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Zhengguo Zhang,Xiaoqin Feng,Xiao-Xia Yue,Fu-Qiang An,Wen-Xia Zhou,Jian-Feng Gao,Tuo-Ping Hu,Chin-Chuan Wei 한국화학공학회 2015 Korean Journal of Chemical Engineering Vol.32 No.8
Nitrogen-containing porous carbons, the 800SP-NH3, were synthesized using sunflower plates as the major carbon source carbonized at 800 oC and activated with concentrated aqueous ammonia at the same temperature. The porous carbons were characterized by nitrogen physical adsorption-desorption, surface area analyzer, FT-IR, and SEM. The adsorption properties of the porous carbons towards phenols were also investigated by batch methods. The test results show that the average pore diameter of porous carbon is smaller than 2 nm, and nitrogen-containing chemical groups are formed on its surface. The adsorption capacity for phenol, 4-chlorophenol, and p-nitrophenol is 316.5mg/g, 330.24mg/g and 387.62mg/g due to its developed pore structure and nitrogen-containing chemical groups. The adsorption isotherm data greatly obey the Langmuir model.
Detection of Sequence-Specific Gene by Multi-Channel Electrochemical DNA Chips
Zhang, Xuzhi,Ji, Xinming,Cui, Zhengguo,Yang, Bing,Huang, Jie Korean Chemical Society 2012 Bulletin of the Korean Chemical Society Vol.33 No.1
Five-channel electrochemical chips were fabricated based on the Micro-electromechanical System (MEMS) technology and were used as platforms to develop DNA arrays. Different kinds of thiolated DNA strands, whose sequences were related to white spot syndrome virus (WSSV) gene, were separately immobilized onto different working electrodes to fabricate a combinatorial biosensor system. As a result, different kinds of target DNA could be analyzed on one chip via a simultaneous recognition process using potassium ferricyanide as an indicator. To perform quantitative target DNA detection, a limit of 70 nM (S/N=3) was found in the presence of 600 nM coexisting noncomplementary ssDNA. The real samples of loop-mediated isothermal amplification (LAMP) products were detected by the proposed method with satisfactory result, suggesting that the multichannel chips had the potential for a high effective microdevice to recognize specific gene sequence for pointof-care applications.
Detection of Sequence-Specific Gene by Multi-Channel Electrochemical DNA Chips
Xuzhi Zhang,Xinming Ji,Zhengguo Cui,Bing Yang,Jie Huang 대한화학회 2012 Bulletin of the Korean Chemical Society Vol.33 No.1
Five-channel electrochemical chips were fabricated based on the Micro-electromechanical System (MEMS)technology and were used as platforms to develop DNA arrays. Different kinds of thiolated DNA strands,whose sequences were related to white spot syndrome virus (WSSV) gene, were separately immobilized onto different working electrodes to fabricate a combinatorial biosensor system. As a result, different kinds of target DNA could be analyzed on one chip via a simultaneous recognition process using potassium ferricyanide as an indicator. To perform quantitative target DNA detection, a limit of 70 nM (S/N=3) was found in the presence of 600 nM coexisting noncomplementary ssDNA. The real samples of loop-mediated isothermal amplification (LAMP) products were detected by the proposed method with satisfactory result, suggesting that the multichannel chips had the potential for a high effective microdevice to recognize specific gene sequence for pointof-care applications.
Kai Lv,Chengwu Shi,Zhengguo Zhang,Chengfeng Ma,Qi Wang 한국물리학회 2018 Current Applied Physics Vol.18 No.6
In this work, PbICl precursor solution in N,N-dimethylformamide was successfully applied to deposit PbS quantum-dots on TiO2 nanorod arrays by successive ionic layer adsorption and reaction method (SILAR). The influence of PbI2, PbBr2, PbICl precursor solution on the morphology, crystal size and optical absorption of PbS quantum-dots was investigated and the photovoltaic performance of the corresponding solid-state PbS quantumdot sensitized TiO2 nanorod array solar cells with spiro-OMeTAD was evaluated. The average crystal sizes of PbS quantum-dots were 9.0 nm of PbI2, 8.6 nm of PbBr2 and 8.4 nm of PbICl and the photoelectric conversion efficiency of the corresponding solar cells achieved 2.63%, 3.00%, 3.45%. The result revealed that PbICl precursor solution was superior to PbBr2 and PbI2.