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멥쌀과 찹쌀중의 지방질 함량 및 중성 지방질의 조성에 관한 비교
신효선,이종용,Shin, Hyo-Sun,Lee, Jong-Yong 한국식품과학회 1986 한국식품과학회지 Vol.18 No.2
우리나라에서 재배된 4품종의 멥쌀과 2품종의 찹쌀 중의 지방질의 함량과 중성지방질의 조성에 대하여 비교 연구하였다. 멥쌀과 찹쌀 중의 총지방질의 평균함량은 건물중량 기준으로 각각 0.94% 및 1.78% 였다. 총지방질 중의 중성지방질, 당지방질, 인지방질의 함량비는 멥쌀에서는 76.5 : 14.8 : 8.6% 이였고, 찹쌀에서는 82.4: 11.1 : 6.5% 였다. 중성지방질의 주요 성분은 triglyceride, free fatty acid, steryl ester, free sterol, monoglyceride 및 diglyceride 였으며, 이들 함량은 멥쌀과 찹쌀간에 유의적인 차이가 없었다. 멥쌀과 찹쌀 중의 총지방질과 중성지질의 구성 주요 지방산은 linoleic, oleic및 palmitic acid 였다. The lipids content and neutral lipid component of milled rice grain were studied for four nonglutionous and two glutinous varieties grown in Korea. The average total lipid contents in nonglutinous and glutinous varieties were 0.94% and 1.78% by dry weight basis, respectively. The ratios of neutral lipid, glycolipid and phospholipid in the total lipid were 76.5 : 14.8 : 8.6 in the nonglutionous and 82.4 : 11.1 : 6.5 in the glutinous, respectively. Main classes of the neutral lipids were triglycerides, free fatty acids, steryl esters, free sterols, monoglycerids and diglycerides in both of nonglutinous and glutinous, and no significance was observed in the content of the classes between both varieties. The major fatty acid composition of total and neutral lipids were linoleic, oleic and palmitic acids in both of nonglutinous and glutinous varieties.
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옥수수기름과 극도경화대두 혼합유의 이화학적 성질에 대한 무작위 에스테르 교환의 영향
신효선,정광현,전제현,Shin, Hyo-Sun,Chung, Kwang-Hyun,Chun, Je-Hyun 한국식품과학회 1991 한국식품과학회지 Vol.23 No.3
가정용 마아가린의 물성에 적합한 원료유지를 제조하기 위하여 옥수수기름(corn germ oil, CGO)과 극도경화 대두유(fully hydrogenated soybean oil, FHSO)의 혼합유를 무작위 에스테르 교환하였을 때 이들 혼합유의 이화학적 성질의 변화를 연구하였다. 에스테르 교환은 triglyceride 조성을 분석한 결과 $80^{\circ}C$에서 sodium methoxide를 0.4% 사용하였을 때 35분만에 반응이 완결되었다. 융점과 고체지 함량은 에스테르 교환에 의해 현저하게 감소하였고, 거칠고 큰 결정형태는 미세하고 균일한 크기로 변화하였다. 에스테르 교환 전후의 지방산 조성은 변화가 없었으나, triglyceride 조성은 상당한 변화를 나타내었다. PN별로 triglyceride 조성을 분석한 결과 PN 42, 44, 52 및 54는 감소하였는데 이는 $GU_3$와 $GS_3$의 감소와 관련이 있으며, PN 46, 48 및 50은 증가 하였는데 이는 $GU_2S$와 $GUS_2$의 증가와 관련있는 것으로 판단되었다. 본 연구에서 융점, 고체지 함량, 결정형태 등의 변화와 지방산 조성으로 볼 때 CGO와 FHSO를 80 : 20과 75 : 25로 혼합하여 에스테르 교환한 것이 가장 바람직한 물성과 영양성을 갖는 가정용 마아가린의 원료 유지임을 알 수 있었다. Effect of random interesterification on the physicochemical properties in blends of corn germ oil and fully hydrogenated soybean oil was studied. Interesterification by using 0.4% sodium methoxide at $80^{\circ}C$ was completed in 35 minutes as determined by HPLC analysis for triglyceride composition. Changes of melting point, solid fat content, crystal form, fatty acid and triglyceride composition was investigated. After the interesterification, melting point and solid fat content were decreased, and coarse and large crystals were modified to fine and uniform. Fatty acid composition was not altered but triglyceride composition was largely altered. Interesterified blends of corn germ oil and fully hydrogenated soybean oil made with 80%, 20% and 75%. 25%, respectively, had desirable characteristics of the margarine for home use.
