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고상추출카트리지를 이용한 잔류농약 다중분석과정에서 정제용매에 따른 회수율 비교
두옥주,정보경,김경식,정의근,김진곤,김명희 한국환경농학회 2002 한국환경농학회지 Vol.21 No.2
채소류 중 비교적 matrix효과가 적고, 수분 함량이 적절하여 회수율이 양호한 오이를 대상으로 하여 총 16종의 농약 성분을 A, B 두 group으로 나누어, 농약의 동시 다성분 분석의 전처리 과정 중 정제에 사용하는 용출용매로서 5%~20%의 acetone/hexane과 5%~20%의 ethyl acetate/hexane을 사용하여 각각의 회수율을 분석하여 얻은 결과는 다음과 같다. Acetone/hexane을 사용한 경우 5% acetone에서 총 16종의 농약 성분 중 ethalfluralin, trifluralin, chlorothalonil 등 11종의 농약은 높은 회수율을 보였으나, alachlor와 iprodione, endosulfan sulfate, bifenthrin, fenarimol은 매우 낮은 회수율을 나타내었고, 10% 이상의 acetone/hexane에서는 bifenthrin과 fenarimol 제외한 14종의 농약에서 높은 회수율을 얻을수 있었다. 그러나 bifenthrin은 20%의 acetone/hexane을 사용한 경우는 용출되지 않았고, fenarimol은 10% 이하의 acetone/hexane을 사용하였을 때는 낮은 회수율을 나타냈었다. Ethyl acetone/hexane을 사용하여 총 16 종의 농약 성분의 회수율 분석을 한 결과, 5% ethyl acetone에서 ethalfluralin, α-endosulfan, β-endosulfan (A group), vinclozolin, tetradifon, cyprethrin, fenvalerate (B group)에서만 70% 이상의 회수율을 얻었다. 10%의ethyl acetone/hexane을 사용하여 분석한 경우는 trifuralin, chlorothalonil, α-endosulfan, β-endosulfan, endosulfan sulfate(A group), vinclozolin, procymidone, tetradifon, cypermethrin, 그리고 fenvalerate(B group) 에서는 70% 이상의 회수율을 얻었고, 20%의 cthyl acetone/hexane 을 사용하여 분석한 경우는 5%나 10%의 ethyl acetone/hexan 을 사용하여 분석했을 때보다 좋은 결과를 나타내어 전체 16종의 농약 중 14종에서 75% 이상의 회수율을 얻었으나, alachlor와 bifenthrin은 매우 낮은 회수율을 보여서 ethyl acetate 와 hexane의 혼합용매가 이들 두 농약성분의 분석에는 적합하지 않은 용출 용매임을 알 수 있었다. A study was carried out to optimize the cleanup step using a solid-phase extraction (SPE) cartridge, SupelClean^(TM) Florisil, for multiresidue analysis of 16 pesticides in cucumber matrix. Eluting efficiencies of two solvent systems including acetone/n-hexane and ethyl acetate/n-hexane mixtures were critically evaluated by recoveries of target anaytes from the SPE Florisil column. Based on the recovery as a measure of eluting efficiency, an acetone/n-hexane (20/80,v/v) mixture provided more than 80% recovery for 15 pesticides except bifenthrin. In case of ethyl acetate/n-hexane, 14 pesticides showed recoveries higher than 75%, while those for alachior and bifenthrin were less than 30%.
장보경 ( Bo Gyung Jang ),최윤지 ( Yoon Ji Choi ),황정임 ( Jeong Im Hwang ) 한국농촌지도학회 2011 농촌지도와 개발 Vol.18 No.3
The purpose of the study was to identify the needs assessment for urban agricultural program. The findings were as follows; Citizens at urban cities said that educational program of ``shortage of farming technology education`` should be developed, and wanted to be given ``farming technology`` of urban agriculture education area more than other education areas. The citizens asked for urban agricultural program with both theories and practice education than existing urban agricultural program that relied upon basic theory education. And, they wanted urban agricultural program that was based on ``farming technology`` to consist of practice education and theory education at the ratio of 80 and 20 and to be professional and differentiated. The citizens preferred 3 to 6 months of education period the most, and more than 95 percent of them wanted to join the program when it is developed.
장보경(Bo-Gyung Jang),최윤지(Yoon-Ji Choi),황정임(Jeong-Im Hwang) 한국농어촌관광학회 2013 농어촌관광연구 Vol.20 No.2
The study has investigated cases of promotion of farm village experience tourism. The purpose of the study is to help urban migrants to rural who are interested in farm village experience tourism project and want to promote and give materials to the migrants and let them contribute to the project. The subject is urban migrants to rural who have settled down in farming villages to promote farming village experience tourism project. The findings are: The urban migrants have difficulties at economic hardship, lack of public relations for invitation of customers, subscription to insurance to keep visitors’safety, lack of accommodation facilities for visitors, lack of experience program and/or manuals, and progress methods of farm village experience program. So, the study has given implications.
Dohyung Kee,Bo Gyung Jeong,Jae Chun Lee,Kyung Min Hwang,Han Byel Lee 대한인간공학회 2014 大韓人間工學會誌 Vol.33 No.2
Objective: This study aims to develop a new desk with a built-in bookholder and desktop-mounted sliding drawer for reducing stress of seated reading postures and to analyze its effect. Background: It is general for readers to bend their back and neck when reading books on desks, which may result in high back and neck postural stress. In addition, postures using vertically layered drawers positioned at the side of users may be awkward. Method: For reducing the postural stress, a new desk with a built-in bookholder and sliding drawer was developed based on a standard of KS G 4208 for student desk. The muscle activities of reading postures on both existing and new desks were measured using EMG, in which seven male and three female college students participated. The postural stress, and musculoskeletal discomfort and ease of usage for existing and new drawers were analyzed by RULA and questionnaire survey, respectively. Results: Compared to existing desk, the muscle activity for the new desk with a bookholder was reduced by 47% when reading books. In addition, musculoskeletal discomforts in the shoulder, neck and low back were significantly lower when using the new desk with a bookholder. Although the stresses for postures using the desktopmounted sliding drawer and general drawer were not significantly different, the questionnaire survey revealed that the new desktop-mounted sliding drawer is easier to use. Conclusion: A new desk developed in this study significantly reduced postural stress and enhanced subjective preference when reading. Application: This would be useful when developing new desks with low postural stress.