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- 저자 : 이재욱 ( Jae Woog Lee ) (검색결과 4 건)
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다양한 온도 조건에서의 ZnS:Mn/ZnS 코어-쉘 양자점의 합성 및 광 특성에 관한 연구
이재욱,황청수,Lee, Jae-Woog,Hwang, Cheong-Soo 대한화학회 2009 대한화학회지 Vol.53 No.6
본 논문에서는 ZnS:Mn/ZnS 코어-쉘 양자점을 유기금속전구체의 열분해 방법으로 합성하였다. 쉘의 형성온도를 135$^{\circ}C$로 고정한 반면 코어 나노입자의 합성 온도 조건을 다양화 하여 각 조건하에서 형성된 양자점들의 특성을 조사하였다. 실험을 통해 얻은 양자점들은 UV-Vis, 액체 photoluminescence (PL) spectroscopy 방법으로 광 특성을 조사하였으며, 또한 XRD, HR-TEM, 및 EDXS 분석으로 입자크기와 조성 등을 측정하였다. 실험 결과 가장 좋은 광 특성을 보인 나노입자의 합성조건은 코어와 쉘 모두 135$^{\circ}C$인 것으로 밝혀 졌으며, 이 조건에서 얻은 양자점은 583 nm 의 PL 발광 피이크와 42.15%의 높은 양자효율을 나타내었다. HR-TEM 으로 측정한 ZnS:Mn/ZnS 양자점의 평균 입자크기는 지름이 약 4.0 - 5.4 nm 정도였으며, 특히 150$^{\circ}C$의 온도 조건에서는 타원형의 입자가 형성되는 것이 관찰되었다. ZnS:Mn/ZnS core-shell quantum dots (QDs), were synthesized via a thermal decomposition reaction of organometallic precursors in a hot solvent mixture. The synthetic conditions of the quantum dots were monitored at various reaction temperatures for the core formation, while the shell formation temperature was fixed at 135$^{\circ}C$. The obtained colloidal nanocrystals at corresponding temperatures were characterized by UV-Vis, solution photoluminescence (PL) spectroscopies, and further obtained powders were characterized by XRD, HR-TEM, and EDXS analyses. The synthetic temperature condition to obtain the best PL emission intensity for the core-shell QD was 135$^{\circ}C$, for both core and shell formation. At this temperature, solution PL spectrum showed a narrow emission peak at 583 nm with a relative PL quantum efficiency of 42.15%. In addition, the measured spherical particle sizes for the ZnS:Mn/ZnS nanocrystals via HR-TEM were in the range of 4.0 to 5.4 nm, while ellipsoidal particles were obtained at 150$^{\circ}C$.
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석동화,오창하,이재욱,Suk, Dong Hwa,Oh, Chang Ha,Lee, Jae Woog 한국압력기기공학회 2010 한국압력기기공학회 논문집 Vol.6 No.2
In this study, the axial ODSCC occurrence of domestic OPR 1000 steam generator tube was caused by the tube weakness and the sludge accumulation in the secondary side of steam generator. Inconel 600 HTMA used as tube material is related to most of tube leakage accidents in the world and also these ODSCCs were detected mainly at the 5th TSP(Tube Support Plate) to the 8th TSP of hot leg side. These elevations(5th TSP to 8th TSP) pave the way for the sludge accumulation. As a result of EC(Eddy Current) Bobbin and RPC data analysis, ODSCCs were occurred at contact points of tube and tube support plate. The more accumulated sludge, the higher occurrence frequency of ODSCC.
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고원석 ( Won Seok Koh ),이재욱 ( Jae Woog Lee ),임정철 ( Jeong Cheol Im ),한재철 ( Jae Cheol Han ),이희문 ( Hee Mun Lee ) 한국가축위생학회 2005 韓國家畜衛生學會誌 Vol.28 No.2
In order to monitor the parasites, 204 fecal samples were taken from Korean indigenous goats of Iksan-branch. Then identification of the parasites was determined by the fecal examination using the floatation and microscopical examination, respectively. The detection of rates was 91.2%, and mixed infection rates were single 38.7%, double 28.4%, triple 15.2%, Quadraple 6.9% and Qunituple 20.0%. The isolated were identified as Eimeria spp from 169 heads, Strongyloides papillosus from 56 heads, Ostertagia spp from 24 heads, Trichostrongylus spp from 22 heads, Moniezia expensa from 18 heads, Oesophagostomum spp from 17 heads, Bonostomum spp from 12 heads, Cooperia spp from 12 heads, Heamonchus spp from 8 heads and Capillaria spp from 2 heads.
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고원석 ( Won Seok Koh ),이재욱 ( Jae Woog Lee ),허철호 ( Cheal Ho Hur ),배정준 ( Jeong Joon Bae ),이희문 ( Hee Moon Lee ),김종승 ( Chong Sung Kim ),양홍지 ( Hong Ji Yang ) 한국가축위생학회 2004 韓國家畜衛生學會誌 Vol.27 No.2
In order to monitor the parasites, 83 fecal samples were taken from monkeys such as Cercopithecus mitis(6), Macaca fuscata(32), Saimiri sciurea(27), Macaca nigra(5), Papio hamadrysa(8), and Macaca mulatta(5) in Jeonbuk area. Isolation and Identification of the parasites from the feces were determined by the fecal examination using the floatation and microscopical examination, respectively. The detection rate was 21.6%, and mixed infection rate was single 18.0%(15 heads), double 2.4%(2 heads), and triple 1.2% (1 head). The isolates were identified as Strongyloides axei from 7 heads. Trichuris spp from 3 heads, Entamoeba histolytica 3 heads, Toxacaris leonina from 3 heads, and Eimeria spp from 2 heads.
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