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신효선,양주홍,Shin, Hyo-Sun,Yang, Joo-Hong 한국식품과학회 1986 한국식품과학회지 Vol.18 No.2
우리나라에서 재배된 4품종의 멥쌀과 2품종의 찹쌀 중의 극성지방질의 조성에 대하여 비교 연구하였다. 멥쌀과 찹쌀 중의 당지방질의 주요성분은 esterified sterylglycosides, monogalactosyl diglycerides, steryl glycosides, digalactosyl diglycerides 및 cerebrosides 였으며, 이들 함량은 멥쌀과 찹쌀간에 유의적인 차이가 없었다. 멥쌀과 찹쌀 중의 인지방질의 주요성분은 Iysophosphatidyl cholines, phosphatidyl cholines, phosphatidyl inositols 및 phosphatidyl ethanolamines 이였다. 그러나 lysophosphatidyl cholines과 phosphatidyl cholines은 멥쌀이 찹쌀에서 보다 많이 함유되어 있었고. phosphatidyl ethanolamines 과 phosphatidyl inositols는 찹쌀이 멥쌀에서 보다 많이 함유되어 있었다. 멥쌀과 찹쌀의 당 및 인지방질 획분의 주요 지방산은 palmitic, linoleic 및 oleic acid였다. 그러나 당지방질 획분 중의 palmitic acid는 멥쌀이 찹쌀에서 보다 함량이 높았고, 인지방질 획분 중의 oleic 및 stearic acid는 멥쌀이 찹쌀에서보다 적었으나, linoleic acid는 멥쌀이 찹쌀에서 보다 많았다. The composition of glycolipids and phospholipids of milled rice grain were studied for four nonglutinous and two glutinous varieties grown in Korea. Main classes of the glycolipids were esterified sterylglycosides, monogalactosyl diglycerides, steryl glycosides, digalactosyl diglycerides and cerebrosides in both of nonglutinous and glutinous, and no differences in individual content of the classes between both varieties. Of the phospholipids, Iysophophatidyl cholines, phosphatidyl cholines, phosphatidyl ethanolamines, phosphatidyl inositols and phosphatidyl serines were the major components, comprising oveer 85% of this class, and smaller amounts of diphosphatidyl glycerols and phosphatidyl glycerols were present. There was significant differences individual content of the phospholipid classes between both varieties. The major fatty acids of glycolipids and phospholipids fractions were palmitic, linoleic and oleic acids in both of nonglutinous and glutinous varieties. But content of palmitic acid in glycolipids fraction and stearic, oleic and linoleic acids in phospholipids fraction showed significant differences between both varieties.
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상이한 조건하에서 저장한 압출보리의 품질특성에 관한 이화학적 평가 -제 2 보 : 비효소적 갈색화-
신효선,제이아이그레이,에스엘큐페트,Shin, Hyo-Sun,Gray, J. Ian,Cuppett, Susan L. Korean Society of Food Science and Technology 1983 한국식품과학회지 Vol.15 No.3
3가지 다른 조건하에서 제조된 압출보리와 생보리를 0.31 및 0.71의 수분활성과 $25^{\circ}C$ 및 $40^{\circ}C$의 온도에서 각각 4개월 저장하면서 색도, 갈색화지수, 가용성 단백질, 환원당 및 유효성 리진의 변화에 대한 수분활성과 온도의 영향에 대하여 연구하였다. 저장기간의 경과와 함께 수분활성과 온도가 증가함에 따라 모든 시료에서 백색도의 손실이 증가하였다. 생보리는 압출보리보다 저장중 갈색화 지수의 증가가 심하였고, 설탕을 첨가하여 제조한 압출보리는 다른 압출보리보다 저장중 갈색화가 적었다. 수분활성과 온도가 증가함에 따라 모든 시료중의 환원당, 가용성 단백질 및 유효성 리진의 함량이 감소하였으며, 이와같은 결과는 저장중 Maillard반응에 의한 것임을 알았다. Change of color, browning index, soluble protein, reducing sugar content, and available lysine were monitored for raw and extruded barely powders during four months of ambient and accelerated storage temperatures with $A_w$ of 0.31 and 0.71, respectively. Loss of whiteness and soluble browning pigments increased with increased $A_w$ and temperature. The raw sample had an increased rate of browning intensity than the extruded samples. Among the extruded samples, the added sucrose sample had the lowest rate of browning during storage. Loss of reducing sugar content in all samples increased with increased $A_w$ and temperature. The loss of soluble protein and of the available lysine also increased with increased $A_w$ and temperature. The loss of reducing sugar and of the available lysine was at least partly due to the Maillard browning reaction. These results have important implications in teh processing and storage of raw and extruded burleys.
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신효선(Hyo-Sun Shin) 한국식품과학회 2017 식품과학과 산업 Vol.50 No.4
In Korea, sesame oil has been used as a flavor source mainly by edible oil since ancient times, and it has been used by domestic screw pressing. In the 1960’s, the demand for edible oils and fats increased significantly due to the improvement of national income and changes in food consumption patterns. In the early 1970’s, a few edible oil manufacturing companies with modern solvent extraction and refining plants were established. In Korea, edible oil manufacturers account for more than 85% of employees with 50 or fewer employees. In Korea, there is a very shortage of raw materials for edible oils and fats, domestic production of edible oil is decreasing year by year and import volume is continuously increasing. While importing the edible oil bearing ingredients including soybean and extracted oil in the past, recently mainly imports crude oil and refines it in Korea. Soybean oil, palm oil and tallow account for 70~90% of total imported edible oils. Due to the recent well-being trend, the demand for olive, canola and grapeseed oils as household edible oil has increased and the production of blended oil has been greatly increased. Since the late 1980’s, people have recognized edible oil and fat as a food instead of seasoning ingredient and have increased their edible oil and fat intake in Korea. Since the early 2000’s, refined oil and fat products produced in Korea have been exported and is increasing every year.
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신효선(Hyo-Sun Shin) 한국식품영양과학회 1990 한국식품영양과학회지 Vol.19 No.5
Processing, preparation and storage of foods can produce a wide variety of actually or potentially toxic substances, such as pyrorganic toxicants(polycyclic aromatic hydrocarbons, toxicants derived from amino acids, acrolein), nonpyrorganic toxicants derived from amino acids(premelanoidine), toxicants derived from oxidation of fats and oils(toxicants in rancid and heated fats and oils, malonaldehyde, cholesterol oxidation products) and others. This review dealt briefly with the mechanism of the generation of those toxic substances in food systems, the factors affecting their generation, their levels in foods, safety-related considerations, and the mechanism of the toxicological effects of the substances.
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