctors. Reliable markers in easy‐assembling samples are of considerable clinical diagnostic value. In this work, laser Raman spectroscopy (LRS) was developed a new method that potentially allows early and differential diagnosis of AD from the platelet sample. Raman spectra of platelets isolated from different ages of AD transgenic mice and non‐transgenic controls were collected and analyzed. Multilayer perceptron networks (MLP) classification method was used to classify spectra and establish the diagnostic models. For differential diagnosis, spectra of platelets isolated from AD, Parkinson’s disease (PD) and vascular dementia (VD) mice were also discriminated. Two notable spectral differences at 740 and 1654 cm<SUP>–1</SUP> were revealed in the mean spectrum of platelets isolated from AD transgenic mice and the controls. MLP displayed a powerful ability in the classifying of early, advanced AD and the control group, and in differential diagnosis of PD and advanced AD, as well as VD and advanced AD. The results suggest that platelet detecting by LRS coupled with MLP analysis appears to be an easy and accurate method for early and differential diagnosis of AD. This technique could be rapidly promoted from laboratory to the hospital. (© 2011 by Astro Ltd., Published exclusively by WILEY‐VCH Verlag GmbH & Co. KGaA) (© 2011 by Astro Ltd., Published exclusively by WILEY‐VCH Verlag GmbH & Co. KGaA)</P>
Sun, G.A.,Wang, X.L.,Wang, Y.D.,Woo, W.C.,Wang, H.,Liu, X.P.,Chen, B.,Fu, Y.Q.,Sheng, L.S.,Ren, Y. Elsevier Sequoia 2013 Materials science & engineering. properties, micro Vol.560 No.-
High-energy synchrotron X-ray diffraction technique was used to in-situ characterize microstructure, lattice strain, and phase transition behavior of a Ni<SUB>47</SUB>Ti<SUB>44</SUB>Nb<SUB>9</SUB> shape memory alloy. Phase transformation kinetics and deformation mechanisms were studied under a uniaxial tension at three testing temperatures, i.e., -70<SUP>o</SUP>C, 25<SUP>o</SUP>C, and 150<SUP>o</SUP>C. At a testing temperature of -70<SUP>o</SUP>C, a complicated phase transformation with four stages of micromechanical deformation was identified which is associated with changes of martensite substructures. At room temperature of 25<SUP>o</SUP>C, there was no stress-induced selection process of variants of B19' phases observed. Whereas at a testing temperature of 150<SUP>o</SUP>C, there was no any phase transformation observed. It is verified that β-Nb phase, an effective stabilizer for the austenite, delays the process of martensitic transformation and relaxes the strain energy without strengthening the matrix. This new finding is important to understand the relationship between the micromechanical deformation behavior and phase transformations in the Ni<SUB>47</SUB>Ti<SUB>44</SUB>Nb<SUB>9</SUB> SMA.
Microwave Absorption and Magnetic Properties of Cobalt Ferrites/Carbon Nanotubes Nanocomposites
B. B. Zhang,P. F. Wang,J. C. Xu,Y. B. Han,H. X. Jin,D. F. Jin,X. L. Peng,B. Hong,J. Li,J. Gong,H. L. Ge,Z. W. Zhu,X. Q. Wang 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2015 NANO Vol.10 No.5
Owing to the unique microstructure and the excellent dielectric properties, carbon nanotubes(CNTs) were decorated with CoFe2O4 nanoparticles to synthesize the CoFe2O4/CNTs nanocomposites by the solvothermal method. The phase structure, morphology, magnetic properties and microwave absorption performance of the as-prepared CoFe2O4/CNTs were characterized and discussed by X-ray diffraction (XRD), thermal gravity analysis (TGA), transmission electron microscope (TEM), vibrating sample magnetometer (VSM) and vector network analyzer (VNA). All results indicated that the diameter of CoFe2O4 nanoparticles decorating on the surface of CNTs increased with the solvothermal temperature. CoFe2O4/CNTs prepared at 180℃, 200℃ and 220℃ exhibited superparamagnetism, while the other samples presented ferromagnetism at room temperature. And with the increasing solvothermal temperature, the saturation magnetization and coercivity increased up to 72 emu/g and 2000 Oe for the sample prepared at 260℃ (S-26). And the reflection loss of CoFe2O4/CNTs nanocomposites increased with the solvothermal temperature up to -15.7 dB for S-26 with the bandwidth of 2.5 GHz.
Wang J.J.,Deng Q.J.,He Y.Y.,Feng Y.N.,Kang M.P.,Duan X.L.,Yang Y.L. 한국물리학회 2022 Current Applied Physics Vol.39 No.-
CCTO (Calcium copper titanate) powder as inorganic filler was synthesized by the Sol-gel method firstly. CCTO/ PVDF (Polyvinylidene fluoride) composite was fabricated by solution mixing based on high temperature resistance of PVDF and insulated property of CCTO. The composite of CCTO/PVDF were characterized by X-ray diffraction, Fourier Transform infrared spectroscopy, Scanning Electron Microscope and impedance analysis. The results showed that the addition of CCTO and increasing in its content did not affect the phase- and microstructure of the composites,but the increase of CCTO content can induce the generation of C–F new bonds. PVDF/CCTO composites were enhanced in performance of thermal and frequency-depended stability with increasing in the fraction of CCTO. The dielectric constant of CCTO/PVDF composite materials with 50% CCTO achieved to a maximum value of 50 almost, which is 5 times higher the pure PVDF. The conductivity felled into 10-8 to 10-1 S m-1 during the frequency of 102–108 Hz. The composite material would be expected to be applied in the field of integrated circuit.