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파괴표면분석을 통한 WC-Co복합재료의 Fracture Toughness측정방법과 Failure Behavior
한동빈,J.J Mecholsky, Jr. 한국세라믹학회 1989 한국세라믹학회지 Vol.26 No.5
Specimens of WC-Co were indented to measure the resulting crack size and unindented samples were fractured in 3-point flexure to obtain the strength and to measure characteristic features on the fracture surface. Fracture toughness was determined using fractography and compared to those determined using identation techniques. We show that principles of fracture mechanics can be applied WC-Co composites and can be used to analyze the fracture process. The fracture surfaces were examined by scanning electron microscopy and optical microscopy. Characteristic feature observed in glasses, single crystals and polycrystalline materials known as mirror, mist, hackle, and crack branching were identified for these composites. We discuss the importance of fracture surface analysis in determining the failure-initiating sources and the failure behaviorof WC-Co composites.
Fe-Scale과의 반응에 의한 $Cr_3C_2$계 복합체의 산화손상
한동빈,홍기곤,박병학 한국세라믹학회 1994 한국세라믹학회지 Vol.31 No.7
In a salb-preheating furnace of steel-making industry, the oxidation/degradation behavior of Cr3C2 ceramic composited dkid button reaction with scale in Fe-oxide system occurs and was thermodynamically examined. The reaction of scale with Cr3C2 skid button produces Cr3C2(s) and C(s), and Co gas is then evolved from the reaction of C(s) with Fe-scale. Cr3C2(s) from oxidation of Cr3C2(s) reacted with Fe-oxide(s) becomes high-melting chromite. The chromite acts as protection layer against further oxidation and improves resistance of the reaction of Cr3C2 skid button with Fe-scale.
한동빈,박병학,김영우,배원수 한국세라믹학회 1999 한국세라믹학회지 Vol.36 No.5
Recently regenerative burner system was developed and begins to be gradually used for better energy savings. Compared to conventional burner system the regenrative one has the several merits such as higher fuel efficiency light weigh of apparatus low harmful toxic gas and homogeneous heating zone etc. The regenerative material a very important component of the new regenerative burner system should possess the properties of low specific density higher surface area and high specific heat capacity. Ceramics is the best regenerative material because of stable mechanical properties even at high temperature and better thermal properties and excellent chemical stability. In this study alumina ball alumina tube 3-D ceramic foam and hoeycomb as regenerative materials were tested and evaluated. The computer silumation was conducted and compared to the result of field test. This paper is aimed to introduce a new application of ceramics at high temperature.
Mechanical Properties and Failure Analysis of $Al_2O_3/ZrO_2$ Composites
홍기곤,한동빈,Hong, Gigon-Hong,Han, Dong-Bin Materials Research Society of Korea 1992 한국재료학회지 Vol.2 No.3
$Al_2O_3/ZrO_2$복합분말에 상릉분말을 침가하여 상압소결법으로 $Al_2O_3/ZrO_2$복합체를 제조한 후, 밀도, 강도, 경도 및 파괴인성등의 물성을 측정하였으며 미세구조 및 파괴단면도 관찰하였다. 상용분말의 침가량이 중량비로 50%이하인 경우에는 평균 꺽임 강도가 640 MPa정도로 거의 변화가 없었으며, 50%이상 첨가된 경우에는 강도가 저하되었는데, 이는 미세조직과 관계가 있는 것으로 생각된다. 또한 파괴인성(4.3-5.3 $Mpam^{1/2}$)값은 상용분말 첨가량에 비례하여 증가하였다. 파괴단면 관찰결과 파괴원인으로는 가공에서 생기는 표면 결함, $ZrO_2$ agglomeration에 의한 crack-like void 및 $Al_2O_3/ZrO_2$ nano복합체 분말과 상용분말간의 소결성 차이에서 생기는 계면 분리등이 관찰되었는데, nano 복합 분말만을 사용한 소결체에서는 가공에 의한 표면 결함만이 파괴원으로 작용하였다. 또한, 파괴형태는 주로 transgranular fracture이었다 $Al_2O_3/ZrO_2$ composites were fabricated by pressureless sintering from commercial powders and/or nano composite powder of $Al_2O_3/ZrO_2$. The Properties of the composites such as density, strength, hardness and fracture toughness were evaluated. Microstructures and fracture surfaces ware also examined. The flexural strength remains unchanged(~640 MPa) as long as the content of commercial powders is not extreamly high, and depends on microstructures of the composites. Fracture toughness(4.3-5.3 $Mpa{\cdot}m^{1/2}$) increases with increasing content of commercial powders. Fractography shows that failure-initiating sources are 1)surface flaws resulting from machining damage, 2)crack-shaped voids formed due to $ZrO_2$ agglomeration, and 3)surface separation caused by inhomogeneous blending and by sinterability difference between nato composite powder and commercial powders of $Al_2O_3/ZrO_2$. Failure mode of the composites was mainly transgranular.
김지환,한동빈,김기태 한국세라믹학회 1995 한국세라믹학회지 Vol.32 No.11
Creep behaviors of Cr3C2 composites containing 90 wt% Cr3C2 and 10 wt% Ni were studied at high temperature. Compression tests at 100$0^{\circ}C$ and bending tests at 100$0^{\circ}C$ and 105$0^{\circ}C$ were done in argon environment. In all test conditions primary and steady-state creep behaviors were observed. Stress exponent and activatiion energy were determined from the experimental data. By microstructural analysis of Cr3C2 composites after creep test, the separate agglomerations of Ni phase were observed. Numerical analysis was also studied to analyze bending creep behaviors of Cr3C2 by assumming different tensile and compressive creep behavior in a bending sample. From the analysis, it was found that the stress state at the compressive region as applied stress increased. The observed creep rates were compared with the predicted creep rates by estimating power-law creep parameters from bending test data.
Screen Printable MoSi<sub>2</sub> 도전성 Paste를 이용한 세라믹 면상 발열체 제조
김배연,한동빈,정철원,Kim, Bae-Yeon,Han, Dong-Bin,Jeong, Cheol-Weon 한국세라믹학회 2010 한국세라믹학회지 Vol.47 No.4
Screen printable $MoSi_2$ paste and its ceramic sheet heater were investigated. $MoSi_2$ powder without $Mo_5Si_3$ second phase, which causes so-called pest phenomena, was synthesized by SHS technique. Over glaze was also developed for preventing pest phenomenon. The maximum temperature of $MoSi_2$ ceramic heater was over $500^{\circ}C$. After several heat up and cooling cycle, the $MoSi_2$ heater reveals pest phenomenon. Conductive $MoSi_2$ paste could be used in electronic ceramics, i.e., MLCC, LTCC, HTCC, and etc.
Screen Printable MoSi2 도전성 Paste를 이용한 세라믹 면상 발열체 제조
김배연,한동빈,정철원 한국세라믹학회 2010 한국세라믹학회지 Vol.47 No.4
Screen printable MoSi2 paste and its ceramic sheet heater were investigated. MoSi2 powder without Mo5Si3 second phase, which causes so-called pest phenomena, was synthesized by SHS technique. Over glaze was also developed for preventing pest phenomenon. The maximum temperature of MoSi2 ceramic heater was over 500oC. After several heat up and cooling cycle, the MoSi2 heater reveals pest phenomenon. Conductive MoSi2 paste could be used in electronic ceramics, i.e., MLCC, LTCC, HTCC, and etc.