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RISS 인기검색어
- 검색키워드
- 저자 : Mustafa Serdar Karakaş (검색결과 3 건)
- 무료
- 기관 내 무료
- 유료
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Properties and Corrosion Resistance of AISI H13 Hot-Work Tool Steel with Borided B4C Powders
Ali Günen,İsmail Hakki Karahan,Mustafa Serdar Karakaş,Bülent Kurt,Yusuf Kanca,Vedat Veli Çay,Murat Yıldız 대한금속·재료학회 2020 METALS AND MATERIALS International Vol.26 No.9
In this study, the surface of AISI H13 steel was borided with powder blends of B4Cand NaBF4using the powder-pack methodat 800, 900 and 1000 °C for 2, 4 and 6 h. The structural and mechanical characteristics of the boride layers formed on thesurface were characterized using scanning electron microscopy, energy dispersive spectroscopy, X-ray diffractometry, 2Dsurface profilometry, microhardness and electrochemical corrosion (3.5 wt% NaCl) tests. The boride layer exhibited a singlephase structure (Fe2B) in samples coated at 800 °C and a dual-phase structure (FeB + Fe2B) at higher boriding temperatures(900 and 1000 °C). The boride layers were compact and crack-free in all boriding conditions. Depending on boridingparameters, the thickness, hardness and average surface roughness (Ra) of the coatings were found to range between 5.81and 102.46 μm, 1635–1915 HV and 0.315–0.650 μm, respectively. The borided AISI H13 steel displayed up to 33.5 timesand 2.4 times higher corrosion resistance than untreated AISI H13 steel and martensitic AISI 431 steel, respectively. Thissuggests potential use of borided AISI H13 steel in the steam turbines and marine applications as an alternative to the morecostly martensitic and duplex stainless steel grades. The corrosion resistance depended on the phase structure (single- ordual-layer), density, thickness and surface roughness of the boride coatings.
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Pack-Boriding of Monel 400: Microstructural Characterization and Boriding Kinetics
Ali Günen,Mourad Keddam,Azmi Erdoğan,Mustafa Serdar Karakaş 대한금속·재료학회 2022 METALS AND MATERIALS International Vol.28 No.8
Monel 400 was pack-borided in the temperature range of 1173–1273 K for exposure times of 2–6 h. The boride layersproduced on the surface of the alloy were examined by scanning electron microscopy and phase identification was carriedout by X-ray diffraction. The topmost layer on the borided Monel 400 was compact and contained the Ni2Bphase whilethe diffusion zone contained grain boundary precipitates of borides. Boride layers of 35–290 μm thickness and 1002–1476HV0.025hardness were obtained. SEM observations revealed a smooth interface between the boride layer and the diffusionzone. A kinetic model based on the integral method was applied to investigate the kinetics of Ni2Blayer. The boron activationenergy in the Ni2Blayer was estimated as equal to 300.7 kJ mol−1. An experimental validation of the model was madeby comparing the experimental layer thicknesses obtained, after boriding at 1198 K for 1 and 3 h, with predicted values.
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The Effect of Boronizing on the Magnetization Behaviour of Low Carbon Microalloyed Steels
Adnan Calik,Mustafa Serdar Karaka?,Nazim Ucar,Omer Bari? Aytar 한국자기학회 2012 Journal of Magnetics Vol.17 No.2
The change of saturation magnetization in boronized low carbon microalloyed steels was investigated as a function of boronizing time. Specimens were boronized in an electrical resistance furnace for times ranging from 3 to 9 h at 1123 K. The metallurgical and magnetic properties of the specimens were investigated using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD) and vibrating sample magnetometry (VSM). A boride layer with saw-tooth morphology consisting of FeB and Fe₂B was observed on the surface, its thickness ranged from 63 ㎛ to 140 ㎛ depending on the boronizing time. XRD confirmed the presence of Fe₂B and FeB on the surface. The saturation magnetization decreased with increasing boronizing time. This decrease was attributed to the increased thickness of the FeB and Fe₂B phases. Cracks were observed at the FeB/Fe₂B interfaces of the samples. The number of interfacial cracks increased with increasing boronizing time.
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